• Title/Summary/Keyword: zone melting

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Superconducting Properties of (Sm/Y)-Ba-Cu-0 High Tc Composite Superconductors with CeO2 Additive by Zone-Melt Textured Growth (국부용융성장법으로 제조한 (Sm/Y)-Ba-Cu-0계 고온복합초전도체의 CeO2첨가에 따른 초전도특성)

  • 김소정
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.3
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    • pp.269-274
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    • 2002
  • (Sm/Y)-Ba-Cu-O system high Tc composite superconductors with/without $CeO_2$ additive were directionally grown by zone-melting process, haying large temperature gradient, In air atmosphere. Cylindrical green rods of $({Sm/y})_{1.8}Ba_{2.4}Cu_{3.4}O_x$ [(Sm/Y)1.8] composite oxides by cold isostatic pressing(CIP) method using rubber mold were fabricated. The microstructure and superconducting properties were investigated by XRD, SEM, TEM and SQUID magnetometer. The size of nonsuperconducting $({Sm/y})_2BaCuO_5$ inclusions of the melt-textured (Sm/Y)1.8 sample with CeO$_2$ additive were remarkably reduced and uniformly distributed within the superconducting (Sm/Y)1.8 matrix. Both samples, with/without $CeO_2$ additive, showed an onset Tc $\geq$ 90 K and sharp superconducting transition. The critical current density Jc value of the $CeO_2$ addictive were $1{\times}10^5A/\textrm{cm}^2$ in 77 K, 0 Tesla.

A Study on the Formation Mechanism of Discontinuities in $CO_2$ Laser Fusion Zone of Fe-Co-Ni Sintered Segment and Carbon Steel (Pe-Co-Ni 분말 소결 금속과 탄소강의 이종재료간 레이저 용접부의 결함형성기구 연구)

  • 신민효;김태웅;박희동;이창희
    • Journal of Welding and Joining
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    • v.21 no.3
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    • pp.58-67
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    • 2003
  • In this study, the formation mechanism of discontinuities in the laser fusion zone of diamond saw blade was investigated. $CO_2$ laser weldings were conducted along the butt between Fe base sintered tip and carbon steel shank with sets of variable welding parameters. The effect of heat input on irregular humps, outer cavity, inner cavity and bond strengh was evaluated. The optimum heat input to have a proper humps was in the range of 10.4~$17.6kJm_{-1}$. With increasing heat input, both outer and inner cavities were reduced. The outer cavity was caused by insufficient refill of keyhole, while inner cavity was caused by trapping of bubble in molten metal. The bubble came from sintered tip and intensive vaporization at bottom tip of the keyhole. A gas formation and low melting point element vaporization were not occurred during welding. We could not find any relationship between bond strength and amount of discontinuities. Because the fracture were occurred in not only sintered tip but also carbon steel shank due to hardness distributions.

A study on an efficient prediction of welding deformation for T-joint laser welding of sandwich panel PART I : Proposal of a heat source model

  • Kim, Jae Woong;Jang, Beom Seon;Kim, Yong Tai;Chun, Kwang San
    • International Journal of Naval Architecture and Ocean Engineering
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    • v.5 no.3
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    • pp.348-363
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    • 2013
  • The use of I-Core sandwich panel has increased in cruise ship deck structure since it can provide similar bending strength with conventional stiffened plate while keeping lighter weight and lower web height. However, due to its thin plate thickness, i.e. about 4~6 mm at most, it is assembled by high power $CO_2$ laser welding to minimize the welding deformation. This research proposes a volumetric heat source model for T-joint of the I-Core sandwich panel and a method to use shell element model for a thermal elasto-plastic analysis to predict welding deformation. This paper, Part I, focuses on the heat source model. A circular cone type heat source model is newly suggested in heat transfer analysis to realize similar melting zone with that observed in experiment. An additional suggestion is made to consider negative defocus, which is commonly applied in T-joint laser welding since it can provide deeper penetration than zero defocus. The proposed heat source is also verified through 3D thermal elasto-plastic analysis to compare welding deformation with experimental results. A parametric study for different welding speeds, defocus values, and welding powers is performed to investigate the effect on the melting zone and welding deformation. In Part II, focuses on the proposed method to employ shell element model to predict welding deformation in thermal elasto-plastic analysis instead of solid element model.

