대한약학회:학술대회논문집 (Proceedings of the PSK Conference)

대한약학회 (The Pharmaceutical Society of Korea)
권호 표지

Analysis of DA-6034. a New Flavonoid Derivative in Biological Fluids by Fluorescence Detector

  • Jang, Ji-Myun (Research Laboratories, Dong-A Pharmaceutical Co., Ltd.) ;
  • Park, Kyung-Jin (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Lee, Jong-Jin (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Kim, Dong-Goo (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Shim, Hyun-Joo (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Son, Mi-Won (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Kim, Dong-Sung (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Kim, Soon-Hoe (Research Laboratories, Dong-A Pharmaceutical Co., Ltd) ;
  • Yoo, Moo-Hi (Research Laboratories, Dong-A Pharmaceutical Co., Ltd.)
  • 발행 : 2002.10.01
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초록

A high performance liquid chromatographic method was developed for the determination of DA-6034 in biological fluids using fluorescence detector. The method involved deproteinization of biological sample with the same volume of acetonitrile, 0.2M zinc sulphate. and 0.15M barium hydroxide. The aliquot of supernatant was injected onto Nova-pak C18 column and detected by fluorescence detector. Emission and excitation wavelength of detector were 336nm and 440nm. (omitted)

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