• 제목/요약/키워드: vacuum vaporization

검색결과 25건 처리시간 0.031초

MOLTEN SALT VAPORIZATION DURING ELECTROLYTIC REDUCTION

  • Hur, Jin-Mok;Jeong, Sang-Moon;Lee, Han-Soo
    • Nuclear Engineering and Technology
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    • 제42권1호
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    • pp.73-78
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    • 2010
  • The suppression of molten salt vaporization is one of the key technical issues in the electrolytic reduction process developed for recycling spent nuclear fuel from light-water reactors Since the Hertz-Langmuir relation previously applied to molten salt vaporization is valid only for vaporization into a vacuum, a diffusion model was derived to quantitatively assess the vaporization of LiCl, $Li_2O$ and Li from an electrolytic reducer operating under atmospheric pressure. Vaporization rates as a function of operation variables were calculated and shown to be in reasonable agreement with the experimental data obtained from thermogravimetry.

Catalytic growth of single wall carbon nanotubes by laser vaporization and its purification and The carbon nanotube growth on the Si substrate by CVD method

  • Lee, Sung won;Jung in Sohn;Lee, Seonghoon
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2000년도 제18회 학술발표회 논문개요집
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    • pp.213-213
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    • 2000
  • Direct laser vaporization of transition-metal(Co, Ni)/graphite composite pellet produced single wall carbon naotubes(SWNT) in the condensing vapor in a heated flow cylinder-type tube furnace, Transition metal/graphite composite pellet target was made by mixing graphite, Co, and Ni in 98:1:1 atomic weight ratios, pressing the mixed powder, and curing it. The target was placed in a tube furnace maintained at 1200$^{\circ}C$ and Ar inert collision gas continuously flowed into the tube. The 2nd harmonic, 532nm wavelength light from Nd-YAG laser was used to vaporize the tube. The carbon nanotubes produced by the laser vaporization were accumulated on quartz tube wall. The raw carbon nanotube materials were purified with surfactants(Triton X-100) in a ultrasonicator. These carbon nanotubes were analyzed using SEM, XRD, and Raman spectroscopic method. The carbon nanotube growth on the Ni-patterned Si substrate was investigated by the CVD process. Transition-metal, Ni and CH4 gas were used as a catalyst and a reactant gas, respectively. The structure and the phonon frequencies of the carbon nanotubes formed on the patterned Si substrate were measured by SEM and Raman spectrometer.

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폐용제에 함유된 입자의 건조 및 분리용 연속식 순간 진공건조시스템 해석 (Analysis of a Continuous and Instantaneous Vacuum Drying System for Drying and Separation of Suspended Paricles in Waste Solvent)

  • 구재현;이재근
    • 자원리싸이클링
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    • 제9권4호
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    • pp.28-36
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    • 2000
  • 본 연구는 입자가 혼합된 용제를 이중판형 열교환기 내에서 가열 및 증발과정을 통해 건조이자와 용제로 분리하여 회수하기 위한 연속식 순간 진공건조 시스템 해석에관한 것이다. 진공건조시스템은 용제 공급펌프, 이중관형 열교환기, 진공 스프레이 챔버 및 응축기로 구성된다. 연속적으로 공급되는 용제는 이중관형 열교환기 내에서 가열, 팽창 및 증발되며 관 출구부에서 팽창된 증기가 진공 스프레이 챔버 내로 분사되고 증기는 응축기로 수송되어 용제로 회수되고 입자는 관성력에 의해 증기로부터 분리되어 건조된다ㅣ. 안료입자가 함유된 벤젠 및 알킬벤젠의 분리 및 회수성능 실험을 수행한 결과, 습분양 1.1%로 건조된 안료입자를 94% 회수하였고, 99.9 wt%의 고순도 벤젠을 88% 회수하였다. 평균직경이 $6.5\mu\textrm{m}$인 안료입자를 진공건조시스템의 이중관형 열교환기에서 관출구부의 고속 분사에 의한 폭발적 분산력에 의해 입경이 14%감소된 $5.6\mu\textrm{m}$ 크기의 건조 안료입자를 회수하였다. 따라서 진공건조시스템은 용제에 함유된 입자를 건조 및 분리하여 미분제 제품으로 히수하는데 효율적이며 폐용제 정제용으로 적용이 가능하다.

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폐용제 회수용 이중관형 열교환기 특성 해석 (Analysis of a Double Pipe Heat Exchanger for Waste Solvent Recovery)

  • 구재현;이재근
    • 자원리싸이클링
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    • 제9권3호
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    • pp.13-21
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    • 2000
  • 본 연구는 폐용제를 가열, 증발 및 음축과정을 거쳐 용제를 회수하는 시스템의 열교환기 해석에 관한 것으로, 고온 열매체유로 가열되는 이중관형 열교환기를 사용하여 용제 증발과정의 열전달 특성을 분석하고 용제유량과 가열온도에 따라 물, 벤젠 및 알칼벤젠의 증발을 위해 요구되는 전열면적을 분석하였다. 폐용제 회수장치는 용제 공급펌프 이중관형 열교환기, 진공 스프레이 챕버 및 응축기동으로 구성되며, 이중관형 열교환기는 용제액을 열적 포화온도를 가열시키는 구간과 포화된 용제액을 증발시키는 구간으로 구성된다. 관 내 용제의 증발을 위한 전열면적을 열평형 모델링에 의해 예측하였고, 이중관형 열교화기의 관 내 온도분포 측정을 통해 이론값과 비교 분석하였다. 용제유량 0.1~0.51l/mm 및 가열온도 130~$260^{\circ}C$의 범위에서 용제유향 증가 및 가열온도 감속에 따라 단위전열면적당 열전달양이 감소하기 때문에 용제 증발을 위한 전열면적은 증가하였다. 관 내 용제 증발을 위한 전열면적의 이론적 분석결과는 측정값과 일치하였으며, 이중관형 열교환기를 사용한 폐용제의 증발과정을 통해 용제를 회수하는 기술에 적용이 가능하다.

