Concentration of Polycyclic Aromatic Hydrocarbons in Cereals, Pulses, Potatoes, and their Products

곡류, 두류, 서류 및 그 가공품 중 다환 방향족 탄화수소 (polycyclic aromatic hydrocarbons) 화합물 함량

  • Kim, Hee-Yun (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Chung, So-Young (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Sho, Yo-Sub (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Park, Seong-Soo (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Lee, Eun-Ju (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Suh, Jung-Hyuk (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Lee, Yun-Dong (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Choi, Woo-Jeong (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Kim, Jung-Soo (Doosan R&D Center, Food Safety Research Team) ;
  • Eom, Ji-Yoon (Food Contaminant Division, Food Safety Evaluation Department, Korea Food and Drug Administration) ;
  • Park, Hui-Og (Department of Food and Drug, Chosun University) ;
  • Jin, Myeong-Sig (Department of Food and Drug, Chosun University) ;
  • Kim, Dong-Sul (Research Planning and Management Office, KFDA) ;
  • Ha, Sang-Chul (Department of Confectionary Decoration, Daegu Mirae College) ;
  • Lee, Jong-Ok (Test & Analytical Lab. Gyungin Regional KFDA)
  • 김희연 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 정소영 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 소유섭 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 박성수 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 이은주 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 서정혁 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 이윤동 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 최우정 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 김정수 (두산 R&D센터 식품안전연구팀) ;
  • 엄지윤 (식품의약품안전청 식품안전평가부 식품오염물질과) ;
  • 박희옥 (조선대학교 식품의약학과) ;
  • 진명식 (조선대학교 식품의약학과) ;
  • 김동술 (식품의약품안전청 연구기획조정담당관실) ;
  • 하상철 (대구미래대학 제과데코레이션과) ;
  • 이종옥 (경인지방식품의약품안전청 시험분석실)
  • Published : 2005.08.31

Abstract

Estimation of concentrations of PAHs [benzo(a)anthracene, chrysene, benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, dibenzo(a,h)anthracene, benzo(g,h,i)perylene, indeno(1,2,3-c,d)pyrene] in cereals, pulses, potatoes, and their products available in Korean markets gave mean levels of 0.13, 0.08, 0.06, 0.03, 0.08, 0.15, 0.45, and $0.14{\mu}g/kg$, respectively, with recoveries between 82.6-106.6%. Methodology involved saponification and extraction with n-hexane, purification on Sep-Pak Florisil cartridges, and high performance liquid chromatography using a fluorescence detector.

곡류, 서류, 두류 및 그 가공품 총 200건을 대상으로 benzo(a)pyrene등 8개 PAHs 화합물에 대하여 분석하였다. 시료 중 PAHs 화합물을 n-hexane으로 추출한 후 Sep-Pak Florisil cartridge로 정제한 후 HPLC-fluorescence로 분석하였다. 분석한 대상식품 중 PAHs 평균 함량은 각각 benzo(a)anthracene $0.13{\mu}g/kg$, chrysene $0.08{\mu}g/kg$, benzo(b)fluoranthene $0.06{\mu}g/kg$, benzo(k)fluoranthene $0.03{\mu}g/kg$, benzo(a)pyrene $0.08{\mu}g/kg$, dibenzo(a,h)anthracene $0.15{\mu}g/kg$, benzo(g,h,i)perylene $0.45{\mu}g/kg$, indeno(1,2,3-c,d)pyrene $0.14{\mu}g/kg$이었다.

Keywords

References

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