• Journal of the Korean Ceramic Society
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• v.27 no.6
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• pp.735-740
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• 1990

The phase transformation of Y-TZP by low temperature aging treatments and its related behaviors of crack formation were investigated. The kinetics of phase transformation was greatly dependent on the amounts of Y2O3, grian size and microstructures of sintered body. The phase transformation happened to start at specimen surface and near the pore in the first place, where the change of strain energy during the phase transformation was small and the water vapor that accelerated phase transformation easily diffused.

• Transactions of Materials Processing
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• v.19 no.1
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• pp.25-31
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• 2010

To achieve desired microstructure and mechanical property of a manufacturing product, heat treatment process is applied as a secondary process after forging. Especially, quenching process is used for improving strength, hardness, and wear resistance since phase transformation occurs owing to rapid heat transfer from the surface of the specimen. In the present paper, a study on surface temperature measurement for water quenching of eutectoid steel was investigated. In order to determine the temperature history in experiments, three different measuring schemes were used by varying installation techniques of K-type thermocouples. Depending on the measured temperature distribution at the surface of the specimen, convective heat transfer coefficients were numerically determined as a function of temperature by the inverse finite element analysis considering the latent heat generation due to phase transformation. Based on the inversely determined convective heat transfer coefficient, temperature, phase, and hardness distributions in the specimen after water quenching were numerically predicted. By comparing the experimental and computational hardness distribution at three different locations in the specimen, the best temperature measuring scheme was determined. This work clearly demonstrates the effect of temperature measurement on the final mechanical property in terms of hardness distribution.

• Journal of Advanced Marine Engineering and Technology
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• v.21 no.5
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• pp.482-490
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• 1997

The effects of strain amplitude. test temperature and stress on the fatigue properties for Ti-Ni wires were investigated using a rotary bending fatigue tester specially designed for wires. The fatigue test results were discussed in connection with the static tensile properties. The DSC measurement was conducted after fatigue test in order to clarify the change of transformation behavior due to the progress of fatigue. Under the temperature below or near the Af, the strain amplitude($\varepsilon_a$)-failure life (Nf) curve showed to be composed of three straight lines with two turning points. Of the 2 turning points, the upper one was coincident with the elastic limit strain and the lower one with the proportional limit strain. With rising of the test temperature above Af, the pattern of $\varepsilon_a$-Nf curve changed gradually to composition of 2 straight lines. The $\varepsilon_a$-Nf curve shifted depending on test temperature. In the short and medium life zones, the higher the temperature was, the shorter the fatigue life. However, in the long life zone, above the Af temperature, the fatigue life was not affected by the temperature. The transformation enthalpy measured after fatigue test was dependent on Nf, $\varepsilon_a$, and test temperature.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.11a
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• pp.421-424
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• 2006

This study, in order for perceiving the mechanical attribute followed by the explosive spalling of high strength concrete material under high temperature and evaluating capacity of endurance of material, targets understanding capacity of endurance of material such as explosive spalling in high temperature, temperature by thickness of clothing, transformation extent, transformation speed and displacement, stocking the maximum load based on the Allowable Stress Design Method. As a result of experimenting the explosive spalling attribute of high strength concrete material, the one possibly causing serious damage is the 50 MPa concrete. In all aspects of 60 MPa concrete, explosive spalling happens. Especially, it is hazardous enough to reveal all the iron bar. All explosive spalling is intensively concentrated on the surface of concrete for the first $5{\sim}25$ minutes, which urges for the explosive spalling protection action. As a result of evaluating the structural safety by the transformation of high strength concrete, while beam assures the fire safety meeting regulation, 60 MPa shows the dramatic increase of transformation, which only counts 84% of safety. In a column, both the concrete exclusion and excessive explosive spalling are concentrated upper part of column, which brings about the dramatic transformation, so it only meets the 50% of safety regulation. Likewise, in 80, 100 MPa concrete which was never experimented considering the condition of domestic structural endurance stocking devices, the faster collapse is expected.

• Korean Journal of Materials Research
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• v.17 no.1
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• pp.37-42
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• 2007

The effects of immersion time in the liquid nitrogen and deformation-induced martensitic transformation on the behavior of austenite stainless steels used for the hydrogen storage tank of auto-mobile at cryogenic temperature were investigated. With increasing of immersion time in the liquid nitrogen, the tensile strength of all austenite stainless steels at cryogenic temperature was increased because the martensite transformation of unstable austenite. The restraint of crack generation ana transmission also increased the tensile strength by the active ${\alpha}'$ transformation. The elongation decreasing of 321 steel is not the mechanical deformation of austenite phase but the stress induced martensite phase during the tensile test.

