• 제목/요약/키워드: wetting test

검색결과 201건 처리시간 0.027초

Bioactive characteristics of an implant surface coated with a pH buffering agent: an in vitro study

  • Pae, Hyung-Chul;Kim, Su-Kyoung;Park, Jin-Young;Song, Young Woo;Cha, Jae-Kook;Paik, Jeong-Won;Choi, Seong-Ho
    • Journal of Periodontal and Implant Science
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    • 제49권6호
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    • pp.366-381
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    • 2019
  • Purpose: The purpose of this study was to evaluate the effectiveness of conventional sandblasted, large-grit, acid-etched (SLA) surface coated with a pH buffering solution based on surface wettability, blood protein adhesion, osteoblast affinity, and platelet adhesion and activation. Methods: Titanium discs and implants with conventional SLA surface (SA), SLA surface in an aqueous calcium chloride solution (CA), and SLA surface with a pH buffering agent (SOI) were prepared. The wetting velocity was measured by the number of threads wetted by blood over an interval of time. Serum albumin adsorption was tested using the bicinchoninic acid assay and by measuring fluorescence intensity. Osteoblast activity assays (osteoblast adhesion, proliferation, differentiation, mineralization, and migration) were also performed, and platelet adhesion and activation assays were conducted. Results: In both the wetting velocity test and the serum albumin adsorption assay, the SOI surface displayed a significantly higher wetting velocity than the SA surface (P=0.000 and P=0.000, respectively). In the osteoblast adhesion, proliferation, differentiation, and mineralization tests, the mean values for SOI were all higher than those for SA and CA. On the osteoblast migration, platelet adhesion, and activation tests, SOI also showed significantly higher values than SA (P=0.040, P=0.000, and P=0.000, respectively). Conclusions: SOI exhibited higher hydrophilicity and affinity for proteins, cells, and platelets than SA. Within the limits of this study, it may be concluded that coating an implant with a pH buffering agent can induce the attachment of platelets, proteins, and cells to the implant surface. Further studies should be conducted to directly compare SOI with other conventional surfaces with regard to its safety and effectiveness in clinical settings.

플럭스 활성도 및 In 첨가에 따른 Sn-0.3Ag-0.7Cu 솔더 조성의 젖음 특성 변화 (Wettability Evaluation of Sn-0.3Ag-0.7Cu Solder Alloy with Different Flux Activity and Indium Addition)

  • 유아미;김준기;김목순;현창용;이종현
    • 마이크로전자및패키징학회지
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    • 제15권4호
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    • pp.51-57
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    • 2008
  • 저 Ag 함유 Sn-Ag-Cu계 무연솔더 조성, 즉, Sn-0.3Ag-0.7Cu 조성의 젖음 특성과 반응 특성을 Sn-1.0Ag-0.5Cu 및 Sn-3.0Ag-0.5Cu 합금 조성의 결과와 비교, 분석하였다. 또한 Sn-0.3Ag-0.7Cu 조성의 용융 특성을 시차주사열량계(differential scanning calorimeter, DSC)로 측정하고, 인장시험을 통한 응력-변형률 곡선을 관찰하였다. 아울러 Sn-0.3Ag-0.7Cu 조성의 젖음 특성을 향상시키기 위해 halide의 함유량이 많은 플럭스(flux)를 적용하거나 Sn-0.3Ag-0.7Cu 조성에 0.2wt.%의 In을 첨가하여 그 젖음 특성의 개선 정도를 분석해 보았다. 그 결과 halide 함유량이 높은 플럭스를 사용한 경우보다 미량의 In을 첨가한 경우가 $230{\sim}240^{\circ}C$의 저온 영역에서 wettability의 향상에 보다 효과적임을 관찰할 수 있었다.

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In, Bi를 함유한 Sn-Ag계 무연솔더의 솔더링성 연구 (A Study on the Solderability of In and Bi Contained Sn-Ag Alloy)

  • 김문일;문준권;정재필
    • 마이크로전자및패키징학회지
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    • 제8권3호
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    • pp.43-47
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    • 2001
  • Sn-3Ag-8Bi-5In 솔더는 중온계 무연솔더의 하나로서 개발되었다. In함유 솔더는 고가이지만, 솔더의 융점은 Sn-Ag-Cu 합금계보다 낮다. 본 연구에서 사용된 Sn-3Ag-8Bi-5In 솔더의 용융범위는 188~$204^{\circ}C$ 사이이다. 본 연구에서는 Sn-3Ag-8Bi-5In 솔더의 무연솔더로서의 적용가능성을 조사하기 위하여 솔더의 젖음특성을 평가하였다. Sn-3Ag-8Bi-5In 솔더의 젖음성을 기존 솔더 및 다른 무연솔더와 비교하기 위하여 Sn-37Pb, Sn-3.5Ag 공정솔더의 젖음특성도 조사하였다. 실험결과 영점시간과 젖음시간은 Sn-3Ag-8Bi-5In솔더의 경우 $240^{\circ}C$에서 각각 1.1, 2.2 초로서 Sn-37Pb 및 Sn-3.5Ag 무연솔더에 비하여 비슷하거나 다소 우수하였다. 또한, Sn-3Ag-8Bi-5In의 평형젖음력은 $240^{\circ}C$에서 5.8 mN으로 Sn-37Pb 솔더보다 낮고 Sn-3.5Ag 솔더보다 높았다.