The Properties and Processing of Bismuth and Indium Added Sn-Cu-Ni Solder Alloy System (Bi, In을 함유한 Sn-Cu-Ni계 솔더 합금 제조와 물성)

  • 박종원;최정철;최승철
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.1
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    • pp.21-28
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    • 2002
  • Bismuth and Indium added Sn-Cu-Ni solder alloy was investigated for a new lead free solder. The thermal, electrical and mechanical properties were characterized for the Sn-0.7%(Cu+Ni) solder alloy by adding 2~5% Bi and 2~ 10% In. The melting point of solder alloy was in range of 200 to $222^{\circ}C$ and the mushy zone was in range of 20 to $37^{\circ}C$. This alloys could be adapted to middle and high temperature solder materials. A new solder alloy composition. Sn-0.7%(Cu+Ni) -3.5%Bi-2%In is very promising with high performance and effective cost. The melting point was $220^{\circ}C$, the mushy zone range was $25^{\circ}C$, and mechanical, electrical and wetting properties were competitive with those of other lead-free solder except the lower elongation value.

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A study on the laser surface hardening of SM 45C steel (SM 45C강의 레이저 표면경화처리에 관한 연구)

  • 나석주;김성도;이건이;김태균
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.11 no.1
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    • pp.53-62
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    • 1987
  • High power lasers provide a controllable and precise energy source in surface transformation hardening. A careful control of the process is needed in order that the surface layer of the material reaches the austenizing temperature, but that it does not melt. In order to achieve this the results of theoretical and experimental studies on the laser surface hardening of a medium carbon steel are described. A two-dimensional computer program, which can be used generally for the determination of transient temperature distributions in welding and heat treatment, was established on the basis of the finite element method. For the confirmation of the accuracy of the numerical analysis, a medium carbon steel (SM 45C) of 5mm thickness was heat-treated with a 1kW CW CO$_{2}$ laser machine, while the traverse speed and the distance from the focal point (defocused distance) were varied. Experimental and numerical results showed a similar tendency in correlations between the hardened zone shape and the process parameters. With increasing beam spot diameter the width and depth of the hardened zone increased for relatively small beam spot diameters, but decreased rapidly after reaching the maximum value, while with increasing traverse speed the width and depth of the hardened zone decreased monotonously. Too small beam spot diameters are to be avoided, since the surface melting would lower the surface hardness and produce an uneven surface which may be unacceptable because of the possible requirement for subsequent machining. It could be observed that for a given traverse speed and laser power input there exists a optimal range of the beam spot diameter, which produce a large width of the hardened zone but no melting on the surface.

Effects of microstructures of the sintered rod on the single crystal grown by the floating zone method (Floating zone법에 의한 결정성장시 소결봉의 미세구조에 의한 영향)

  • 신재혁;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.3
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    • pp.250-260
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    • 1995
  • In general, a sintered rod is used as a feed in the growth of crystals by the floating zone(FZ) method. The sintering condition of the feed rod affected the stability of molten zone because it influenced the interface shape between the feed and the melt during the crystal growth. In this study, rutile and ruby crystals were chosen as samples to analyze the effect of the microstructures of the feed rods. In sintering of the feed rod for the growth of rutile and ruby single crystals, the difference of grain size between the inner and the outer region of the feed rod increased with the sintering temperature and dwelling time. As a result, it altered melting behavior of the feed. The uniform grain size of the sintered rod was necessary for the optimum growing condition of crystals. The effect of pores in the feed rod was not a dominant factor to grow crystals by the FZ method, which was confirmed by growing crystals with nonsinterd rods as feeds.

