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천연염색에 사용되는 천연매염제에 관한 연구(I) - 볏짚재 -

  • 주영주;남성우
    • Textile Coloration and Finishing
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    • v.9 no.6
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    • pp.33-41
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    • 1997
  • This paper surveys the extraction condition of polygenetic natural dye, Sappan Wood and the effect of ash to the dyeability and fastness. The appropriate time for extracting Sappon Wood was 1hour. The pH was increased as the amount of ash increase. The pH was nearly invariable according to the time of ash solution, the extracting times and temperature. Absorbance of dyeing fabrics was about 480nm. From the result of K/S value determination of fabrics, 10g/$\ell$ quantity of ash was surfficient for treatment and the amount of Sappon Wood was in 100% o.w.f.. K/S value of fabrics pre-mordanted or post-mordanted were higher than that of fabrics simultaneous mordanted.K/S value was increased as pH of mordanting bath decrease and pre-mordanting and post-mordanting fabrics increased the amount of absorption (K/S value) compared with non-mordanted fabrics. It was found that pH of mordanting bath affected the amount of absorption and color change of dyed fabrics. Light fastness of fabric dyed was very poor and the fastness of fabric dyed was not influenced by the mordanting conditions and methods.

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Metallurgical Study of Microconstituents in Transient Liquid Phase Bended Joints of Ni Base Superalloy (Ni기 초내열합금의 액상확산접합부 생성상의 금속조직학적 검토)

  • 김대업
    • Journal of Welding and Joining
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    • v.19 no.1
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    • pp.75-81
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    • 2001
  • The metallurgical study of microconstituents in transient liquid phase bonded joints of Ni-base single crystal superalloys, CMSX-2 and CMSX-4 was investigated employing MBF-80 insert metal. TLP bonding of specimens was carried out at 1,373~1,523K for 0~19.6ks in vacuum. Three types of microconstituents ; needle-like constituent, dot-like constituent and abnormal shape constituent were formed in the bonded interlayer during TLP bonding operation. All these microconstituents were identified as boride. Microconstituents contain a large percentage of Cr in the early stage of bonding. As increasing the holding time, the amount of Cr was decreased and the amount of W, Co and Re were increased. From the analysis results of electron diffraction pattern by TEM, composition of elements in microconstituents were into MBlongrightarrowM$_{5}$B$_3$longrightarrowM$_2$B type with the increased in holding time. It can be explained by the fact that the relative amount of boron in microconstituents was decreased when the holding time was increased.d.

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Influence of Liquid-Phase Amount on the Microstructure and Phase Transformation of Liquid-phase Sintered Silicon Carbide (액상량이 탄화규소 소결체의 미세구조 및 상변태에 미치는 영향)

  • 이종국;강현희;박종곤;이은구
    • Journal of the Korean Ceramic Society
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    • v.35 no.4
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    • pp.413-419
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    • 1998
  • ${\beta}$-silicon carbides with yttrium aluminum garnet of 2,5,10 mol% were prepared by a liquid--phase sint-ering and the microstructural evolution and phase transformation were investigated during sintering as functions of liquid-phase amount and sintering time. The rate of grain growth decreases with the addition of the amount of yttrium aluminum garnet (YAG) in the SiC starting powder however the apparent density and the aspect ratio of grains in sintered body increase. The phase transformation from ${\beta}$-SiC to ${\alpha}$-SiC were dependent on the liquid-phase amount and sintering time.

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A Study on the Efficient Applicability of Fenton Oxidation for the Wastewater Containing Non-biodegradable Organics (생물난분해성 유기물질 함유 폐수처리를 위한 Fenton 산화법의 효율적 적용방안에 관한 연구)

  • Jun, Se Jin;Kim, Mi Jeong
    • Journal of Korean Society of Water and Wastewater
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    • v.14 no.1
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    • pp.76-83
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    • 2000
  • This research is about wastewater containing non-biodegradable TDI(Toluene Diisocyanate) that is treated by the activated carbon adsorption method. In the case of the Fenton oxidation process being applied to the existing process, optimal pH, reaction time, chemical dosing amount, removal rate, and cost were investigated. A pilot plant test was applied after finding optimal conditions with lab experiments. The optimal conditions were pH 3~5(COD removal rate 84~88%) and reaction time 30min~1hr. In higher $H_2O_2$ dosing amount, COD removal rate was a little higher. But there was little difference in the removal rate according to $FeSO_4{\cdot}7H_2O$ dosing amount. Treatment cost was economical in the case of the Fenton oxidation process being operated earlier than activated carbon adsorption system. But chemical dosing point, chemical mixing effect, chemical dosing amount, removal rate, and the cost of facility and others must be considered in practical process.