• Journal of the Korean Society for Heat Treatment
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• v.17 no.2
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• pp.78-86
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• 2004

Effects of the annealing parameters on the formation of ferrites transformed at low temperatures were studied in cold-rolled ultra low carbon steels with niobium and/or chromium. Niobium and chromium were found to be effective in the formation of the low temperature transformation ferrites. The low temperature transformation ferrites more easily formed when both higher annealing temperature and longer annealing time, allowing substitutional alloying elements to distribute between phases, are in combination with faster cooling rate. It was found from EBSD study that the additions of niobium or chromium resulted in the increase in the numbers of high angle grain boundaries and the decrease in those of the low angle grain boundaries in the microstructures. Both granular bainitic ferrite and bainitic ferrite were characterized by the not clearly etched grain boundaries in light microscopy because of the low angle grain boundaries.

• Journal of the Korean Society of Safety
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• v.19 no.4 s.68
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• pp.1-7
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• 2004

This study investigated the effects of aging on the transformation behavior of $Ti-50.1at\%$ Ni alloy by means of differential scanning calorimetry. It was found that aging in the temperature range of $350^{\circ}C\~550^{\circ}C$ induced complex transformation behavior, involving the R-phase and multiple-stage martensitic transformation. Usually aged Ni-rich NiTi alloys undergo martensitic transformation on cooling from high temperatures in two step : B2 to R and then R to Bl9'(normal behavior). But under certain ageing conditions, the transformation can also occur in three or more step(unusual multiple step behavior). In the present study we use differential seaming calorimetry(DSC) for a systematic investigation of the evolution of transformation behavior with ageing temperature and time.

• Journal of the Korean Society for Heat Treatment
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• v.13 no.5
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• pp.346-354
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• 2000

Effect of Nb addition on the phase transformation behavior was studied through continuous cooling transformation tests after reheating(reheating CCT) and deforming(deforming CCT) the 0.07%C-1.3%Mn-0.015%Ti-(0~0.08)% Nb steels. Transformation temperatures for deforming CCT were lower than those for reheating CCT, and the critical cooling rate for bainite transformation during deforming CCT was lower than that during reheating CCT. These enhanced hardenability for deforming CCT was considered to come from the sufficient solid solution of Nb in austenite during high temperature reheating before deformation. With Nb addition, the phase transformation temperature decreased, the bainite formation was enhanced, and the hardness of steel increased. Furthermore, these phenomena were more remarkable for deforming CCT than for reheating CCT. From the results, Nb-Ti bearing low carbon steel was considered to be a very favorable alloy system with good strength/toughness balance by recrystallization control rolling process.

• Journal of Power System Engineering
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• v.16 no.4
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• pp.60-65
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• 2012

This study was carried out to investigate the effect of reverse transformation on the damping capacity in high manganese austenitic stainless steel. ${\alpha}^{\prime}$-martensite was formed with the specific direction and surface relief by deformation. Over 95% of the austenite phase was transformed to deformation-induced ${\alpha}^{\prime}$-martensite by 70% cold rolling. Reverse transformation became rapid above an annealing temperature of $550^{\circ}C$, but there was no significant transformation above $700^{\circ}C$. In addition, with increasing annealing time at $700^{\circ}C$, reverse transformation was induced rapidly, but the transformation was almost completed at 10 min. Damping capacity was increased up to $700^{\circ}C$, and than unchanged with the increasing annealing temperature. Damping capacity increased steeply with an increasing reverse treatment time up to 10min, whereas there were no significant change with a treatment time of more than 10 min. Damping capacity increased with an increasing the reversed austenite and was strongly affected by reversed austenite.

• Korean Journal of Metals and Materials
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• v.50 no.6
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• pp.413-418
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• 2012

This study was carried out to investigate the effect of reverse transformation on the mechanical properties in high manganese austenitic stainless steel. Over 95% of the austenite was transformed to deformation-induced martensite by 70% cold rolling. Reverse transformation became rapid above an annealing temperature of $550^{\circ}C$, but there was no significant transformation above $700^{\circ}C$. In addition, with an increasing annealing time at $700^{\circ}C$, reverse transformation was induced rapidly, but the transformation was almost completed at 10 min. There was a rapid decrese in strength and hardness with annealing at temperature above $550^{\circ}C$, while elongation increased rapidly above $600^{\circ}C$. At $700^{\circ}C$, hardness and strength decreased rapidly, and elongation increased steeply with an increasing reverse treatment time up to 10 min, whereas there were no significant change with a treatment time after 10 min. The reverse-transformed austenite showed an ultra-fine grain size less than $0.2{\mu}m$, which made it possible to strengthen the high manganese austenitic stainless steel.