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Hot Wire Laser Welding of Multilayer for Narrow Gap - Analysis of Wire Melting/Transfer and Arc Formation Phenomenon by High Speed Imaging - (내로우 갭 적용을 위한 핫와이어 송급 레이저용접 - 고속촬영을 통한 와이어 용융/이행 현상과 아크 포메이션 분석 -)

  • Kim, Kyounghak;Bang, Hansur;Bang, Heeseon;Kaplan, Alexander F.H.;Nasstrom, Jonas;Frostevarg, Jan
    • Journal of Welding and Joining
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    • v.34 no.5
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    • pp.26-32
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    • 2016
  • In this study, Hot-wire laser welding (HWLW) without keyhole which deposits filler material by feeding hot wire into the process zone has been performed to increase process performance. From the analysis of High Speed Imaging (HSI), for higher voltage, the process is prone to arc formation and drop transfer, which is disagreeable transfer mode. It is necessary that arc formation and drop (globular) transfer should be avoided by lower voltage. Therefore, continuous wire melting and transfer mode is preferred when adopting this process. The HWLW technique has high potential in terms of performance, precision, robustness and controllability for thick section of narrow gap.

Petrochemical Characteristics and Review on Petrogenesis on Cretaceous to Tertiary Volcanic Rocks in the Kyongsang Basin (경상분지 백악기~제3기 화산암류의 암석화학적 특징과 암석 성인 고찰)

  • Sung, Jong-Gyu;Kim, Jin-Seop
    • The Journal of the Petrological Society of Korea
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    • v.21 no.2
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    • pp.217-233
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    • 2012
  • Major elements abundances of Cretaceous to Tertiary volcanic rocks in Kyongsang basin are similar with Southern Volcanic Zone (SVZ) in Andes. Sr, K, Rb, $Ba{\pm}Th$ abundances, which have low ionic charge, are selectively fertile, on the other hand Ta, Nb, Ce, P, Zr, Hf, Sm, Ti, Y, Yb, Sc, Cr abundances are low. K, Sr, Th show characteristic spikes and Nb show remarkable trough on trace elements spider diagram. Trace elements abundances are higher than that of Andes which is supposed to mantle sources of Kyongsang basin volcanic rocks are produced lower degree of partial melting than SVZ in Andes.

Modeling of burning surface growth and propagation in AP-based composite propellant combustion (AP추진제의 연소면 형성 및 전파 모델링 연구)

  • Jung, Tae-Yong;Kim, Ki-Hong;Yoo, Ji-Chang;Do, Young-Dae;Kim, Hyung-Won;Yoh, Jai-Ick
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.05a
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    • pp.191-195
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    • 2009
  • In the solid rocket propellant combustion, dynamic phase change from solid to liquid to vapor occurs across the melt layer. During the burning surface, micro scale bubbles form as liquid and gas phases are mixed in the intermediate zone between the propellant and the flame. The experimentally measured thickness of this layer called the foam layer is approximately 1 micron at 1 atmosphere. In this paper, we present a new melting layer model derived from the classical phase change theory. The model results show that the surface of burning grows and propagate uniformly at a velocity of $r=ap^n$.

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A Study on the Fiber Laser welding of Ultra-Low Carbon Interstitial Free Steel for Automotive (자동차용 무침입형 극저탄소강의 파이버 레이저 용접에 대한 연구)

  • Oh, Yong-Seok;Shin, Ho-Jun;Yang, Yun-Seok;Hwang, Chan-Youn;Yoo, Young-Tae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.20 no.3
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    • pp.342-349
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    • 2011
  • The purpose of this paper is to describe experimental results about the butt welding and bead on plate welding of the high power Continuous Wave (CW) Fiber laser for Ultra-low carbon Interstitial Free(IF) steel plate for gear part of car. After being welded of the gear parts by the fiber laser and electron beam Microstructures of melting zone had been mixed acicular, granular bainitic, quasi-polygonal and widmanstatten ferrite because of a radical thermal diffusion after welding, difference of critical volume and grain size. As a result of experiment, when gear parts were welded by the fiber laser and electron beam, the fiber laser welding has been stable properties without internal defects more than the electron beam welding. Therefore it has the very advantages of welding high quality and productivity more than conventional melting method. The optimal welding processing parameters for gear parts were as follows : the laser power and welding speed were 3kWatt, 30mm/sec respectively. At this time heat input was $21.2{\times}10^3J/cm^2$.