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Influence of Coating Conditions on Fe Dissolution and Dross Formation in Continuous Hot-dip Galvanizing Process (연속 용융아연도금 공정에서 Fe용출 및 드로스 발생에 미치는 도금조건의 영향)

  • 전선호;김상헌
    • Journal of the Korean institute of surface engineering
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    • v.36 no.5
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    • pp.364-372
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    • 2003
  • In continuous galvanizing process, dissolution of iron into molten zinc results in a fairly great amount of dross. In order to decrease dross, the amount of dissolved iron of strip in molten zinc was investigated in the range of 0∼0.22%Al content, 440∼$470^{\circ}C$ strip temperature and 3∼60 sec dipping time. Uniform Fe-Al-Zn inhibition layer was formed in the coating layer/strip interface not only in the grain boundary but also in the grain of substrate with the increase of Al content in the zinc pot, while the amount of iron dissolution was decreased. Inhibition layer was unstable as the dipping time and strip temperature increased and the amount of iron dissolution increased.

A basic study for the rapid green sand control (신속한 생형사(生型砂) 관리(管理)를 위한 기초연구)

  • Kim, M.H.;Kwun, S.I.;Kang, C.S.;Na, D.J.
    • Journal of Korea Foundry Society
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    • v.7 no.3
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    • pp.199-206
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    • 1987
  • This paper presents experimental data for the computerization of green sand control. The results can be summarized as follows: 1. To obtain the proper compactability at the mixer, the addtion of moisture is far more efficient than the control of mixing time or addtion of clay. 2. The log R(% clay/% moisture) vs. log compactability curve moves upward as the amount of clay increases and moves downward as the amount of seacoal, dead bentonite or coked seacoal increases. 3. The ratio of dead to initial clay amount or coked to initial seacoal amount is changed according to sand to metal ratio, mainly, and according to pouring temperature, partly, at a shake out time of 12hrs.

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THE EFFECTS OF MECHANICAL FORCE ON CULTURED PERIODONTAL LIGAMENT CELLS IN VITRO (물리적 외력이 배양중인 치주인대세포에 미치는 영향)

  • Kim, Hyun-young;Cha, Kyung-Suk
    • The korean journal of orthodontics
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    • v.24 no.2
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    • pp.295-301
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    • 1994
  • The movement of teeth during orthodontic treatment requires bone remodeling process in periodontal tissue. To find out the changes occuring in the cell itself, mechanical force was applied to the cultured periodontal ligament cells. Following results were obtained from measuring the changes in cyclic AMP and $PGE_2$, $^3H$-thymidine incorporation amount in time lapse after application of mechanical force. 1. When mechanical force was applied to cultured PDL cells, the amount of cAMP in cells were increased significantly after 15 min. of force application, but were decreased gradually as time lapsed. 2. When mechanical force was applied to cultured PDL cells, the amount of PGE2 were increased at 20,40,60 min. and was significantly increased at 20 min. 3. When mechanical force was applied to cultured PDL cells, the amount of $^3H$-thymidine incorporation was some increased, but was not statistically significant.

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Effect of Shifting Planting - time and Different Nitrogen Level on the Yield and Characteristics of Plant Growth in Safflower, Carthamus Tinctorius L. (파종기 추동 및 질소비료수준차이가 홍화의 생육, 수량에 미치는 영향)