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강우침투에 의한 산사태 발생 및 모관흡수력과 체적함수비의 변화 특성에 관한 연구 (Characteristics of Landslide Occurrence and Change in the Matric Suction and Volumetric Water Content due to Rainfall Infiltration)

  • 서원교;최정해;채병곤;송영석
    • 지질공학
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    • 제27권4호
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    • pp.475-487
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    • 2017
  • 본 연구에서는 산사태 모형토조 실험을 통해 강우침투에 의해 나타나는 산사태의 발생특성 및 지반재료의 변화특성에 관하여 분석하였다. 실험장치는 모형토조, 강우재현장치, 계측장치로 구성되어 있으며, 인공사면 상부에서 200 mm/hr의 극한강우를 살수함으로써 산사태를 유발하였다. 모관흡수력과 체적함수비 계측장치는 인공사면의 천부(GL-0.2 m), 중부(GL-0.4 m), 심부(GL-0.6 m)의 각 심도별로 3세트씩 설치하였으며, 실험은 화강암 풍화토, 편마암 풍화토, 이암 풍화토 각각에 대한 현장조건과 상대적으로 느슨한 조건 및 조밀한 조건으로 나누어 실험을 진행하였다. 분석결과, 극한강우에 의하여 실험 초반에는 사면 표층에서 세굴현상이 우세하게 나타나다가 이후 국지적으로 발생한 횡적인 인장균열면을 따라서 산사태가 발생했다. 산사태는 강우침투에 따른 습윤전선(wetting front)의 전이로 인해 천부에서부터 심부로 점차 확장되는 천층파괴(shallow failure)의 형태를 띰과 동시에 사면의 선단부(toe part)에서부터 정상부(crest part)로 점차 전이되는 후퇴성붕괴(retrogressive failure)의 양상을 보였다. 강우침투에 따른 포화영역에서 모관흡수력은 아무런 전조현상 없이 급격하게 감소하는 반면에, 체적함수비는 점진적으로 증가하다가 최대값에 도달하여 이 값을 일정시간 유지한 뒤 산사태 발생 시 급격히 감소하는 것으로 나타났다.

은계(BAg) 삽입금속으로 접합된 초경합금 입자와 탄소강 브레이징부의 특성 (Characteristics of the Brazed Joint between Superhard Alloy Particles and Carbon Steel Using BAg System Insert Metals.)

  • 김광수;김상덕
    • 한국산학기술학회논문지
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    • 제9권2호
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    • pp.298-302
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    • 2008
  • 초경합금입자와 탄소강사이의 브레이징 접합부 특성을 평가하였다 선택된 두 종류의 삽입금속은 기계적 합금 공정으로 만들어졌다. 한 가지는 Cu, Zn, Ag (MIM-1) 그리고 다른 한 가지는 Cu, Zn, Ag과 Cd(MIM-2)로 구성하였다. 삽입금속들의 화학조성은 AWS BAg-20계와 BAg-2a계의 성분과 유사하였다. 그리고 상용삽입금속들(CIM-1, CIM-2) 역시 비교 평가하였다. 삽입금속들의 특성은 젖음성 시험, 전단강도 시험, 그리고 미세조직 관찰로서 나타내었다. 젖음성 시험에서 MIM-1과 CIM-1 삽입금속의 젖음각이 MIM-2와 CIM-2보다 크게 나타났고, MIM-1의 젖음각이 CIM-1보다 더 큰 값을 나타났지만 모든 경우 젖음각이 $25^{\circ}$보다 작았다. 삽입금속, MIM-1이 가장 높은 전단강도를 나타냈고, 그 값은 $2.29{\times}10^2MPa$로 측정되었다. 이 값은 상용 삽입금속의 값과 같거나 높은 것으로 나타났다. 삽입금속의 미세조직은 Cu-rich 초정영역과 Ag-rich 공정영역으로 구성되었다. MIM-1계로 만들어진 초경합금과 탄소강의 접합부는 일부 접합부 계면에 기공을 포함하지만 초정을 기지로 하는 안정적인 미세조직을 나타냈다.

