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Encapsulation of Pine Agaric ( Tricholoma matsutake) Flavor with Alginates

알긴산을 이용한 송이 향의 캡슐화

  • You Byeong Jin (Dept. Food Science, Kangnung National Univ) ;
  • Lim Yeong seon (East Coastal Marine Bioresources Research Center, Kangnung National Univ)
  • 유병진 (강릉대학교 식품과학과) ;
  • 임영선 (강릉대학교 해양생물자원센터)
  • Published : 2002.05.01

Abstract

Encapsulating 1-octen-3-ol with alginates solution, the effects of physical properties (viscosity, emulsion activity, emulsion stability) of alginates solutin on the retention of 1-octen-3-ol in capsules were investigated. Only alginates solutions haying less than 350 cP in viscosity were capable to be adopted to spray dry. Adding citric acid to alginates solution in order to reduce its viscosity, the concentration of citric acid became higher, the viscosity of alginates solution were lower. Adding $0.1\% of citric acid could reduce viscosity of alginates solution to 150 cP. The viscosity of alginates solution after emulsifying showed higher value than that of solution before emulsifying, but its viscosity were within the possible ranges for spray drying. The lower viscosity of alginates solution were, EAI became higher but ESI and amount of remaining 1-octen-3-ol in capsules were lower, In reducing the viscosity of alginates solutions, heating time after adding citric acid were longer, the their viscosity became lower. Differences of viscosity of alginates solution after and before emulsifying were little, In encapsulating raw pine agaric with alginates solution, the adding amount of soybean oil increased, the amounts of remaining 1-octen-3-ol in capsules increased. After freeze drying the amount of remaining 1-octen-3-ol in alginates capsules prepared with raw pine agaric was higher than that after cold air flow drying.

국내산 송이의 특징인 송이 향을 효과적으로 보존할 수 있는 방법을 개발하기 위하여 알긴산으로 송이 향의 주된 성분인 1-oc-ten-3-ol을 캡슐화 공정과 송이 향의 잔존량에 영향을 미치는 요인을 조사한 결과는 다음과 같다. 분무건조를 위한 alginates의 점도는 350cp 이하가 되어야 하므로, alginates 용액의 점도를 낮추기 위하여 첨가한 citric acid 량이 증가할수록 점도는 낮아졌으며, 또한 $0.1\%의 농도에서 150cp 이하의 점도를 나타내었다. 1-octen-3-ol과 유화제를 첨가하여 에멀젼시킨 alginates 용액의 점도는 에멀젼시키기 전의 점도보다 높았지만 150cp 이하를 나타내 분무 건조 공정에는 영향이 없었다. alginates 용액의 점도가 낮을수록 용액의 EAI는 증가하였으나 ESI는 감소하였고 캡슐의 1-octen-3-of의 잔존량이 감소하였다. alginates 용액의 점도를 낮추는 공정에서 citric acid 첨가 후 가열시간이 길어질수록 점도는 급격히 감소하였고 에멀전 전후의 점도는 큰 차이 없었다 생송이를 알긴 산용액으로 캡슐화할 때 첨가되는 대두유의 량이 많을수록 1-oc-ten-3-ol의 잔존량이 많았다. 생송이를 alginates용액으로 캡슐화한 후 진공동결건조한 캡슐이 풍건한 것보다 1-octen-3-ol의 잔존량이 많았다.

