DOI QR코드

DOI QR Code

Mixed Micellar Properties of Sodium n-Octanoate(SOC) with n-Octylammonium Chloride(OAC) in Aqueous Solution

Sodium n-Octanoate(SOC)와 n-Octylammonium Chloride(OAC)의 혼합마이셀화에 관한 연구

  • Lee, Byeong Hwan (Department of Applied Chemical Engineering, Korea University of Technology)
  • 이병환 (한국기술교육대학교 응용화학공학과)
  • Published : 2002.12.20

Abstract

The critical micelle concentration(CMC) and the counterion binding constant(B) for the mixed micel-lization of sodium n-octanoate(SOC) with n-octylammonium chloride(OAC) were determined as a function of the overall mole fraction of $SOC({\alpha}_1).$ Various thermodynamic parameters($x_i$, $Y_i$, $C_i$, $${\alpha}_i^M$$, and $\Delta$$H_{mix}$) for the mixed micellization of the SOC/OAC systems have been calculated and analyzed by means of the equations derived from the nonideal mixed micellar model. The results show that there are great deviations from the ideal behavior for the mixed micellization of these systems. And other thermodynamic parameters(${\Delta}$$G^0_m$, ${\Delta}$$H^0_m$, and ${\Delta}$$S^0_m$) associated with the micellization of SOC,OAC, and their $mixture({\alpha}_1=0.5)$ have been also estimated from the temperature dependence of CMC and B values, and the significance of these parameters and their relation to the theory of the micelle formation have been considered and analyzed by comparing each other.

Sodium n-Octanoate(SOC)와 n-Octylammonium Chloride(OAC)의 혼합마이셀화에 대하여 연구하기 위하여 임계마이셀농도(CMC)와 반대이온 결합상수(B)값을 SOC의 겉보기 몰분율($\alpha_1$)을 변화시키면서 측정하였다. SOC/OAC 혼합시스템의 마이셀화에 대한 여러 가지 열역학적 함수값($x_i$, $Y_i$, $C_i$, ${\alpha}_i^M$${\Delta}H_{mix}$)을 비이상적 혼합마이셀화 모델에 의하여 계산하고 분석하였다. 그 결과 이러한 혼합계면활성제의 마이셀화는 이상적 거동으로부터 큰 음의 벗어남을 알 수 있었다. 그리고 SOC,OAC 및 그들 혼합체($\alpha_1$=0.5)의 마이셀화에 대한 열역학적 함수값(${\Delta}G^0_m$, ${\Delta}H^0_m$${\Delta}S^0_m$)을 계산하기 위하여 온도에 따른 CMC 및 B 값의 변화를 측정하였다. 이러한 변화로부터 계산한 열역학적 함수값을 상호 비교함으로써 순수 및 혼합계면활성제의 마이셀화에 대하여 분석하였다.

Keywords

References

  1. Holland, P. M. In Mixed Surfactant Systems; Holland,P. M.; Rubingh, D. D., Ed.; ACS Symposium Series;Washington DC., U. S. A., 1992; p. 31.
  2. Park, J. W.; Chung, M. A.; Choi, K. M. Bull. KoreanChem. Soc. 1989, 10, 437.
  3. Bergstrom, M.; Eriksson, J. C. Langmuir 2000, 16,7173. https://doi.org/10.1021/la000397k
  4. Matsubara, H.; Muroi, S.; Kameda, M.; Ikeda, N.;Ohta, A.; Aratono, M. Langmuir 2001, 17, 7752. https://doi.org/10.1021/la0104020
  5. Bai, G.; Wang, J.; Yan, H.; Li, Z.; Thomas, R. K. J.Phys. Chem. B 2001, 105, 9576. https://doi.org/10.1021/jp010975l
  6. Kresheck, G. C. J. Phys. Chem. B 2001, 105, 4380. https://doi.org/10.1021/jp004022j
  7. Matsubara, H.; Ohta, A.; Kameda, M.; Ikeda, N.; Aratono,M. Langmuir 2000, 16, 7589. https://doi.org/10.1021/la991499h
  8. Clint, J. H. In Surfactant Aggregation; Chapman andHall; New York, 1992; p. 130.
  9. Kamrath, D. F.; Franses, E. I. In Surfactants in Solution;Mittal K. L. Ed.; Plenum Press; New York, U. S.A., 1984; p. 129.
  10. Kamrath, D. F.; Franses, E. I. J. Phys. Chem. 1984, 88,1642. https://doi.org/10.1021/j150652a041
  11. Lee, B. H. J. Kor. Chem. Soc. 1999, 43, 614.
  12. Lee, B. H. J. Kor. Chem. Soc. 1998, 42, 519.
  13. Chung, J. J.; Kim, Y. C.; Lee, B. H. J. Kor. Chem. Soc.1997, 41, 284.
  14. Chung, J. J.; Lee, S. H.; Kim, Y. C.; Lee, B. H. J.Korean Ind. & Eng. Chemistry 1998, 9, 968.
  15. Lee, B. H. J. Kor. Chem. Soc. 1997, 41, 12.
  16. De Lesi, R.; Inglese, A.; Milioto, S.; Pellerito, A. J.Colloid & Interface Sci. 1996, 180, 174. https://doi.org/10.1006/jcis.1996.0287
  17. Semchyschyn, D. J.; Carbone, M. A.; MacDonald, P.M. Langmuir 1996, 12, 253. https://doi.org/10.1021/la950244a
  18. Kamenka, N.; Burgaud, I.; Zana, R.; Lindman, B. J.Phys. Chem. 1994, 98, 6785. https://doi.org/10.1021/j100078a021
  19. Zana, R.; Levy, H. Langmuir 1997, 13, 402. https://doi.org/10.1021/la9606963
  20. Chatterjee, A.; Moulik, S. P.; Sanyal, S. K.; Mishra, B.K.; Puri, P. M. J. Phys. Chem. B 2001, 105, 12823. https://doi.org/10.1021/jp0123029
  21. Shanks, P. C.; Franses, E. I. J. Phys. Chem. 1992, 96,1794. https://doi.org/10.1021/j100183a055
  22. Holland, P. M.; Rubingh, D. N. J. Phys. Chem. 1983,87, 1984. https://doi.org/10.1021/j100234a030
  23. Rathman, J. F.; Christian, S. D. Langmuir 1990, 6, 391. https://doi.org/10.1021/la00092a018
  24. Zana, R.; Levy, H.; Papoutsi, D.; Beinert, G. Langmuir1995, 11, 3694. https://doi.org/10.1021/la00010a018
  25. Lee, B. H. J. Kor. Chem. Soc. 2000, 44, 177.
  26. Lee, B. H. J. Kor. Chem. Soc. 2001, 45, 7.

Cited by

  1. Studies on Mixed Micellizations of Sodium Dodecanoate and Sodium Octanoate by Means of Electric Conductivity and Light Scattering vol.59, pp.4, 2015, https://doi.org/10.5012/jkcs.2015.59.4.271
  2. DPC와 CDEAB의 혼합마이셀화에 미치는 n-부탄올의 효과 vol.48, pp.3, 2002, https://doi.org/10.5012/jkcs.2004.48.3.236