• Title/Summary/Keyword: time of concentration ratio

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젤라틴 전처리 면직물의 에탄올-물 혼합용매에 의한 코치닐 염색성 향상 (Improving the Dyeability of Gelatin Pretreated Cotton Fabrics Dyeing with Cochineal in Ethanol-Water Mixture)

  • 하수영;장정대
    • 한국염색가공학회지
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    • 제31권3호
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    • pp.127-134
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    • 2019
  • Cotton fabrics were treated with gelatin to improved their dyeability, color strength toward cochineal dye. Gelatin were used as the protein. Gelatin is containing a large number of hydrophilic groups. Pad-dry-cure method was used for the treatment process(10g/L concentration). The scanning electron micrograph showed the gelatin was deposited on the surface of cotton. Pretreated fabrics were mordanted with 10%(owf) alum. Then the fabrics were dyed with cochineal. Compared with original cotton fabric the K/S value with cochineal dyes was significantly improved on gelatin modified cotton. Treating cotton with 10g/L concentration gelatin offered higher cochineal adsorption. The dyeability of pH 4 yielded the highest color strength. In dyebaths of a ratio of ethanol and water such as; 10:0, 9:1, 8:2, 7:3, 6:4, 5:5, 4:6, 3:7, 2:8, 1:9, 0:10, fabrics were dyed. The ratio of ethanol and water had powerful effects on solution polarity. Cochineal dye uptake showed maximum value, when the proportion of ethanol and water was 9:1. Dyeing at increased temperatures and with increased time resulted in higher dye uptake and reddish-purple color(5RP). The washing fastness was 1-2grade, and the fastness to light was 2-3grade.

Empirical modelling of chemically enhanced backwash during ultrafiltration process

  • Daramola, M.O.;Adeogun, A.G.
    • Membrane and Water Treatment
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    • 제2권4호
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    • pp.225-237
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    • 2011
  • In this study, response of reversibility of membrane flux during chemically enhanced backwash (CEB) to changes in filtration time, filtration flux and coagulant concentration dosing during ultrafiltration (UF) process was investigated using a regression model. The model was developed via empirical modelling approach using response surface methodology. In developing the model, statistically designed UF experiments were conducted and the results compared with the model output. The results showed that the performance of CEB, evaluated in terms of the reversibility of the membrane flux, depends strongly on the changes in coagulant concentration dosage and the filtration flux. Also the response of the reversibility of membrane flux during CEB is independent of the filtration time. The variance ratio, VR << $F_{value}$ and $R^2$ = 0.98 obtained from the cross-validation experiments indicate perfect agreement of the model output with experimental results and also testify to the validity and suitability of the model to predict reversibility of the membrane flux during CEB in UF operation.

고체상미량분석법(SPME)을 이용한 GC/FID에서 PCE 및 TCE 최적 분석법 (The Optimal Analytical Method for the Determination of PCE and TCE by GC/FID with SPME technieque)

  • 안상우;이시진;장순웅
    • 한국환경과학회지
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    • 제13권10호
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    • pp.903-909
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    • 2004
  • A new method based on solid phase microextraction(SPME), coupled with GC/FID, has been developed for the determination of PCE and TCE in water samples. The experimental parameters affecting the SPME process (i.e, kinds of fibers, extraction time, desorption time, extraction temperature, volume ratio of sample to headspace, salt addition, and magnetic stirring) were optimized. The coefficients of determination ($R^2$) for PCE and TCE were 0.9951 and 0.9831, respectively when analytes concentration ranges from 10 to 300$\mu$g/L. The relative standard deviations were 3.4 and $2.1\%$ for concentration of 10$\mu$g/L(n=5), respectively. The detection limits of PCE and TCE were 0.5 and l.3$\mu$g/L, respectively.

합성수용액의 Preheating 시간을 변화시켜 수열합성법으로 성장시킨 산화아연 나노선 (ZnO Nanowires Grown by Hydrothermal Synthesis Using Synthesis Solution Prepared with Various Preheating Time)

  • 노임준;신백균
    • 한국전기전자재료학회논문지
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    • 제25권6호
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    • pp.481-485
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    • 2012
  • ZnO nanowires were synthesized by hydrothermal technique. Prepared synthesis aqueous solutions were preserved by preheating in autoclave type synthesis equipment with various preheating time of 1 h difference. ITO-coated corning glass substrates deposited with AZO seed layers were then inserted in the preheated synthesis aqueous solutions and ZnO nanowires were grown for 180 min at $90^{\circ}C$. Density, length and aspect ratio of the grown ZnO nanowires were investigated. Composition, structural and optical properties of the grown ZnO nanowires were analyzed. Characteristics of the ZnO nanowires were comparatively studied in relation with $Zn^{2+}$ ion concentration measured directly after the preheating of synthesis aqueous solution.

