• 제목/요약/키워드: surface treating

검색결과 429건 처리시간 0.028초

아르곤 저온 플라즈마 처리에 의한 CTA 필름의 접착성 연구 (A Study on Adhesive Properties of Cellulose Triacetate Film by Argon Low Temperature Plasma Treatment)

  • 구강;박영미
    • 한국염색가공학회지
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    • 제16권5호
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    • pp.28-34
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    • 2004
  • The polarizing film application exploits the unique physicochemical properties between PVA(Poly vinyl alcohol) film and CTA(Cellulose triacetate) film. However, hardly any research was aimed at improving the adhesion characteristics of the CTA film by radio frequency(RF) plasma treatment at argon(Ar) gaseous state. In this report, we deal with surface treatment technology for protective CTA film developed specifically for high adhesion applications. After Ar plasma, surface of the films is analyzed by atomic force microscopy(AFM), roughness parameter and peel strength. Furthermore, the wetting properties of the CTA film were studied by contact angle analysis. Results obtained for CTA films treated with a glow discharge showed that this technique is sensitive to newly created physical functions. The roughness and peel strength value increased with an increase in treatment time for initial treatment, but showed decreasing trend for continuous treatment time. The result of contact angle measurement refer that the hydrophilicity of surface was increased. AFM studies indicated that no considerable change of surface morphology occurred up to 3 minutes of treatment time, but a considerable uneven of surface structure resulted from treating time after 5 minutes.

전기 응고법을 이용한 커피박의 전처리 및 기능성 필터 특성 연구 (A Study on the Pretreatment of the Spent Coffee Grounds using Electrocoagulation and Its Filter Characteristics)

  • 박수빈;한하늘;박하늘;임승현;유봉영;윤상화
    • 한국표면공학회지
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    • 제54권4호
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    • pp.209-214
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    • 2021
  • As coffee consumption per person increases annually to 323 cups in 2018, treating the spent coffee ground has arisen because spent coffee ground results in soil and air pollution. The demands of air purification filters are increasing more and more because the air pollution due to the fine dust has become worse. The spent coffee grounds had a porous structure, however, the pore was blocked by organic oil compounds. Electrocoagulation, which is one of the electrochemical methods, has the potential to remove the organic compounds. The surface area of spent coffee grounds increased effectively after the electrocoagulation treatment, and surface morphology and surface area were confirmed using SEM and BET, respectively. Using the FT-IR, both the spent coffee grounds and the electrocoagulated spent coffee grounds were characterized. The filter characteristics were examined by the adsorption test using formaldehyde, one of the air pollutants.

타이타늄 표면 코팅 처리에 따른 타이타늄도재관의 파절강도 비교 (A COMPARISON OF FRACTURE STRENGTHS OF PORCELAIN-FUSED-TO-TITANIUM CROWN AMONG TITANIUM SURFACE COATING TREATMENTS)

  • 김지혜;박상원;방몽숙;양홍서;박하옥;임현필;오계정;김현승;이광민;이경구
    • 대한치과보철학회지
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    • 제45권2호
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    • pp.203-215
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    • 2007
  • Statement of problem: Titanium and its alloy, with their excellent bio-compatibility and above average resistance to corrosion, have been widely used in the field of dentistry. However, the excessive oxidization of titanium which occurs during the process of firing on porcelain makes the bonding of titanium and porcelain more difficult than that of the conventional metal-porcelain bonding. To solve this problem related to titanium-porcelain bonding, several methods which modify the surfaces, coat the surfaces of titanium with various pure metals and ceramics, to enable the porcelain adhesive by limiting the diffusion of oxygen and forming the adhesive oxides surfaces, have been investigated. Purpose: The purpose of this study was to know whether the titanium-porcelain bonding strength could be enhanced by treating the titanium surface with gold and TiN followed by fabrication of clinically applicable porcelain-fused-to-titanium crown Material and method: The porcelain-fused-to-titanium crown was fabricated after sandblasting the surface of the casting titanium coping with $Al_2O_3$ and treating the surface with gold and TiN coating followed by condensation and firing of ultra-low fusing porcelain. To compare with porcelain-fused-to-titanium crowns, porcelain-fused-to-gold crowns were fabricated and used as control groups. The bonding strengths of porcelain-fused-to-gold crowns and porcelain-fused-totitanium crowns were set for comparison when the porcelain was fractured on purpose to get the experimental value of fracture strength. Then, the surface were examined by SEM and each fracturing pattern were compared with each other Result:Those results are as follows. 1. The highest value of fracture strength of porcelain-fused-to-titanium crowns was in the order of group with gold coating, group with TiN coating, group with $Al_2O_3$ sandblasting. No statistically significant difference was found among the three (P>.05). 2. The porcelain-fused-to-gold crowns showed the highest value in bonding strength. The bonding strength of crowns porcelain-fused-to-titanium crowns of rest groups showed bonding strength reaching only 85%-94% of that of PFG, though simple comparision seemed unacceptable due to the difference in materials used. 3. The fracturing patterns between metal and porcelain showed mixed type of failure behavior including cohesive failure and adhesive failure as a similar patterns by examination with the naked eye and SEM. But porcelain-fused-to-gold crowns showed high incidence of adhesive failure and porcelain-fused-to-titanium crowns showed high incidence of cohesive failure. Conclusion: Above results proved that when fabricating porcelain-fused-to-titanium crowns, treating casting titanium surface with gold or TiN was able to enhance the bonding strength between titanium and porcelain. Mean value of masticatory force was found to showed clinically acceptable values in porcelain bonding strength in all three groups. However, more experimental studies and evaluations should be done in order to get better porcelain bonding strength and various surface coating methods that can be applied on titanium surface with ease.

