Evaluation of Cu nano-colloid prepared by electrical wire explosion in liquid phase

액중 전기선폭발법으로 제조된 구리 나노콜로이드의 특성 평가

  • Yoon, Jae-Cheol (Powder Technology Research Group, Korea Institute of Materials Science) ;
  • Yang, Sang Sun (Powder Technology Research Group, Korea Institute of Materials Science) ;
  • Yu, Ji-Hun (Powder Technology Research Group, Korea Institute of Materials Science)
  • 윤재철 (한국기계연구원 부설 재료연구소 분말기술연구그룹) ;
  • 양상선 (한국기계연구원 부설 재료연구소 분말기술연구그룹) ;
  • 유지훈 (한국기계연구원 부설 재료연구소 분말기술연구그룹)
  • Received : 2010.03.02
  • Accepted : 2010.03.22
  • Published : 2010.03.30

Abstract

Cu nano-colloid was prepared by wire electric explosion process under de-mineralized water and anhydrous ethanol. To control the properties of Cu nano-colloid, experimental conditions such as diameter of Cu wire and applied voltage were changed. The optimal Cu nano-colloid was prepared when the 0.1mm diameter of Cu wire with the applied voltage of 2000 V was used. The shape of Cu particles in colloid was spherical and the XRD result revealed that the phase of Cu particles was cubic phase. About 20nm Cu nanoparticles with high crystallinity were successfully prepared using wire explosion process under anhydrous ethanol and they showed more than 100 hours dispersion stability.

