• 제목/요약/키워드: vacuum treatment

검색결과 1,080건 처리시간 0.025초

주조용 TiAl 합금의 조직 미세화를 위한 반복열처리 공정 조건에 관한 연구 (The Effects of Cyclic Heat Treatment Process for Fine Microstructure of TiAl Cast Alloy)

  • 공만식;양현석
    • 열처리공학회지
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    • 제32권5호
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    • pp.195-200
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    • 2019
  • For expanding the applications and workability of TiAl alloy, elongation is very important property. Fine microstructure is needed for elongation and physical properties of TiAl alloys. In this study, The effects of cyclic heat treatment process for fine microstructure of Ti-46Al-Nb-W-Cr-Si-C alloy, which was made by VAR (vacuum arc remelting) and VIM(vacuum induction melting) centrifugal casting process, was investigated. Cycle heat treatment process was very effective for recrystallization of this TiAl system, which has microstructure size of $50{\sim}100{\mu}m$ through pre-heat treatment, cyclic heat treatment in ${\alpha}+{\gamma}$ phase region and solution heat treatment respectively. Refined grain size was finally confirmed by photos of optical microscope and scanning electron microscope.

스퍼터링 타겟용 저온 분사 Cu-15 at.%Ga 코팅 소재의 특성에 미치는 열처리 분위기의 영향 (Effect of Heat Treatment Environment on the Properties of Cold Sprayed Cu-15 at.%Ga Coating Material for Sputtering Target)

  • 최병철;박동용;김형준;오익현;이기안
    • 한국분말재료학회지
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    • 제18권6호
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    • pp.552-561
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    • 2011
  • This study attempted to manufacture a Cu-15 at.%Ga coating layer via the cold spray process and investigated the effect of heat treatment environment on the properties of cold sprayed coating material. Three kinds of heat treatment environments, $5%H_2$+argon, pure argon, and vacuum were used in this study. Annealing treatments were conducted at $200{\sim}800^{\circ}C$/1 hr. With the cold sprayed coating layer, pure ${\alpha}$-Cu and small amounts of $Ga_2O_3$ were detected in the XRD, EDS, EPMA analyses. Porosity significantly decreased and hardness also decreased with increasing annealing temperature. The inhomogeneous dendritic microstructure of cold sprayed coating material changed to the homogeneous and dense one (microstructural evolution) with annealing heat treatment. Oxides near the interface of particles could be reduced by heat treatment especially in vacuum and argon environments. Vacuum environment during heat treatment was suggested to be most effective one to improve the densification and purification properties of cold sprayed Cu-15 at.%Ga coating material.

냉수침지 숙성법이 진공포장 한우육의 연도 및 미생물 증식에 미치는 효과 (Effects of Submersion Aging in Chilled Water on Tenderness and Microbial Growth of Vacuum-Packed Hanwoo Meat)

  • 주선태;이한기;강근호;신철우;양한술;문성실;이정일;김영환;박구부
    • 한국축산식품학회지
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    • 제22권3호
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    • pp.228-233
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    • 2002
  • 본 연구는 진공포장 한우육의 냉수침지 숙성방법이 한우육의 연도 및 미생물증식에 미치는 영향을 구명하고자 수행하였다. 저장기간이 경과함에 따라 근절길이는 냉수침지 처리구가 저장 3일째 유의적(p<0.05)으로 긴 것으로 나타났으며, 저 장 3일째를 제외 한 저 장기간 동안 유의적 인 차이는 없었으나 대조구에 비해 긴 경향을 보였다. 또한 유리칼슘 농도에 있어서도 저장 7일 째 냉수침지 처리구가 유의적(p<0.05)으로 높게 나타났으며, 역시 저장 7일째를 제외한 저장기간 동안 유의적인 차이는 없었으나 대조구에 비해 높은 경향을 보였다. 한편 전단가와 근원섬유 소편화 지수에 있어서는 저장기간이 경과함에 따라 두 처리구간에 있어서 유의적인 차이는 나타나지 않았지만, 냉수침지 처리구가 상대적으로 낮은 전단가와 높은 소편화지수의 경향을 보였다. 이 같은 결과는 냉수침지 숙성이 일반공기순환냉장고의 숙성보다 근절의 길이를 길게 하고, 근형질내 칼슘의 농도를 높이며, 소편화 지수를 높게 한 결과 연도를 향상시킬 수 있다는 가능성을 제시한 것으로 사료된다. 덧붙여, 총세균수는 일반공 기순환냉장실에 저장한 것에 비해 냉수침지 처리구가 유의적(p<0.05)으로 낮은 것으로 나타나, 온도의 변이를 줄이는 것에 기인하여 미생물의 성장억제에도 효과적일 것으로 사료된다.

Experimental study on treatment of waste slurry by vacuum preloading with different conditioning agents

  • Wu, Yajun;Jiang, Haibo;Lu, Yitian;Sun, Dean
    • Geomechanics and Engineering
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    • 제17권6호
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    • pp.543-551
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    • 2019
  • In China, serious environmental problems are induced by the extremely soft construction waste slurries in many urban areas, and there is no appropriate method to treat it presently. In this paper, four model tests were conducted to investigate the efficiency of waste slurry treatment by combining three conditioning agents which can change characteristics of the slurries with a traditional vacuum preloading method. The tests of size analysis of particle aggregate were conducted to investigate the influence of different conditioning agents on the size distributions of particle aggregate. During the model test, the discharged water volumes were monitored. The pore-size distribution and void ratio of the waste slurries after the vacuum preloading were measured by mercury intrusion porosimetry (MIP). It is found that 1) During the natural precipitation, volume of water out of the organic agent is higher than that of the mixed agent, but it is smaller than that of the mixed agent in the vacuum preloading stage; 2) the mixed agent has a higher total volume of water out than the organic agent and the inorganic agent after test, while the organic agent and the inorganic agent have little difference with respect to the drainage effect. The results demonstrate that the combination of mixed conditioning agent and vacuum preloading for the solid-liquid separation in waste slurry has a satisfactory effect and can be applied in engineering practice.