• Korean Journal of Materials Research
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• v.10 no.6
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• pp.409-414
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• 2000

Three different white cast irons alloyed with Cr, V, Mo and W were prepared in order to study their transformation behavior of matrix structures in heat-treated conditions. The specimens were produced using a 15kg-capacity high frequency induction furnace. Melts were super-heated to $1600^{\circ}C$, and poured at $1550^{\circ}C$ into Y-block pepset molds. Three combinations of the alloying elements were selected so as to obtain the different types of carbides and matrix structures : 3%C-10%Cr-5%Mo-5%W(alloy No. 1), 3%C-10%V-5%Mo-5%W(alloy No. 2) and 3%C-17%Cr-3%V(alloy No. 3). The heat-treatments were conducted as follows: frist of all, as-cast specimens were homogenized at $950^{\circ}C$ for 5h under the vacuum atmosphere. Then, they were austenitized at $1050^{\circ}C$ for 2h and followed by air-hardening in air. The air-hardened specimens were tempered at $300^{\circ}C$ for 3h. The observation of morphology of the matrix structures was carried out in the states of as-cast(AS), air-hardened(AHF) and tempered(AHFT). The matrix structures of each alloy were almost fully pearlitic in the as-cast state but it was transformed to martensite, tempered martensite and retained austenite by the heat-treatments such as air-hardening and tempering.

• Journal of Korea Foundry Society
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• v.28 no.3
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• pp.119-123
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• 2008

Wear test on two die steels for aluminum die casting was carried out by dipping and rotating the specimens into the molten aluminum maintained $680^{\circ}C{\sim}780^{\circ}C$. The rotating speed of the specimen was $4.5rpm{\sim}20.0rpm$. Diffusion layer was formed between the die steel and molten aluminum, and became thicker with dipping time. Wear rate was not proportional with the thickness of the diffusion layer, but was closely related to the density of the diffusion layer. Wear rate was little affected by the kind of die steel and by the microstructure such as martensite, tempered martensite, and pearlite. Specimen with nitrided surface showed good wear resistance, and its wear rate was decreased with increase in the thickness of nitrided layer. While whole surface was worn in heat treated specimens, wear of nitrided specimens was proceeded by pitting partially.

• Tribology and Lubricants
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• v.36 no.1
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• pp.18-26
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• 2020

The effects of the carburizing process on the sliding wear behavior of SCM420H steel have been investigated. In particular, the effects of grain boundary corrosion observed in the surface layer after gas carburizing and the effects of hardness of the carburized cases after heat-treatment on the sliding wear properties were examined. Pin specimens carburized by two methods (gas carburizing and vacuum carburizing) were tempered at two temperatures of 180℃ and 400℃ after oil-quenching, respectively. Sliding wear tests were carried out against heattreated SKH51 steel at several sliding speeds using a pin-on-disc type test machine. As results, it can be found that there is no difference in the wear behavior between the pins carburized using two methods. This implies that the grain boundary corrosion that formed in the surface layer after gas carburizing has no effect on the sliding wear behavior of carburized SCM420H steels. Additionally, there is no significant difference in the wear behavior between carburized pins tempered at 400℃ and at 180℃ after oil-quenching, regardless of the carburizing method. This is because carburized pins tempered at 400℃ have a troostite structure, which exhibits higher tribochemical reactivity even though its hardness is lower than that of martensite structure. In this respect, it can be considered that good wear resistance of carburized cases is maintained at least until the effective case depth.

• Journal of the Korean Society for Heat Treatment
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• v.35 no.6
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• pp.303-313
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• 2022

The purpose of this study was to test and analyze the effects of the mechanical properties and structural changes of the austenitized and tempered martensite STS 410 stainless steel containing 11.5~13%Cr and 0.10%C on its temper embrittlement. The STS 410 stainless steel test pieces for each 3 hours at 960℃, 1000℃ and then, tempered them for 2 hours at 300℃, 350℃, 400℃, 450℃, 500℃, 550℃, 600℃, 650℃ and 700℃ known as the intervals vulnerable to temper embrittlement to observe the changes of their structures and mechanical properties. In case autenitizing was insufficient due to lower temperature of thermal treatment for solution, unsolved carbides and ferrites remained in the structure after quenching, which meant that the parts could wear out and corrode to embrittle at the room temperature. Elongation and impact energy changes with Tempering conditions showed minimum results in range of 400~500℃. The decrease in elongation and impact energy at 400~500℃ was the hardening effect of the subgrain due to the precipitation of many M₃C or M₇C₃, M₂₃C₆. And STS 410 stainless steel corrosion tested in 10% NaCl solution at 30℃ after tempering treatment. The degree of corrosion sensitization showed increasing tendency with increase of tempering temperature and Cr carbide precipitation were observed in grain boundary.