불연속면을 포함하고 있는 회전형 완전도체의 전류분포특성 (Current distribution of a conducting body of revolution includig discontinuous surface)

  • 김경언
    • 한국광학회:학술대회논문집
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    • 한국광학회 1990년도 제5회 파동 및 레이저 학술발표회 5th Conference on Waves and lasers 논문집 - 한국광학회
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    • pp.29-33
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    • 1990
  • Efficient numerical method is developed for treating electromagnetic problems of scattering and radiation from surfaces. Special consideration is given to the treatment of edges so that rather arbitrary geometrical configurations may be handled. For the conducting body problems considered, an electric field integral formulation is used, and the method of moments is applied using pulse expantions to present currents. Numerial results indicate that the approach is free os anomalies in the behavior of current for body of revoution.

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숏크리트용 폴리프로필렌 섬유의 개발 (Development of Polypropylene Fiber for Shotcrete)

  • 하태욱;양형식
    • 터널과지하공간
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    • 제14권4호
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    • pp.241-247
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    • 2004
  • 본 연구에서는 숏크리트 보강용으로 폴리프로필렌 섬유의 표면을 무수말레인산이 그라프트된 폴리프로필렌(mPP)으로 표면 개질 처리한 새로운 폴리프로필렌 섬유를 개발하고, 개발된 섬유의 분산성을 조사하였다. 이 보강섬유가 혼입된 숏크리트의 강도 특성을 조사하였다.

Production of a Monoclonal Antibody and Ultrastructure of the Sporozoite of Cryptosporidium parvum

  • Choi, Young-Sook;Lee, Sung-Tae;Cho, Myung-Hwan
    • Journal of Microbiology
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    • 제34권4호
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    • pp.379-383
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    • 1996
  • Cryptosporidium parvum causes a life-threatening diarrhea in acquired immunodeficiency syndrome (AIDS) patients. THe sporozoite stage of C. parvum has been known to be a target in treating cryptosporidiosis in AIDS patients as it is an extracellular stage. A sporozoite was ultrastructurally observed. It has a creascent shape with a rounded posterior end and a tapering body. The compact nucleus was located at the posterior end. A monoclonal antibody was produced, which recognized a 43 kDa of sporozoite antigens in a western blot analysis and showed the surface labeling in immunofluorescence.

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강관 유도 광휘 열처리 시스템 개발에 관한 연구 (A Study on the Development of Induction Bright Annealing System for Stainless Steel Welded Pipe & Tubes)

  • 신완호;배종수;이주석
    • 연구논문집
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    • 통권22호
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    • pp.97-105
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    • 1992
  • This study aimed to develop the heat treating equipment which could produce austenitic stainless steel welded pipes & tubes maintaining its peculiar brightness even after heat treatment. The results of this study are as follows:- Development of 8.5kHz, 150kw bright annealing system was achieved. - Bright annealing of austenitic stainless steel welded pipes & tubes was performed by the developed pilot-system through this study and heat-treatment effects were quite successful in viewpoint of surface brightness, hardness distribution, microstructure, removal of residual stress, strength and corrosion resistance.

