• 대한화학회지
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• 제59권5호
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• pp.407-412
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• 2015

A preconcentration procedure for determination of palladium by laser thermal lens spectrometry (TLS) is proposed. It is based on cloud point extraction of palladium(II) ions as 2-(3,5-dichloro-2-pyridylazo)-5-dimethylaminoaniline (3,5-diCl-PADMA) complexes using octylphenoxypolyethoxyethanol (Triton X-114) as surfactant. The effects of various experimental conditions such as pH, concentration of ligand and surfactant, equilibration temperature and time on cloud point extraction were studied. Under the optimized conditions, the calibration graph was linear in the range of 0.15~6 ng mL⁻¹, and the detection limit was 0.04 ng mL⁻¹ with an enrichment factor of 22. The sensitivity was enhanced by 846 times when compared with the conventional spectrophotometric method. The recovery of palladium was in the range of 96.6%~104.0%. The proposed method was applied to the determination of palladium in water samples.

• 한국기계가공학회지
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• 제19권2호
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• pp.47-54
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• 2020

Themo-mechanical analysis was carried out using the finite element method for the steel shell of a cupola furnace. When the outer surface of the shell was cooled with water to within the temperature range of 35-80 ℃ during operation of the cupola, the inner surface of the shell was expected to exhibit a temperature of 65-248 ℃ based on heat transfer analysis. The shell was also expected to have an equivalent stress range of 100-280 MPa in the outer surface over the temperature range examined. Upon cooling the shell to obtain an outer surface temperature <80 ℃, the maximum equivalent stress of the shell did not exceed the yield strength. Although the temperature of the outer surface varied between 35 and 80 ℃ periodically due to the cooling control problem, the fatigue stress at the outer surface of the shell was calculated to be within the fatigue strength. During a non-operational period to examine the system between furnace operations, the thermal stress presented in the shell was sufficiently low to reach the desired yield strength and fatigue limit.

• Journal of Mechanical Science and Technology
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• 제18권5호
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• pp.820-829
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• 2004

The In-Containment Refueling Water Storage Tank (IRWST), one of the design improvements applied to the APR -1400, has a function to condense the high enthalpy fluid discharged from the Reactor Coolant System (RCS). The condensation of discharged fluid by the tank water drives the tank temperature high and causes oscillatory condensation. Also if the tank cooling water temperature approaches the saturated state, the steam bubble may escape from the water uncondensed. These oscillatory condensation and bubble escape would burden the undue load to the tank structure, pressurize the tank, and degrade its intended function. For these reasons simple analytical modeling and experimental works were performed in order to predict exact tank temperature distribution and to find the effective cooling method to keep the tank temperature below the bubble escape limit (93.3$^{\circ}C$), which was experimentally proven by other researchers. Both the analytical model and experimental results show that the temperature distributions are horizontally stratified. Particularly, the hot liquid produced by the condensation around the sparger holes goes up straight like a thermal plume. Also, the momentum of the discharged fluid is not so strong to interrupt this horizontal thermal stratification significantly. Therefore the layout and shape of sparger is not so important as long as the location of the sparger hole is sufficiently close to the bottom of the tank. Finally, for the effective tank cooling it is recommended that the locations of the discharge and intake lines of the cooling system be cautiously selected considering the temperature distribution, the water level change, and the cooling effectiveness.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 춘계학술대회 논문집 유기절연재료 전자세라믹 방전플라즈마 일렉트렛트 및 응용기술
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• pp.132-137
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• 2002

The mold transformers have been widely used in underground substations in large building and have some advantages in comparison to oil-transformer, that is low fire risk, excellent environmental compatibility, compact size and high reliability. In addition, the application of mold transformer for outdoor is possible due to development of epoxy resin. The mold transformer generally has cooling duct between low voltage coil and high voltage coil. A mold transformer made by one body molding method has been developed for small size and low loss. The life of transformer is significantly dependent on the thermal behavior in windings. To analyse winding temperature rise, many transformer designer have calculated temperature distribution and hot spot point by finite element method(FEM). Recently, numerical analyses of transformer are studied for optimum design, that is electric field analysis, magnetic field, potential vibration, thermal distribution and thermal stress. In this paper, the temperature distribution of 50 kVA pole mold transformer for power distribution are investigated by FEM program and the temperature rise test of designed mold transformer carried out and test result is analyzed compare to simulation data. In this result, the designed mold transformer is satisfied to limit value of temperature and the other property is good such as voltage ratio, winding resistance, no-load loss, load loss, impedance voltage and percent regulation.

• 설비공학논문집
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• 제18권2호
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• pp.129-136
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• 2006

Optimal design of an air-to-liquid finned plate heat exchanger is considered theoretically in this study. Based on existing correlations for the pressure loss and the heat transfer in channel flows, the optimal configuration of the plate heat exchanger including the optimal plate pitch and the optimal fin pitch is obtained to maximize the heat transfer within the limit of the pressure drop for a given flow depth of the plate heat exchanger. It is found that the optimal fin pitch is about one ninth of the optimal plate pitch. In the optimal configuration, the flow and thermal condition in the channels is just at the boundary between the laminar developing and laminar fully developed states. It is also found when reducing the flow depth of plate heat exchangers for compactness, the heat transfer performance can be maintained exactly the same if the geometric parameters such as the plate thickness, plate pitch, fin thickness, and fin pitch are reduced proportional to the square root of the flow depth as long as the flow keeps laminar within the heat exchangers.