Keywords

References

  1. Abraham, T. and Rittner, M. N.(1998), Nanostructured materials: An overview and commercial analysis, Journal of Metals, 50(1), 36-37.
  2. Kim, B. K.(2002), Journal of Korean Powder Metallurgy Institute, 9, 324.
  3. Gary, A., Gorge, C., and Hadjipanayis(1991), Science and Technology of nanostructured magnetic materials, New York, Plenum press, pp 1-176.
  4. Kim, Y. H.(2003), The effect of zeta-potential on the stabilization of silver nanoparticle colloid prepared by alcohol reduction method with PVP, Journal of Korean Industrial and Engineering Chemistry, 14(4), 487-492.
  5. Back, I. H., Cho, T. H., Lee, J. H., and Park, S. D.(2004), Stabilization of nanometer-sized silver-ethylene glycol colloid prepared with using ployacrylamide-co-acrylic acid, Journal of Korean Industrial and Engineering Chemistry, 15, 402-406.
  6. Gleiter, H.(2000), Nanostructured materials: Basic concepts and microstructure, Acta materialia, 48, 1-29. https://doi.org/10.1016/S1359-6454(99)00285-2
  7. Cahill, David, G., Jeffery, A. E., and Pawel, K.(2005), Nanofluids for thermal transport, Materials Today, 8, 36-44.
  8. Chace, W. G. and Moore(1964), Exploding wires, New York, Plenum press.
  9. Agnew, S. R., Elliot, B. R., Hemker, K. J., and Youngdahl, C. J.(2000), Microstructure and mechanical behavior of nanocrystalline metal, Materials Science and Engineering, 285(1-2), 391-396. https://doi.org/10.1016/S0921-5093(00)00669-9
  10. Kotov, Y. A. and Samatov, O. M.(1999), Production of nanometer sized A1N powder by the explosion wire method, Nanostructured Materials, 12, 119-122. https://doi.org/10.1016/S0965-9773(99)00078-1
  11. Chung, K. S., Eom, S. Y., Lee, J. C., Lee, H., and Yoo, E. A.(2008), Synthesis of highly concentrated $TiO_{2}$ nanocolloids and coating on boron nitride powder, Colloids and Surfaces A, 313-314, 175-178. https://doi.org/10.1016/j.colsurfa.2007.04.127
  12. Kim, J. H., Kim, R. H., and Kwon, H. S.(2008), Preparation of copper foam with 3-dimensionally interconnected spherical pore network by electrodeposition, Electrochemistry Communications, 10, 1148-1151. https://doi.org/10.1016/j.elecom.2008.05.035
  13. Huang, L., Kim, K. B., and Lee, E. S.(2005), Electrodeposition of monodisperse copper nanoparticles on highly oriented pyrolytic graphite electrode with modulation potential method, Colloids and Surfaces A, 262, 125-131. https://doi.org/10.1016/j.colsurfa.2005.03.023
  14. Furumi, S., Sakk, Y., and Shirahata, N.(2009), Micro-emulsion synthesis of blue-luminescent silicon nanoparticles stabilized with alkoxy monolayers, Journal of Crystal Growth, 311, 643-637.
  15. Meng, S., and Wu, S.(2006), Preparation of micron size copper powder with chemical reduction method, materials letters, 60, 2438-2442. https://doi.org/10.1016/j.matlet.2004.08.051
  16. Im, S., and Oh, S.(1999), Preparation of ultrafine nanoparticles in surfactant aggregate as a reaction medium, Applied Chemistry, 3, 168.
  17. Chang, W., Danforth, S. C., Kear, B. H., and Skandan, G.(1994), Chemical vapor condensation of nanostructured ceramic powders, Nanostructured Materials, 4(3), 345-351. https://doi.org/10.1016/0965-9773(94)90144-9
  18. Guk, Y. H., and Jo, S. C.(1995), Colloid and Surfactant, Dae Kwang, pp 9-26, 86-114.
  19. Jiang, W.(1998), Pulsed wire Discharge for nanosized Powedr Synthesis, Institute of Electrical and Electronics Engineers Transaction on Plasma Science, 26(5), 1498-1501.
  20. Shi, J., Wang, Q., Yang, H., and Zou, G.(2001), One-step synthesis of the nanometer particles of $\gamma-Fe_{2}O_{3}$ by wire electrical explosion method, Materials Research Bulletin, 36, 503-509. https://doi.org/10.1016/S0025-5408(01)00544-X
  21. Kim, J. S., Kwon, Y. S., Illyn, Jung, Y. H., and Yavorovsky, A. P.(2001), Ultra-fine powder by wire explosion method, Scripta materialia, 44, 2247-2251. https://doi.org/10.1016/S1359-6462(01)00757-6
  22. Beketov, T. I., Demina, A. M., Kotov, Y. A., Murzakaev, O. M., and Samatov(1995), Characteristics of ZrO2 nanopowders produced by electrical explosion of wire, Journal of Aerosol Science, 26, s905-s906. https://doi.org/10.1016/0021-8502(95)97360-Q
  23. Chakravarthy, S. R., Sarathi, R., and Sindhu, T. K.(2008), Understanding nanoparticle formation by a wire explosion process through experimental and modelling studies, Nanotechnology, 19, 1-11.
  24. Guangtian Z., Haibin Y., and Shushan D.(2001), Thermal characteristic of ultrafine-grained aluminum produced by wire electrical explosion, Scripta materialia, 44, 17-23. https://doi.org/10.1016/S1359-6462(00)00552-2
  25. De Groot, J. S., Sarkisov, G. S., and Vauer, B. S.(2001), Homogeneous electrical explosion of tungsten wire in vaccum, Journal of Experimental and Theoretical Physics Letter, 73, 69-74. https://doi.org/10.1134/1.1358422
  26. Kortkhonjia, V. P.(2003), On the role of exothermal chemical reaction during wire explosion in water, Techenical Physics Letter, 29, 797-800.
  27. Gerhard, E., Helena, S., Hermann, K., Jaroslaw, W., Paola, P. G., and Paul, A., (2009), The fundamentals of nano- and submicro-scaled ceramic particles incorporation into electrodeposited nickel layers: Zeta potential measurements, Surface & Coating Technology, 203, 1806-1814. https://doi.org/10.1016/j.surfcoat.2008.12.031
  28. Li, X., Wang, X., and Zhu, D.(2007), Evaluation on dispersion behavior of the aqueous copper nanosuspensions, Journal of colloid and Interface Science, 310, 456-463. https://doi.org/10.1016/j.jcis.2007.02.067
  29. Ahn, Y. C., Cheong, S. I., Hwang, Y., Jeong, Y. M., Kim, S. H. Lee, J. K., and Lee, J. K.(2008), Production and dispersion stability of nanoparticles in nanofluids, Powder Technology, 186, 145-153. https://doi.org/10.1016/j.powtec.2007.11.020
  30. Jung, S. J., Lee, S. J., and Lim, H. M.(2003), Effect of the concentration of suspension and electrolyte on zeta potential, Journal of the Korean ceramic Society, 40, 293-300. https://doi.org/10.4191/KCERS.2003.40.3.293