• Title/Summary/Keyword: synchrotron

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Synchrotron X-Ray Diffraction Studies on Crystalline Domains in Urea-Formaldehyde Resins at Low Molar Ratio

  • WIBOWO, Eko Setio;PARK, Byung-Dae;CAUSIN, Valerio;HAHN, Dongyup
    • Journal of the Korean Wood Science and Technology
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    • v.50 no.5
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    • pp.353-364
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    • 2022

  • The crystalline domain of thermosetting urea-formaldehyde (UF) resins at low formaldehyde-to-urea (F/U) molar ratios (≤ 1.0) is known to be responsible for their poor performance as wood adhesives. Crystallization has been observed in 1.0 F/U UF resins during the addition reaction stage and at the end of the synthesis process (neat UF resins). The crystallinity and X-ray diffraction (XRD) spectra of the uncured neat UF resins, on the other hand, differed significantly from those of the cured neat UF resins, raising the possibility that their crystal structures were also different. This study demonstrates for the first time that the crystalline domains in 1.0 F/U UF resins generated from uncured and cured samples are identical. Despite having a lower crystallinity value, the synchrotron XRD patterns of purified neat UF resins were equivalent to the XRD patterns of cured neat UF resins. Transmission electron microscope images of the cured UF resins showed that the crystals were lamellar structures. This finding suggests that the crystal at low molar ratio UF resins are isotropic polycrystals with random orientation.

  • https://doi.org/10.5658/WOOD.2022.50.5.353 인용 PDF KSCI

Magnetic Field Strengths of Flaring Region in the Jet of CTA 102

  • Kim, Sang-Hyun;Lee, Sang-Sung
    • The Bulletin of The Korean Astronomical Society
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    • v.46 no.1
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    • pp.32.1-32.1
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    • 2021

  • We present the magnetic field strengths of CTA 102 using multi-frequency data at 2.6-343.5 GHz in order to study the physical origins of radio flares. The observations at 22 and 43 GHz were conducted using the single-dish radio telescopes of the Korean VLBI Network (KVN) from December 2012 until May 2018 (MJD 56200-58400). We used multi-frequency data obtained from the Effelsberg 100-m, OVRO 40-m, Metsähovi 14-m, IRAM 30-m, SMA, ALMA, and VLBA telescopes. During the period of the observations, two major flares (R1 and R2) are seen clearly at 15 and 37 GHz during MJD 57500-57800 and MJD 58000-58300, respectively. The source shows typical variability with time-scales ranging from 20-161 days at 15 GHz. The variability Doppler factor is in the range of 11.51-31.23. The quasi-simultaneous radio data are used to investigate the synchrotron spectrum of the source, finding that the synchrotron radiation is self-absorbed. The turnover frequency and the peak flux density of the synchrotron self-absorption (SSA) spectra are in ranges of 38.06-167.86 GHz and 1.49-10.38 Jy, respectively. From the SSA spectra, magnetic field strengths are estimated to be < 10 mG. The equipartition magnetic field strengths are larger than the SSA magnetic field strengths by a factor of > 100. This indicates that the radio flares may be related to a particle energy-dominated emission region.

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