The Korean Journal of Ceramics

한국세라믹학회 (The Korean Ceramic Society)
권호 표지

Prepartion and Characterization of the Pt doped $TiO_2$ Membranes

  • Bae, Dong-Sik (Div. of Ceramics, Korea Insitute of Sci. and Tech., Seoul) ;
  • Han, Kyong-Sop (Div. of Ceramics, Korea Institute of Sci. and Tech) ;
  • Choi, Sang-Hael (Dept. of Inorg. Mat. Engineering, Hanyang Univ)
  • 발행 : 1997.03.01
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초록

The Pt doped $TiO_2$ composite membranes were prepared by the sol-gel process. The Pt doped titania sol was peptized with hydrochloric acid in the pH range of 1.23 to 1.32 at 5$0^{\circ}C$. The average particle size of the Pt doped titania sol was shown to be below 15nm and well dispersed in the solution. XPS show the Pt elements continuous and homogeneous dispersed in the $TiO_2$ membrane. The mean particle size of the Pt doped $TiO_2$ composite membrane has smaller than that of the undoped $TiO_2$ composite membrane. The average pore size of the Pt doped $TiO_2$ composite membrane was increased from 58 to 193 $\AA$ with firing temperature changed from 550 to 85$0^{\circ}C$. It was observed that the Pt doped $TiO_2$ composite membranes showed crack-free and homogeneous microstructue as well as narrow particle size distribution up to above 75$0^{\circ}C$.

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