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루츠형 중진공펌프 국산화 개발 (Development of Localized Roots Type Medium-Vacuum Pump)

  • 탁봉열;김병덕;양해경;한기영;이소아
    • 한국유체기계학회 논문집
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    • 제14권3호
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    • pp.23-27
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    • 2011
  • Due to a roots type medium vacuum pump is operated in condition of $1{\sim}10^{-3}$ torr vacuum, it could be applied for production and process of industrial parts, such as precise processing, vaporization, enrichment, separation, casting, metaling, welding, transportation. Therefore, the demand of this pump is increasing nowadays in our industrial markets of semiconductor, electric, electronic, automobile, material, environmental and transporting industries. However, the pumps are almost imported, because the domestic pumps are inferior in fields of vacuum range as under $10^{-1}$torr, relevant techniques(design, fabrication, casting, test, etc.) to the imported ones. In this study, essential parts of the development pump are designed with using of CFD and 3D decodes, FEM for analysing strength and deformation, generated heat, vibration and noise control, and are casted with using of mechanochemistry techniques for decreasing of weights, increasing of heat resistances and abrasion durability of materials for pump caing and impellers especially. Besides, in order to achieve ultimate vacuum around $10^{-3}$torr, this pump is composed of 6 stages, among which 1st stage is operated separately from remained stages. Additionally, a test rig for prototype pumps(300$m^3/h$ and 2,500$m^3/h$) is designed and procured as to apply for multi-staged rootz type vacuum pump, with modification of the test method recommended by KS B 6314 "Positive-displacement oil-sealed rotary vacuum pumps".

Measurement of characteristics of plasma discharge in liquid

  • Kim, Ju-Sung;Min, Boo-Ki;Kang, Seong-Oun;Choi, Eun-Ha
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
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    • pp.153-153
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    • 2015
  • Application of the plasma is already highlighted as a new technology in the last few years. In these days, there are lots of attempt in various application with plasma in that it is known as an effective treatment to animal, plants, material and so on. Plasma in liquid, one of new plasma applications, has advantages in ability to treat bio-cell or solutions. For example, electro-surgery, water purification, radical generation and so on. Especially, plasma discharge in solutions is very useful technique and difficult to generate due to electrolysis, vaporization and something else. In this study, we have performed plasma discharge and checked sustainability of plasma in solution(saline 0.9%). And we have measured basic characteristics of plasma in liquid. Such as electrical energy and plasma density are calculated from discharging current and voltage. Also, its thermal energy is measured with IR camera.

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Characterization and process of Parylene polymer film for high transparent film, water barrier property

  • 이두원;국윤봉;홍태권
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제40회 동계학술대회 초록집
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    • pp.357-358
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    • 2011
  • Dichloro-(2,2)-paracyclophane을 출발 물질로 하여 화학기상증착법(CVD)을 이용해 우수한 투명성과 수분 투과성을 갖는 poly(p-xylylene) 코팅 막을 얻었다. 상기 코팅 막을 얻기 위한 최적의 공정 조건은 Deposition Pressure 0.02~0.04Torr, Vaporization temperature $110{\sim}150^{\circ}C$으로 확인 되었다. 이러한 공정 조건으로 500 mm*500 mm size의 PET bare film을 코팅 기재로 사용하여 $10{\mu}m$, $20{\mu}m$의 parylene 코팅 막을 얻었고 이를 특성 분석해 보았다. 상기 코팅 막은 전체적으로 ${\pm}1{\mu}m$의 thickness uniformity가 관찰 되었고 투과율은 90% 이상을 보였으며 수분 투과율은 기재 대비 상대적으로 40%의 향상이 기대 되었다. 또한 우수한 내식성, 내염기성, 내용제성을 갖고 있었으며 PET 기재에 대해 우수한 부착력을 가지고 있었다. surface morphology는 AFM을 통해 분석하였으며 Ra가 15.123, Rq가 22.859로 측정 되었다.

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Analysis of characteristics of discharge in liquid

  • Kim, Ju-Sung;Min, Boo-Ki;Hong, Young-June;Kang, Seong-Oun;Choi, Eun-Ha
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.209.2-209.2
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    • 2016
  • Up to now, Plasma applications are thought as a leading technology in industrial, chemical and even medical and biological field. Especially, Due to direct discharge in liquid with reaction in ambient solution, plasma in liquid is useful plasma technology. Such as electro-surgery, water purification, radical generation for synthesis. For using those plasma applications efficiently, plasma characteristics should be understood in advance. But discharge in liquid is not much well-known about its characteristics. And plasma discharge in solution is difficult to generate and analysis due to electrolysis, vaporization and radical generation. So, We make stable plasma discharge in solution(saline 0.9%) without input gas. We also analyze new type of plasma source in thermal and electrochemical view. And we check characteristics of plasma in liquid. For example, plasma density and radical density(OH) with optical emission, thermal energy with thermometer, electrical energy with oscilloscope and so on. And we try to explain the bubble and plasma formation with circuit analysis.

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