Keywords

References

  1. Ahn J.S. and K.H. Lee. 1986. Studies on the volatile aroma Com-pounds of edible mushroom (Tricholoma matsutake) of Korea. J. Korean Soc. Food Nutr., 15, 253-257 (in Korean)
  2. Anandaraman, S. and G.A. Reineccius. 1986. Stability of encapsulated orange peel oil. Food TechnoL, 40, 88-93
  3. Anker, M.H. and G.A. Reineccius. 1988. Encapsulated orange oil; In-fluence of spray-dryer air temperatures on retention and Shelf-life. In Flavor Encapsulation. ACS sym. Ser., 370, pp. 78-86 https://doi.org/10.1021/bk-1988-0370.ch009
  4. Chattopadhyaya, S., R.S. Singhal and P.R. Kulkarni. 1998. Oxidised starch as gum arabic substitute for encapsulation of flavours. Carbohydrate Polymers, 37, 143-144 https://doi.org/10.1016/S0144-8617(98)00054-X
  5. Ducan, D.B. 1955. Multiple-range and multiple F tests. Biometrics, 11 1-42 https://doi.org/10.2307/3001478
  6. Haug, A., B. Lasen and 0. Smidsr$\phi$d. 1966. A study of the Constitu-tion of alginic acid by partial acid hydrolysis. Acta Chem. Scand., 20, 183-190 https://doi.org/10.3891/acta.chem.scand.20-0183
  7. Kim, Y.D. and C.V. Morr. 1996. Microencapsulation properties of gum arabic and several food proteins: Spray-dried orange oil emulsion particles. J. Agric. Food Chem., 44, 1314-1320 https://doi.org/10.1021/jf9503927
  8. Kim, Y.D., C.V. Morr and T.W. Schenz. 1996. Microencapsulation properties of gum arabic and several food proteins: Liquid orange oil emulsion particles. J. Agric. Food Chem., 44, 1308-1313 https://doi.org/10.1021/jf950391e
  9. Lacroix, C., C. Paquin and J.P. Amaud. 1990. Batch fermentation with entrapped growing cells of Lactobacillus casei. Appl. Micro-biol. Biotechnol., 32, 403-408 https://doi.org/10.1007/BF00903773
  10. Muka, J.R. and D.B. Nelson. 1988. Preparation of encapsulated flavors with high flavor level. Modified procedures now allow preparation of encapsulated flavors with flavor levels over twice that of prior commercial products. Food Technol, 42, 154-157
  11. Pearce K.N. and J.E. Kinsella. 1978. Emulsifying properties of Pro-teins: evaluation of turbidimetnc technique. Agric. Food Chem., 26, 716-723 https://doi.org/10.1021/jf60217a041
  12. Reineccius G.A. 1991. Carbohydrates for flavor encapsulation; Malto-dextrins, corn syrup solids, modifed starch, and gum acasia each have strengths and weaknesses in flavor encapsulation. Food Tech., 45, 144-149
  13. Risch, S.J. and G.A. Reineccius. 1986. Flavor encapsulation. Symp. Series 370. Am. Chem. Soc., Washington, D.C
  14. Skopec, R.A., P.E. Collee and L.K. Shallenberger. 1995. High-viscosity gel encapsulation for core preservation and improved reservoir evaluation. J, Pet. Tech., 5, 399
  15. Subramania, A. 1997. Starch-encapsulated flavours. U.S. Patent US55 06353 in Trends in Food Sci. & Technol., 8, 95
  16. Yilmaz, G., R.O.J. Jongboom, J.J.G. van Soest and H. Feil. 1999. Effect of glycerol on the morphology of starch-sunflower oil composites. Carbohydrates Polymers, 38, 33-39 https://doi.org/10.1016/S0144-8617(98)00086-1
  17. You, B.J. and J.M. Shim. 1999a. Effects of extracting conditions on film properties of seatangle alginates. J. Korean Fish. Soc., 32, 664-668 (in Korean)
  18. You, B.J. and J.M. Shim. 1999b. Effects of processing conditions on physical properties of alginates film. J. Korean Fish. Soc., 32, 582-586 (in Korean)
  19. You, B.J. and J.M. Shim. 2000. Effects of processing conditions of seatangle (Laminana spp.) alginates film on permeability of ester compounds. J. Korean Fish. Soc., 33, 143-147 (in Korean)
  20. Ziberboim, R., I.J. Kopelman and Y. Talmon. 1986. Microencapsula-tion by a dehydrating liquid: Retention of paprika oleresin and aromatic esters. J. Food Sci., 51, 1301-1306 https://doi.org/10.1111/j.1365-2621.1986.tb13110.x
  21. 박중곤. 1999. 국내허브산업의 현황과 발전방향.고려대 자연자원대학원석사학위 논문