한국재료학회지 (Korean Journal of Materials Research)

  • 제17권10호
  • /
  • Pages.548-554
  • /
  • 2007
  • /
  • 1225-0562(pISSN)
  • /
  • 2287-7258(eISSN)
한국재료학회 (Materials Research Society of Korea)
권호 표지
DOI QR코드

DOI QR Code

Preparation of BaTiO3 Thick Film by an Interfacial Polymerization Method

  • Iwasaki, Mitsunobu (Department of Applied Chemistry, School of Science & Engineering, Kinki University) ;
  • Park, Won-Kyu (Department of Material Engineering, Graduate School of Paichai University)
  • 발행 : 2007.10.27
PDF 다운로드
⟨ 이전 논문 다음 논문 ⟩

초록

[ $BaTiO_3$ ] thick film by an interfacial polymerization method was prepared at the liquid/liquid interface between benzyl alcohol saturated solution with the basic catalyst [diethyl amine ($NHEt_2$) or triethylamine ($NEt_3$)], and the water dissolved with $TiO_2$ and $Ba(CH_3COO)_2$. The film thickness increased gradually with an increase in diethyl amine($NHEt_2$) or triethylamine($NEt_3$) volume and the reaction time. The homogeneity of $BaTiO_3$ thick film after sintered at $600^{\circ}C$ was confirmed by EPMA analysis, which showed that both of Ba and Ti element were homogeneously distributed on the surface as well as in the perpendicular direction of the film. The thickness of $BaTiO_3$ film obtained by this process was $8.75\;{\mu}m$.

키워드

참고문헌

  1. A. I. Kingon and S. K.Streiffer, Current Opinion in Solid State & Materials Science, 4(1), 39 (1999) https://doi.org/10.1016/S1359-0286(99)80009-6
  2. J. Schwarzkopf and R. Fornari, Progress in Crystal Growth and Characterization of Materials, 52(3), 159 (2006) https://doi.org/10.1016/j.pcrysgrow.2006.06.001
  3. T. Asamaki, Introduction to the fabrication of thin films, Nikkan kogyoshinnbunn-sha (1984) (in Japanese)
  4. T. Chiba, K. Itoh and O.Matsumoto, Thin Solid Films, 300(1), 6 (1997) https://doi.org/10.1016/S0040-6090(96)09506-5
  5. Z. Jianming, W. Hong, W. Ming, S. Suxia, W. Zuo and L. Chenglu, Journal of Physics D, Applied Physics, 31 (19), 2416 (1998) https://doi.org/10.1088/0022-3727/31/19/009
  6. Fundamental knowledge of advanced materials, Ed. by Society of Materials Science, Japan (1991) (in Japanese)
  7. M. Yamane, M. Iwasaki and S. Ito, Ceramic Transactions, 81, 113 (1998)
  8. S. Saka, The science of sol-gel process, Chapter 9, Published by Agne Shouhusya (1998) (in Japanese)
  9. G. Munuera, A. R. Gonzalez-Elipe, A. Fernandez, P. Malet and J. P. Espinos, J. Chern. Soc. Faraday Trans., 1, 85(6), 1279 (1989) https://doi.org/10.1039/f19898501279
  10. C. F. Bass Jr., and R. E. Mesmer, The hydrolysis of cations, Krieger Publishing Company, 147 (1976)
  11. Experiments in inorganic qualitative analysis, Ed. by Kyoto University, Kyoritushuppan, (1994) (in Japanese)