저온연소조건에서 급속압축기를 이용한 n-heptane/n-butanol 혼합연료의 착화지연에 관한 연구 (The investigation on the Ignition Delay of n-heptane/n-butanol Blend Fuel using a Rapid Compression Machine at Low Temperature Combustion Regime)

  • 송재혁;강기중;;;최경민;김덕줄
    • 한국연소학회:학술대회논문집
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    • 한국연소학회 2013년도 제46회 KOSCO SYMPOSIUM 초록집
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    • pp.25-28
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    • 2013
  • This study presents both experimental and numerical investigation of ignition characteristics of n-heptane and n-butanol mixture. The $O_2$ concentration was fixed to 9-10% to make high exhaust gas recirculation(EGR) rate condition. Experiments were performed using a rapid compression machine. In addition, a numerical study of the ignition delay time was performed using CHEMKIN codes to validate experimental results and predict chemical species after combustion process. The results showed that the ignition delay time increased with increasing n-butanol ratio and the reactivity decreased by low $O_2$ concentration.

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가공 인자에 다른 미세 전해 가공 속도 변화 연구 (Study on Machining Speed according to Parameters in Micro ECM)

  • 권민호;박민수;신홍식;주종남
    • 한국정밀공학회지
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    • 제28권3호
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    • pp.308-314
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    • 2011
  • In micro electrochemical machining (micro ECM), machining conditions have been determined to maintain a small side gap and to machine a workpiece stably However, machining speed is slow. To improve machining speed while maintaining the form accuracy, the paper investigates machining parameters such as pulse amplitude, duty ratio, pulse on-time, and the electrolyte's temperature and concentration. The experiment in this study shows that the electrolyte's concentration is the key factor that can reduce machining time while maintaining the form accuracy Micro square columns were fabricated to confirm the machining parameters' effects.

ADEPT공정을 거친 돈사폐수의 아질산화-아탈질 공정을 이용한 질소제거 (Nitrogen Removal from ADEPT Effluent of Piggery Wastewater using Nitritation/Denitiritation System)

  • 이화선;민경석
    • 한국물환경학회지
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    • 제22권1호
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    • pp.134-139
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    • 2006
  • Partial nitirification and denitrification process has been reported to be technically feasible and economically favorable, especially for wastewater treatment with high ammonium concentration or low Carbon/Nitrogen ratio. This research was performed to survey nitrite accumulation by nitritation in treating ADEPT effluent of piggery wastewater, which contains highly concentrated ammonia. To estimate the possibility of nitrite accumulation, DO concentration and SRT were investigated as key operational parameters. This result proved that nitritation to nitrite was steadily obtained under short sludge retention time. Oxygen limitation was proved to be just a subsidiary parameter. Energy efficiency of nitritation-denitritation process was higher than complete nitrification-denitrification because external carbon requirement for denitritation could be saved. Though the influent contained significant nonbiodegradable organic substrate, total nitrogen removal efficiency was more than 51% in nitritation-denitritation system.

복합토양층의 불포화대와 포화대에서 연속주입 추적자시험을 이용한 수리분산특성 연구 (A Study of Hydrodynamic Dispersions in the Unsaturated and the Saturated Zone of a Multi-soil Layer Deposit Using a Continuous Injection Tracer Test)

  • 정상용;강동환;이민희;손주형
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제11권4호
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    • pp.48-56
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    • 2006
  • 여러 개의 층으로 구성된 토양층에서 연속주입 추적자시험을 수행하여, 불포화대와 포화대 구간에서의 수리분산특성 차이를 추적자의 농도이력곡선, 시간에 따른 농도변화 및 농도변화율, 그리고 거리에 따른 농도비 분석을 통해 비교 연구하였다. 연속주입 추적자시험에 의하면, 약 160시간이 경과된 후에 불포화대와 포화대에서 Rhodamine WT 최대농도의 차이는 약 $13{\sim}15$배 정도에 달하였고, 시험시간 대 추적자 농도증가율의 차이는 약 10배 정도로 나타났다. 또한 시간에 따른 추적자 농도이력곡선의 변화와 농도변화율이 불포화대에 비하여 포화대에서 크게 나타났다. 주입공에서의 이격거리에 따른 추적자의 농도비는 포화대 구간에서 더 빠르게 선형적으로 감소하였으며, 그 이후에 농도비가 2배 이하로 완만해 지는데 걸린 시간은 포화대 구간이 더 길었다. 이러한 차이들은 여러 개의 층서로 구성된 토양층의 포화대에서는 지하수가 존재하며, 또한 매질의 불균질성이 크고 투수성이 다양하기 때문에, 비교적 균질한 층서를 이루는 불포화대에 비하여 추적자 용액의 농도는 낮고, 추적자의 확산이 느리게 진행되어진데서 기인하였다. 그리고 포화대 구간에서의 유효공극율은 $10.19{\sim}10.50%$, 종분산지수는 $0.80{\sim}l.98m$, 횡분산지수는 $0.02{\sim}0.04m$의 범위로 산정되었으며, 실내주상시험의 종분산지수와 비교할 때 12배 이상의 규모종속효과가 나타났다.