Development of a three dimensional circulation model based on fractional step method

  • Abualtayef, Mazen;Kuroiwa, Masamitsu;Sief, Ahmed Khaled;Matsubara, Yuhei;Aly, Ahmed M.;Sayed, Ahmed A.;Sambe, Alioune Nar
    • International Journal of Naval Architecture and Ocean Engineering
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    • 제2권1호
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    • pp.14-23
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    • 2010
  • A numerical model was developed for simulating a three-dimensional multilayer hydrodynamic and thermodynamic model in domains with irregular bottom topography. The model was designed for examining the interactions between flow and topography. The model was based on the three-dimensional Navier-Stokes equations and was solved using the fractional step method, which combines the finite difference method in the horizontal plane and the finite element method in the vertical plane. The numerical techniques were described and the model test and application were presented. For the model application to the northern part of Ariake Sea, the hydrodynamic and thermodynamic results were predicted. The numerically predicted amplitudes and phase angles were well consistent with the field observations.

POSSIBILITY OF PARTIAL MELTING SOLDERING PROCESS WITH OFF EUTECTIC LEAD FREE SOLDER ALLOYS

  • Kang, Choon-Sik;Ha, Jun-Seok;Park, Jae-Yong;Jung, Jae-Pil
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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    • pp.791-797
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    • 2002
  • This paper introduces the partial melting process for solder application and characterization of its feasibility using Sn-Ag, and Sn-Cu solder alloys. ill order to show that the liquid phase in the semi-liquid state maintains the similar wettability as single-phase liquid, the wetting balance tests are conducted with varying temperatures and compositions. Also, as a new soldering technology, the microstructural and mechanical test were investigated. The results from this research indicate that the partial melting can yield satisfactory sider joints as long as the liquid phase acquires sufficient chemical activity. At a condition where the partial melting is effective, a direct correlation between the wettability and the surface tension is found to exist.

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마이크로 솔더볼의 레이저 솔더링에 관한 연구 (Research on Laser Soldering of Micro Solder-balls)

  • 강희신;서정;이제훈;김정오;신희원;김도열
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2006년도 춘계학술대회 논문집
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    • pp.661-662
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    • 2006
  • This research is on a laser soldering using the micro solder-balls used in flip chip packaging process. A laser source used in laser soldering is Nd:YAG laser(250W and 60W). Solder-balls of 100, 300, $500{\mu}m$ size are used in experiments. The laser head to deliver a laser beam and the nozzle to transfer solder-balls are manufactured to bump solder-balls. After soldering solder-balls the shear test is carried out to determine the wetting at the interface between the surface and a solder-balls With the results of solder bumping tests a laminated molding is accomplished for manufacturing the three dimensional molding.

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Influence of flexural loading on chloride ingress in concrete subjected to cyclic drying-wetting condition

  • Ye, Hailong;Fu, Chuanqing;Jin, Nanguo;Jin, Xianyu
    • Computers and Concrete
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    • 제15권2호
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    • pp.183-198
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    • 2015
  • Chloride ingress implies a complex interaction between physical and chemical process, in which heat, moisture and chloride ions transport through concrete cover. Meanwhile, reinforced concrete structure itself undergoes evolution due to variation in temperature, relative humidity and creep effects, which can potentially change the deformation and trigger some micro-cracks in concrete. In addition, all of these process show time-dependent performance with complex interaction between structures and environments. In the present work, a time-dependent behavior of chloride transport in reinforced concrete beam subjected to flexural load is proposed based on the well-known section fiber model. The strain state varies because of stress redistribution caused by the interaction between environment and structure, mainly dominated by thermal stresses and shrinkage stress and creep. Finally, in order to clear the influence of strain state on the chloride diffusivity, experiment test were carried out and a power function used to describe this influence is proposed.

인공경량골재 사용 경량투수블록의 제조시간 변화에 따른 배합 및 압축강도 특성 (A Compressive Strength and Mixing Properties of Lightweight Porous Block Using Lightweight Aggregate by Variation of Manufacture Time)

  • 김영욱;이경수;오태규;정수빈;반준모;최세진
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2018년도 추계 학술논문 발표대회
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    • pp.118-119
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    • 2018
  • The purpose of this study is to investigate the compressive strength and mixing properties of the lightweight block, which has been manufactured without the pre-wetting process, in the lightweight block using domestic artificial lightweight aggregate. The test results of the specimens produced within 30 minutes after the preparation showed high compressive strength but poor permeability. Therefore, the elapsed time after the manufacture, which is expected to have required compressive strength and permeability, was about 60 minutes in this study.

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