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4-META의치상레진과 Cobalt-Chromium계 합금의 접착강도에 관한 연구 (A STUDY ON THE BOND STRENGH OF 4-META ACRYLIC RESIN DENTURE BASE TO COBALT-CHROMIUM ALLOYS)

  • 성무경;김광남;장익태
    • 대한치과보철학회지
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    • 제28권2호
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    • pp.29-51
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    • 1990
  • This study was designed to compre the tensile bond strength of 4-META containging denture base resin to Co-Cr alloys after various surface treatments. Especially the surface treatment of sandblasting the mental with aluminum oxide and treating in oxidizing solution composed of 3% aqueous sulfuric acid with 1% potassium manganate were compared. Effect of surface roughness on bonding was measured after sandblasting with 50um, 300um aluminun oxide and polishing with emery pater. Also the effects of wax and wax solvent on bonding were observed. According to the type of polymerization process, heat-cured Meta-Dent resin and autopolymerizing Meta-Fast resin were used. For some specimnens, the tensile bond strength were measured agter three pre-conditions : 1day after bonding, immersed in water at $75^{\circ}C{\pm}3^{\circ}C$ for 4weeks, under normal ambient condition for 4weeks. The following results were obtained from this study : 1. The bond strengths of resins containing 4-META were significantly higher than those of conventional denture base resins(p<0.05). 2. Autopolymerizing Meta-Fast resin had higher bond strength than heat-cured Meta-Dent, resin(p<0.05). 3. The bond strengths of Biosil and Nobilium to 4-META containging resins were not significally different(p>0.05). 4. Stable adhesion can be achieved when mechanically roughen the metal surface by snadblasting with $50{\mu}m$ aluminum oxide than treating in an oxidizing soluing with potassium manganate(p<0.05). 5. Once the metal surface is contaminated with wax, the bond srtength decreased greatly in spite of wax wash with boiling water. But the bond strength recovered significantly with the use of wax solvent 6. Meta-Dent resin had higher bond strength when roughen the metal surface with $50{\mu}m$ aluminum oxide than with $300{\mu}m$ aluminum oxide(p<0.05). In case of Meta-Fast, resin, the use of $300{\mu}m$aluminum oxide was a little advantageous of bonding, but was statistically insignificant(p>0.05).

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SiC 증착층 계면의 표면조도에 미치는 흑연 기판의 표면조도 영향 (Effects of the Surface Roughness of a Graphite Substrate on the Interlayer Surface Roughness of Deposited SiC Layer)

  • 박지연;정명훈;김대종;김원주
    • 한국세라믹학회지
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    • 제50권2호
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    • pp.122-126
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    • 2013
  • The surface roughness of the inner and outer surfaces of a tube is an important requirement for nuclear fuel cladding. When an inner SiC clad tube, which is considered as an advanced Pressurized Water Cooled Reactor (PWR) clad with a three-layered structure, is fabricated by Chemical Vapor Deposition (CVD), the surface roughness of the substrate, graphite, is an important process parameter. The surface character of the graphite substrate could directly affect the roughness of the inner surface of SiC deposits, which is in contact with a substrate. To evaluate the effects of the surface roughness changes of a substrate, SiC deposits were fabricated using different types of graphite substrates prepared by the following four polishing paths and heat-treatment for purification: (1) polishing with #220 abrasive paper (PP) without heat treatment (HT), (2) polishing with #220 PP with HT, (3) #2400 PP without HT, (4) polishing with #2400 PP with HT. The average surface roughnesses (Ra) of each deposited SiC layer are 4.273, 6.599, 3.069, and $6.401{\mu}m$, respectively. In the low pressure SiC CVD process with a graphite substrate, the removal of graphite particles on the graphite surface during the purification and the temperature increasing process for CVD seemed to affect the surface roughness of SiC deposits. For the lower surface roughness of the as-deposited interlayer of SiC on the graphite substrate, the fine controlled processing with the completed removal of rough scratches and cleaning at each polishing and heat treating step was important.

표면결정화유리에 관한 연구 (A Study on the Surface Crystallization of Glass)

  • 박용완;강은태
    • 한국세라믹학회지
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    • 제14권4호
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    • pp.230-235
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    • 1977
  • In this paper the conditions of surface crystallization of glass were studied. The basic glass which is apt to crystallize, with $SiO_2$ 72.50, $Al_2O_3$ 5, 00, $Na_2O$ 8.00 $K_2O$ 3.50, CaO 5.00, MgO 3.00, $B_2O_3$ 3.00 Wt% is chosen. The strain point and softening point of this glass is 4$25^{\circ}C$ and 778$^{\circ}C$ each, and between the two temperatures we could get grystal on its surface by immersion in salt baths during some controlled hours. The kind of crystal on the surface of glass was confirmed by X-ray diffraction analysis and the change of the thickness of crystalline layers depending on temperature and time, was surveyed by using optical microscope. The results are as follows; 1. The chloride group is more suitable than sulfate group for the treating salt. 2. In the condition with 50 LiCl.50NaCl at 62$0^{\circ}C$ for 2 hrs and with 50 LiCL.20-30 NaCl.30-20 $CaCl_2$ at 72$0^{\circ}C$ for 15-20 min. we could get the best crystalline layers. 3. The crystal was silica-O and petalite with a little tridymite and nepheline. 4. The thickness of crystalline layers increased with increasement of temperature and time.

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