Bulletin of the Korean Chemical Society

  • 제24권5호
  • /
  • Pages.555-558
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  • 2003
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  • 0253-2964(pISSN)
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  • 1229-5949(eISSN)
대한화학회 (Korean Chemical Society)
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Sorbent Extraction of Some Metal Ions on a Gas Chromatographic Stationary Phase Prior to Their Flame Atomic Absorption Determinations

  • Soylak, M. (Erciyes University, Faculty of Art and Science, Department of Chemistry) ;
  • Saracoglu, S. (Erciyes University, Faculty of Education) ;
  • Elci, L. (Pamukkale University, Faculty of Art-Science, Department of Chemistry)
  • 발행 : 2003.05.20
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초록

An enrichment/separation system for atomic absorption spectrometric determinations of Cu(Ⅱ), Fe(Ⅲ), Ni(Ⅱ) and Co(Ⅱ) has been established. The procedure is based on the adsorption of the analytes as calmagite chelates on Chromosorb-102. The effects of some parameters including pH, amount of ligand, salt matrix, flow rates of sample and eluent solutions were investigated. Under optimized conditions, the relative standard deviation of the combined method of sample treatment, preconcentration and determination with FAAS (N=5) is generally lower than 5%. The limit of detection (3σ) was between 6.0-112.9 ㎍/L. The results were used for preconcentration of analytes from some sodium and ammonium salt.

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