한국동물위생학회지 (Korean Journal of Veterinary Service)

  • 제26권2호
  • /
  • Pages.157-162
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  • 2003
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  • 3022-7372(pISSN)
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  • 2287-7630(eISSN)
한국동물위생학회 (The Korean Society of Veterinary Service)
권호 표지

식용란중 벤지미다졸계 구충제 분석

Analysis for benzimidazoles in eggs

  • 강형주 (충청남도축산위생연구소) ;
  • 김문배 (충청남도축산위생연구소) ;
  • 이재봉 (충청남도축산위생연구소) ;
  • 김봉식 (충청남도축산위생연구소) ;
  • 김영갑 (충청남도축산위생연구소)
  • Kang, Hyung-Joo (Chungnam Livestock & Veterinary Research Institute) ;
  • Kim, Mun-Bae (Chungnam Livestock & Veterinary Research Institute) ;
  • Lee, Jae-Bong (Chungnam Livestock & Veterinary Research Institute) ;
  • Kim, Bong-Sik (Chungnam Livestock & Veterinary Research Institute) ;
  • Kim, Young-Kab (Chungnam Livestock & Veterinary Research Institute)
  • 발행 : 2003.06.01
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초록

This stud was attempted to detect six benzimidazoles[thiabendazole(TBZ), oxfendazole(OFZ), mebendazole(MBZ), flubendazole(FLBZ), albendazole(ABZ), and febendazole(FBZ)] in eggs using high performance liquid chromatography(HPLC) with photodiode array detector(DAD) simultaneously. The eluates were determined by HPLC on a waters X-Terra$^{TM}\;C_{18}$ reverse-phase column($4.6{\times}250nm,\;5{\mu}m$) with DAD at 295nm. The mobile phase was 0.04M ammonium phosphate(pH 7.5)/ACN(62.28 v/v) run isocratically. The calibration curves were linear(r>0.999) for six benzimidazoles. Average recovery rate from eggs were 94.54% for TBZ, 97.71% for OFZ, 88.82% for MBZ, 93.71% for FLBZ, 78.61% for ABZ, and 75.09% for FBZ, respectively. The limits of detection and quantification were 2.27ppb, 3.88 for TBZ, 9.34ppb, 15.61ppb for OFZ, 28.53ppb, 45.15ppb for MBZ, 27.39ppb, 40.95ppb for FBZ, 8.61ppb, 13.95ppb for ABZ and 12.79ppb, 22.34ppb for FBZ, respectively.

키워드

참고문헌

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