Effect of Fuel on Synthesis of Nanocrystalline Ni particles by a Combustion Synthesis Process

연소합성법을 이용한 Ni 분말 합성에서 첨가 연료의 영향

  • 정충환 (한국원자력연구소 원자력재료기술개발팀 기능성재료) ;
  • 신형철 (충남대학교 공과대학 재료공학과) ;
  • 이희균 (한국원자력연구소 원자력재료기술개발팀 기능성재료) ;
  • 홍계원 (한국원자력연구소 원자력재료기술개발팀 기능성재료) ;
  • 윤순길 (충남대학교 공과대학 재료공학과)
  • Published : 2001.03.01

Abstract

Ni and NiO particles were made by a combustion synthesis process. The characteristics of synthesized powders were investigated with various kinds and amounts of fuels such as urea, citric acid and glycine. Ni phase particles without NiO phase were obtained through combustion synthesis process in air atmosphere with-out further calcinations process, when the content of glycine was 2.44 times of the stoichiometric ratio in the precursor solution. Primary particle sizes of synthesized Ni and NiO particles were about 20∼30 nm.

Keywords

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