Bulletin of the Korean Chemical Society

  • 제30권10호
  • /
  • Pages.2265-2268
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  • 2009
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  • 0253-2964(pISSN)
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  • 1229-5949(eISSN)
대한화학회 (Korean Chemical Society)
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Polymorphic Forms of Furosemide Characterized by THz Time Domain Spectroscopy

  • Ge, Min (Shanghai Institute of Applied Physics, Chinese Academy of Sciences) ;
  • Liu, Guifeng (Shanghai Institute of Applied Physics, Chinese Academy of Sciences) ;
  • Ma, Shihua (Shanghai Institute of Applied Physics, Chinese Academy of Sciences) ;
  • Wang, Wenfeng (Shanghai Institute of Applied Physics, Chinese Academy of Sciences)
  • 발행 : 2009.10.20
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초록

Terahertz time domain spectroscopy (THz-TDS) is applied in transmission to identify the five forms of modifications of furosemide and one commercial product from 0.3 THz to 1.6 THz at room temperature. The different absorption spectra of the different forms are sensitive to crystal structures. Density function theory (DFT) calculation was used to understand the vibrational modes of furosemide in the THz region. X-ray powder diffractometry (XRPD) was applied to confirm the different forms of modifications. The results demonstrate that THz-TDS is a potential analytical technique in investigating polymorphic forms in the pharmaceutical fields.

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피인용 문헌

  1. High solubility crystalline hydrates of Na and K furosemide salts vol.16, pp.22, 2014, https://doi.org/10.1039/C3CE42347F
  2. Novel furosemide cocrystals and selection of high solubility drug forms vol.101, pp.2, 2009, https://doi.org/10.1002/jps.22805
  3. Optical properties of Meloxicam in the far-infrared spectral region vol.512, pp.None, 2009, https://doi.org/10.1016/j.chemphys.2018.04.022
  4. Characteristic terahertz absorption spectra of paramylon and paramylon-ester compounds vol.244, pp.None, 2009, https://doi.org/10.1016/j.saa.2020.118828