• Journal of Welding and Joining
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• v.15 no.4
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• pp.116-125
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• 1997

Electron beam weldability of 9%Ni steels has been investigated to apply EBW to the construction of LNG storage tank. While mechanical properties of welded joints were satisfied by ASTM specification, impact energy of weld metal was as low as 27 - 55J at $-196^{\circ}C$. As the result of Ni wires inserted at the joint to be welded, Ni content of weld metal was increased to about 10%, resulting on the improvement of impact toughness to 110 ~ 120J at $-196^{\circ}C$. This improvement of impact toughness in weld metal was due to the formation of tempered martensite and retained austenite. Above results indicate that, if Ni content of weld metal was increased about 10% by Ni wires addition, electron beam welded 9%Ni steels weld metal had sufficient impact energy necessary for a LNG storage tank.

• Steel and Composite Structures
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• v.14 no.3
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• pp.229-242
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• 2013

Corrosion is important reason for the deterioration of the bond between reinforcing steel and the surrounding concrete. Corrosion of the steel mainly depends on its microstructure. Smooth S220, ribbed S420 and S500 grade reinforcing steels were used in the experiments. Samples were subjected to accelerated corrosion. Pullout tests were carried out to evaluate the effects of corrosion on bond strength of the specimens. S500 grade steel which has tempered martensite microstructure showed lower corrosion rate in concrete than S220 and S420 steels which have ferrite+perlite microstructure. S500 grade steel showed highest bond strength among the other steel grades in concrete. Bond strength between reinforcing steel and concrete increased with increase in the strength of steel and concrete. It also depends on whether reinforcing bar is ribbed or not.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1992.04a
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• pp.84-88
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• 1992

Laser beam hardenling of 12%-Cr steel has been evaluated by using a continuous wave 3 kW CO$\_$2/ laser with a hardening mirror set. Experiment was performed on the optimum hardening condition with a laser power of 2.85kW and travel speed of 10 and 5 m/min. Multi passes have been alsotried to find the hardening characteristics of partly overlapped zone. The black paint to use at high temperature was adopted to increases the absorptivity of laser beam energy with the wavelength of 10.6 .mu. m at the surface of bese metal. The microstructure of the hardened layers was observed by using a light microscopy. SEM and TEM. A fine lamellar martensite formed in the hardened zones exhibits very high Vickers microhardness of 600 Hv, whereas the tempered martesite distributes in the base metal with Vickers microhardness of 240 Hv. It has been found that laser hardening with multi pass showed no significant drop of the hardness between adjacent passes.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.03a
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• pp.240-243
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• 1997

The Quenching and Self Tempering (QST) rolling is treated in terms of an advance process on Controlled Rolling and Cooling Technology (CRCT). In the analysis, the effect of this process is governed by both quenching and finishing conditions in the related with temperature. The objective of the QST model is to simulate the temperature gradient of the stock being rolled in the rolling mill. A comparison of computer simulated and manufactured micro structure as well as mechanical properties shows a good consistency. The micro structure of this high-strength round bar consists of tempered martensite and ferrite + pearlite phases.

• Journal of the korean Society of Automotive Engineers
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• v.9 no.2
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• pp.28-33
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• 1987

This thesis is to improve the mechanical properties of carbon steel by the ion-nitriding, and post-heat treatment. The structures of ion-nitrided SM45C steel were changed to martensite by quenching from 730.deg. C and 800.deg. C. And then a few of the quenched specimens was tempered at 200.deg. C for 120 min. The emphasis in this study is focussed on Comparison of hardness and fatigue strength with the ion-nitrided steel. The results obtained are summerized as follows. 1. To improve the hardness and fatigue strength of ion-nitrided steels, it is effective to under take diffusion treatment for a short time at the austenite temperature(800.deg. C). 2. If ion-nitrided steel is heated for a long time at high temperature, de-nitriding occure. 3. The quenching treatment after nitriding on the carbon steel is necessary to improve the mechanical properties of the steels.

• Journal of the Korean institute of surface engineering
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• v.17 no.1
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• pp.7-13
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• 1984

Carburizing of a 12%Cr steel containing 0.6%Si was performed at 950$^{\circ}C$ for various times, and the microstructure, hardness and the water characteristics of the carburized chromium steel were examined. The results obtained in this study are as follows: 1. Carbide-dispersed layer (CD layer) with fine dispersion of $Cr_7C_3$ in martensite matrix was formed by carburizing. The radius and amount of the carbides in the surface region of CD layer were about 0.3${\mu}m$ and 35% by volume, respectively. 2. Chromium steel carburized and quench-tempered showed better wear resistance and hardness than ordinary high chromium tool steel. It is concluded from these results that fine dispered carbides are very effective in improving wear resistance and hardness.