  • 박종선
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.26 no.1
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    • pp.96-102
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    • 1981
  • Effect of shifting planting-time and different nitrogen on the yield and characteristics of plant growth in safflower, Chrthamus Tinctorius L. This study was carried out to investigate the optimum sowing-date and the ecological variations due to differerent amount of nitrogen for safflower on the Experiment Farm of Sang Ji college from March 17 to may 16, 1980, sowing seeds with an interval of 10 days and the amount of nitrogen were applied in 5 levels (Non, half-standard, standard, one and half-ordinary amount-No and twice amount). The triple super phosphate and pottassium chloride were applied only in standard amount. The results obtained are summarized as follows; 1. As sowing-date was delayed, the germination-ratio decreased, germinating speed increased, and the time required to attain the most vigorous germinating stage and days required for germination shortened. 2. Plant height, number of branch and stem diameter showed a decrease as sowing-date was delayed. And at the same time, plant height and number of branch showed a tendency to increase as amount of nitrogen was increased. 3. As sowing-date was delayed, the number of pods and the weight of 1000-grains were decreased. Moreover, the earlier sowing-date was, the more it increased. And as amount of nitrogen was increased, number of pods and yield also were strikingly increased. 4. The fresh-weight of flower with orange and orange-red colour, as influenced by the different sowing-date, was found out to be largest at the begining of April. But increasing amount of nitrogen did not show influence upon the promotion of flowering. 5. Judging from the results reported above, the optimum sowing-date of safflower seemed to be the begining of April; also the culture of safflower seemed to be the effects of much amount of nitrogen.

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Evaluation of the Charcoal Tube Sampling Method for Carbon Disulfide in Air (활성탄관법을 이용한 공기중 이황화탄소 농도 측정법에 관한 연구)

  • Lee, Na Roo;Paik, Nam Won
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.3 no.1
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    • pp.22-36
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    • 1993
  • This study was conducted to evaluate the charcoal tube sampling method for carbon disulfide in the air. Breakthrough was investigated according to flow rate, sampling time and air volume. Also the storage stability by storage method and time was investigated. The results are summarized as follows. 1. The samples stored at room temperature($28.2^{\circ}C$), refrigerator($3.8^{\circ}C$) and freezer($-15.6^{\circ}C$) were analyzed every week to five weeks. At one week storage at room temperature, 3.5% of $CS_2$ in the front section of the charcoal tube migrated into the back section and 57.7% at five weeks. The amount of $CS_2$ in the back section of the charcoal increased continuously by storage time. Migration of $CS_2$ was slow at refrigerator, and stopped occur at freezer. Recovery rate $CS_2$ was 52-82% at room temperature and 92-101% at refrigerator, based on the amount at freezer as a reference value. Thus loss was observed at room temperature. 2. When 6-48 L of fresh air were passed through tubes with spiked amounts of 0.379 and 0.759mg sample, the amounts of $CS_2$ in the back section of charcoal were 5.7-132.4 and 0-92% of the amount in the front section, respectively. The total recovery rates of$CS_2$ from 0.379 and 0.759mg spiked sample were 35.7-101.0% and 9l.3-100.1%, respectively. $CS_2$ loss was observed in 0.379mg spiked sample, but not in 0.759mg spiked sample. In the spiked samples, the amount of $CS_2$ in the back section of charcoal was not affected by flow rate when the air volume was controlled. The amount of $CS_2$ in the back section of charcoal increased over sampling time. And the faster the flow rate, the more the migration amount when the sampling time was the same. 3. A known concentration, 10 ppm of $CS_2$, was produced in a 200 L Tedlar bag. When the air volume was 24, 36, 48 L, breakthrough was 5.8, 16.9, 47.4%, respectively. The sampling flow rate of 0.05, 0.1, 0.2 Lpm did not change the breakthrough rate. Breakthrough increased over sampling time. And the faster the flow rate, the more the breakthrough, when the sampling time was the same.

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The Relationship between Private Tutoring and Academic Achievement - An Application of a Multivariate Latent Growth Model -

  • Nam, Su-Jung
    • International Journal of Human Ecology
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    • v.14 no.1
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    • pp.29-39
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    • 2013
  • The study examined how changes in time invested in private tutoring and academic achievement influenced each other through a multivariate latent growth model by using the data from the first to the third year presented in the KYPS. This study identifies not only how changes in the private tutoring experience exerted a direct influence on changes in academic achievement, but also measures what kind of changes in private tutoring and academic achievement had emerged over time. The detailed study results are as follows. First, the analysis of time invested in private tutoring showed that the higher the grades, the greater were the amount of time invested in private tutoring in the case of Korean language study. On the other hand, the results showed that in the case of English and mathematics, the higher the grades, the lesser was the amount of time invested in private tutoring. Second, private tutoring and academic achievement were all in a linear relationship. Third, it was shown that the time invested in private tutoring and academic achievement exerted a negative influence on each other according to the passage of time.