Bioequivalence of Cholicerin Soft Capsule to Gliatilin Soft Capsule (Choline Alphoscerate 400 mg)

  • Kang, Hyun-Ah;Kim, Se-Mi;Kang, Seung-Rae;Kang, Min-Sun;Lee, Sang-No;Kwon, In-Ho;Yoo, Hee-Doo;Kim, Yoon-Gyoon;Lee, Yong-Bok
    • Journal of Pharmaceutical Investigation
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    • 제40권2호
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    • pp.109-115
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    • 2010
  • The purpose of the present study was to evaluate the bioequivalence of two choline alphoscerate soft capsules, Gliatilin soft capsule (Daewoong Pharmaceuticals Co., Ltd.) and Cholicerin soft capsule (Sam Chun Dang Pharm. Co., Ltd.), according to the guidelines of Korea Food and Drug Administration (KFDA). Serum concentrations of choline after oral administration of choline alphoscerate were determined using a validated LC/MS/MS method. This method showed linear response over the concentration range of 0.5-20 ${\mu}g$/mL with correlation coefficient of 0.9999. The lower limit of quantitation using 100 ${\mu}L$ of serum was 0.5 ${\mu}g$/mL which was sensitive enough for pharmacokinetic studies. Thirty six healthy male Korean volunteers received each medicine at the choline alphoscerate dose of 1200 mg in a $2{\times}2$ crossover study. There was a one-week washout period between the doses. Blood samples were taken at predetermined time intervals up to 8 hr. $AUC_t$ (the area under the serum concentration-time curve from time 0 to 8 hr) was calculated by the linear trapezoidal rule method. $C_{max}$ (the maximum serum drug concentration) and $T_{max}$ (the time to reach $C_{max}$) were compiled from the serum concentration-time data. Analysis of variance was carried out using logarithmically transformed $AUC_t$ and $C_{max}$. No significant sequence effect was found for all of the bioavailability parameters, indicating that the crossover design was properly performed. The 90% confidence intervals of the $AUC_t$ ratio and the $C_{max}$ ratio for Cholicerin/Gliatilin were log0.9998-log1.1172 and log0.9938-1.0944, respectively. These values were within the acceptable bioequivalence intervals of log0.80-log1.25. Thus, the criteria of the KFDA guidelines for the bioequivalence was satisfied, indicating Cholicerin soft capsule and Gliatilin soft capsule are bioequivalent.

Effects of different dietary ratio of metabolizable glucose and metabolizable protein on growth performance, rumen fermentation, blood biochemical indices and ruminal microbiota of 8 to 10-month-old dairy heifers

  • Sun, Jie;Xu, Jinhao;Ge, Rufang;Wang, Mengzhi;Yu, Lihuai;Wang, Hongrong
    • Asian-Australasian Journal of Animal Sciences
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    • 제31권8호
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    • pp.1205-1212
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    • 2018
  • Objective: The aim of this experiment was to evaluate the effects of different dietary ratio of metabolizable glucose (MG) to metabolizable protein (MP) on growth performance, blood metabolites, rumen fermentation parameters and the ruminal microbial community of 8 to 10-month-old heifers. Methods: A total of 24 Holstein heifers weighing an average of 282.90 kg (8 month of age) were randomly assigned to four groups of six. The heifers were fed one of four diets of different dietary MG/MP (0.97, 1.07, 1.13, and 1.26). Results: The results showed that the ratio of MG/MP affected the growth performance, blood metabolites, rumen fermentation parameters and the ruminal microbial community of heifers. The average daily gain of heifers was enhanced by increasing the ratio of MG/MP (p<0.05). The concentration of blood urea nitrogen, cholesterol, and low density lipoprotein cholesterol as well as the concentration of total volatile fatty acid in the rumen fluid of heifers decreased with the improvement in the ratio of dietary MG/MP (p<0.05). However, the relative amount of Ruminococcus albus and Butyrivibrio fibrisolvens in the rumen of heifers was increased significantly (p<0.05) when the dietary MG/MP increased. At the same time, with the improvement in dietary MG/MP, the amount of Fibrobacter succinogenes increased (p = 0.08). Conclusion: A diet with an optimal ratio (1.13) of MG/MP was beneficial for the improvement of growth, rumen fermentation, dietary protein and energy utilization of 8 to 10-month-old dairy heifers in this experiment.