DOI QR코드

DOI QR Code

Sintering Behavior of Fe Nanopowder Agglomerates Prepared by Pressureless Compaction

비가압 성형한 Fe 나노분말응집체의 소결거동

  • You, Woo-Kyung (Department of Metallurgy and Materials Science, Hanyang University) ;
  • Jung, Sung-Soo (Department of Metallurgy and Materials Science, Hanyang University) ;
  • Lee, Jai-Sung (Department of Metallurgy and Materials Science, Hanyang University)
  • 유우경 (한양대학교 금속재료공학과) ;
  • 정성수 (한양대학교 금속재료공학과) ;
  • 이재성 (한양대학교 금속재료공학과)
  • Published : 2008.08.28

Abstract

Sintering behavior of iron nanopowder agglomerate compact prepared by slurry compaction method was investigated. The Fe nanopowder agglomerates were prepared by hydrogen reduction of spray dried agglomerates of ball-milled $Fe_2O_3$ nanopowder at various reduction temperatures of $450^{\circ}C$, $500^{\circ}C$ and $550^{\circ}C$, respectively. It was found that the Fe nanopowder agglomerates produced at higher reduction temperature have a higher green density compact which consists of more densified nanopowder agglomerates with coarsed nanopowders. The sintering behavior of the Fe nanopowder agglomerates strongly depended on the powder packing density in the compact and microstructure of the agglomerated nanopowder. It was discussed in terms of two sintering factors affecting the entire densification process of the compact.

Keywords

References

  1. P. Knorr, J. G. Nam and J. S. Lee: Metall. and Mater. Trans. A, A31 (2002) 503 https://doi.org/10.1007/s11661-000-0286-9
  2. J. S. Lee and Y. S. Kang: Scripta Mater., 44 (2001) 1591 https://doi.org/10.1016/S1359-6462(01)00780-1
  3. Y. S. Kang, B. H. Cha, H. G. Kang and J. S. Lee: Mater. Sci. Forum, 534 (2007) 505 https://doi.org/10.4028/www.scientific.net/MSF.534-536.505
  4. S. V. Divinski, F. Hisker, Y. S. Kang, J. S. Lee and Chr. Herzig: Z. Metallkd., 93 (2002) 256 https://doi.org/10.3139/146.020256
  5. S. V. Divinski, F. Hisker, Y. S. Kang, J. S. Lee and Chr. Herzig: Z. Metallkd., 93 (2002) 265 https://doi.org/10.3139/146.020265
  6. S. V. Divinski, F. Hisker, Y. S. Kang, J. S. Lee and Chr. Herzig: Interface Sci., 11 (2003) 67 https://doi.org/10.1023/A:1021587007368
  7. G. Petzow and H. E. Exner: Z. Metallkd, 67 (1976) 611
  8. J. S. Lee, W. A. Kaysser and G. Petzow: Modern Development in Powder Metallurgy, 15 (1985) 489
  9. J. S. Lee, H. G. Kang and Y. S. Kang: To be printed in the Proceedings of World Congress on PM 2008, MPIF, Washington D.C, 2008
  10. R. M. German: Particle Packing Characteristics, MPIF, Princeton, NJ, (1989) 141
  11. K. Ridgway and K. J. Tarbuck: Chemical and Process Engineering, 49(2) (1968) 103
  12. N. Epstein and M. J. Young: Nature, 196 (1962) 885 https://doi.org/10.1038/196885a0
  13. G. D. Scott and G. J. Kovacs: J. Physics D: Applied Physics, 6 (1973) 1007 https://doi.org/10.1088/0022-3727/6/8/314

Cited by

  1. A Feasibility Study on the Surface Hardening of Sintered Iron Nanopowder by Plasma Ion Nitriding vol.19, pp.1, 2012, https://doi.org/10.4150/KPMI.2012.19.1.013