• The Journal of the Acoustical Society of Korea
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• 제29권2E호
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• pp.55-63
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• 2010

High Intensity Focused Ultrasound (HIFU) is a noninvasive surgical method mainly targeting deeply located cancer tissue. Ultrasound is generated from an extemally located transducer and the beam is focused at the target volume, so that selective damage can be achieved without harm to overlying or surrounding tissues. The mechanism for cell killing can be combination of thermal and cavitational damage. Although cavitation can be an effective means of tissue destruction, the possibility of massive hemorrhage and the unpredictable nature of cavitational events prevent clinical application of cavitation. Hence, thermal damage has been a main focus related to HIFU research. 2D phased array transducer systems allow electronic scanning of focus, multi-foci, and anti-focus with multi-foci, so that HIFU becomes more applicable in clinical use. Currently, lack of noninvasive monitoring means of HIFU is the main factor to limit clinical applications, but development in MRI and Ultrasound Imaging techniques may be able to provide solutions to overcome this problem. With the development of advanced focusing algorithm and monitoring means, complete noninvasive surgery is expected to be implemented in the near future.

• 설비공학논문집
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• 제18권3호
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• pp.231-239
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• 2006

An experimental investigation of a Reversible Loop Heat Pipe (RLHP) was conducted to determine the operating limits and performance characteristics as functions of the thermophysical parameters, the heat input, and the cooling intensity. Variations in both temperature and heat transport capacity were measured and analyzed in order to accurately evaluate the transient operating characteristics. In addition, the maximum heat transport as a function of the mean evaporator temperature, the ratio of heat transport to heater input power as a function of the mean evaporator temperature, and the overall thermal resistance as a function of the overall heat transport capacity were examined as well. Results indicated that the cooling intensity played an important role on the operating characteristics and performance limitation. The maximum heat transports corresponding to cooling intensity $72W/^{\circ}C$ and $290W/^{\circ}C$ were 446 W and 924 W, respectively. Also, observation of the startup characteristics indicated that the mean evaporator temperature should be maintained between $40^{\circ}C$ and $60^{\circ}C$, and overall thermal resistance were measured as $0.02^{\circ}C/W$.

• 한국산업융합학회 논문집
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• 제23권6_2호
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• pp.935-941
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• 2020

In this study, the effect of different shapes on the heat dissipation characteristics of other porous frames on LED lighting frames was studied using finite element analysis. In addition, the heat transfer characteristics of LED frames were tested using a thermal imaging camera and the results of finite element analysis were compared to derive the optimal hole shape. According to the study, the heat dissipation effect was better for frames with hole compared to existing ones without holes. In particular, the heat dissipation characteristics test showed that for frames with holes, the rise time to the maximum temperature is fast and the maximum temperature is significantly lower. Also, we could see that the square and diamond shapes were smaller than the circular pores, but had a greater heat dissipation effect. Through this study, we have concluded that there is a limit to increasing the heat dissipation effect of the frame with a perforated shape, and it is necessary to conduct further research on the change in the shape of the frame in order to achieve a better heat dissipation effect in the future.

• Nuclear Engineering and Technology
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• 제54권1호
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• pp.72-83
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• 2022

This paper presents a numerical investigation of two-phase natural circulation flows established when external reactor vessel cooling is applied to a severe accident of the APR1400 reactor for the in-vessel retention of the core melt. The coolability limit due to external reactor vessel cooling is associated with the natural circulation flow rate around the lower head of the reactor vessel. For an elaborate prediction of the natural circulation flow rate using a thermal-hydraulic system code, MARS-KS1.5, a three-dimensional computational fluid dynamics (CFD) simulation is conducted to estimate the flow rate and pressure distribution of a liquid-state coolant at the brink of significant void generation. The CFD calculation results are used to determine the loss coefficient at major flow junctions, where substantial pressure losses are expected, in the nodalization scheme of the MARS-KS code such that the single-phase flow rate is the same as that predicted via CFD simulations. Subsequently, the MARS-KS analysis is performed for the two-phase natural circulation regime, and the transient behavior of the main thermal-hydraulic variables is investigated.

• 한국축산식품학회지
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• 제43권6호
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• pp.989-1001
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• 2023

Processed foods containing pork fat tissue to improve flavor and gain economic benefit may cause severe issues for Muslims, Jews, and vegetarians. This study aimed to develop an indirect enzyme-linked immunosorbent assay (iELISA) based on a monoclonal antibody specific to thermal stable-soluble protein in pork fat tissue and apply it to detect pork fat tissue in heat-processed (autoclave, steam, roast, and fry) beef meatballs. To develop a sensitive iELISA, the optimal sample pre-cooking time, coating conditions, primary and secondary dilution time, and various buffer systems were tested. The change in the iELISA sensitivity with different 96-well microtiter microplates was confirmed. The detection limit of iELISA performed with an appropriate microplate was 0.015% (w/w) pork fat in raw and heat-treated beef. No cross-reactions to other meats or fats were shown. These results mean that the iELISA can be used as an analytical method to detect trace amounts of pork fat mixed in beef.