대한약학회:학술대회논문집 (Proceedings of the PSK Conference)

대한약학회 (The Pharmaceutical Society of Korea)
권호 표지

Simultaneous determination of corticosteroids in a herbal medicinal preparation by GC-MS

  • Jeong, Jae-Chul (Durg Analysis Lab., Supreme Public Prosecutor′s Office) ;
  • Kim, Jin (Division of Medicinal Chemistry, Korea Food ＆Drug Administratio) ;
  • Kim, Mee-Jung (Department of Chemistry, Graduate School, Yonsei University) ;
  • Choi, Don-Woong (Department of Chemistry, Graduate School, Yonsei University) ;
  • Chang, Seung-Yeup (Department of Chemistry, Graduate School, Yonsei University) ;
  • Im, Moon-Kyo (Department of Chemistry, Graduate School, Yonsei University) ;
  • Paeng, Ki-Jung (Department of Chemistry, Graduate School, Yonsei University)
  • 발행 : 2002.10.01
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초록

The determination method for 11 corticosteroids (betamethasone, cortisol. cortisone, cortisone acetate. dexamethasone. cortisol acetate, isoflupredone acetate, methylprednisolone. prednisone, prednisolone, and triamcinolone acetonide) in a herbal medicinal preparation (Sibjeondaibotang) by a gas chromatography-mass spectrometric (GC-MS) method with selected ion monitoring (SIM) mode is described. Samples (4 mL) were extracted by liquid-liquid extraction with diethyl ether. (omitted)

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