• 한국압력기기공학회 논문집
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• 제13권2호
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• pp.60-66
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• 2017

The standard master curve (MC) approach has the major limitation because it is only applicable to homogeneous datasets. In nature, materials are macroscopically inhomogeneous and involve scatter of fracture toughness data due to various deterministic material inhomogeneity and random inhomogeneity. RPV(reactor pressure vessel) steel has different fracture toughness with varying distance from the inner surface of the wall due to cooling rate in manufacturing process; deterministic inhomogeneity. On the other hand, reference temperature, $T_0$, used in the evaluation of fracture toughness is acting as a random parameter in the evaluation of welding region; random inhomogeneity. In the present paper, four regions, the surface, 1/8T, 1/4T and 1/2T, were considered for fracture toughness specimens of KSNP (Korean Standard Nuclear Plant) SA508 Gr. 3 steel to investigate deterministic material inhomogeneity and random inhomogeneity. Fracture toughness tests were carried out for four regions and three test temperatures in the transition region. Fracture toughness evaluation was performed using the bimodal master curve (BMC) approach which is applicable to the inhomogeneous material. The results of the bimodal master curve analyses were compared with that of conventional master curve analyses. As a result, the bimodal master approach considering inhomogeneous materials provides better description of scatter in fracture toughness data than conventional master curve analysis. However, the difference in the $T_0$ determined by two master curve approaches was insignificant.

• Journal of Welding and Joining
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• 제29권1호
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• pp.99-106
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• 2011

Joint strength between a solder ball and a pad on a substrate is one of the major factors which have effects on electronic device reliability. The effort to improve solder joint strength via surface cleaning, heat treatment and solder composition change have been in progress. This paper will discuss the method of solder ball joint strength improvement using LF hydrogen radical cleaning treatment and focus on the effects of surface treatment condition on the solder ball shear strength and interfacial reactions. In the joint without radical cleaning, voids were observed at the interface. However, the specimens cleaned by hydrogen-radical didn't have voids at the interface regardless of cleaning time. The shear strength between the solder ball and the pad was increased over 120%(about 800gf) when compared to that without the radical treatment (680gf) under the same reflow condition. Especially, at the specimen treated for 5minutes, ball shear strength was considerably increased over 150%(1150gf). Through the observation of fracture surface and cross-section microstructure, the increase of joint strength resulted from the change of fracture mode, that is, from the solder ball fracture to IMC/Ni(P) interfacial fracture. The other cases like radical treated specimen for 1, 3, 7, 9min. showed IMC/solder interfacial fracture rather than fracture in the solder ball.

• 지질공학
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• 제17권4호
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• pp.517-523
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• 2007

이 연구에서는 초정지역의 충적층 지하수와 관련된 풍화대분포를 파악하고 단층파쇄대 조사를 위해 복합물리탐사(탄성파굴절법, 전기비저항, 지하투과레이더탐사)를 수행하였다. 탄성파속도 정보로부터 풍화대는 대상지역의 남서부로 갈수록 깊어지는 것으로 나타나는데 기반암까지의 심도 즉 풍화대의 두께는 또한 기존의 시추자료 및 지하수위 자료와 거의 일치한다. 소규모 단층과 관련된 파쇄대 조사에서는 탄성파굴절법, 전기비저항, 레이더탐사 자료를 속도와 비저항 구조를 복합적으로 천부까지 해석하여 단층파쇄대의 지표 경계등을 파악하였다. 복합 지구물리탐사로 정확히 제시된 풍화대와 파쇄대 등에 대한 정보는 충적층 지하수의 분포를 알아내는데 충분히 활용될 수 있을 것으로 보인다.

• 대한기계학회논문집A
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• 제35권9호
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• pp.1119-1129
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• 2011

쇼트피닝(shot-peening) 처리를 한 베어링강의 고사이클 피로거동을 연구하였다. 열처리한 베어링강(JISSUJ2) 시험편과 열처리 후 쇼트피닝 표면가공을 추가한 시험편을 사용해 회전굽힘피로시험을 수행하고 파단 된 시험편의 파면을 분석하였다. 시험편의 피로파괴는 표면 결함에서 비롯된 표면 파괴와, 내부의 비금속개 재물에서 비롯된 내부형 파괴의 두 종류로 발생하였다. 내부 파괴의 경우 비금속 개재물 주변에 어안(fisheye) 모양의 파괴양식이 관찰되었다. 개재물은 표면으로부터의 깊이와 형상에 따라 피로 수명에 큰 영향을 주었다. 쇼트피닝 가공을 한 베어링강은 저사이클 하중영역 및 고사이클 하중영역에서 모두 피로수명이 향상되었으며, 하중이 작아질수록 피로수명의 개선은 더욱 커졌다. 또한 2 모수 와이블(Weibull) 분포를 이용하여 베어링강의 확률-응력-수명 (P-S-N) 곡선을 구하여 신뢰도 높은 피로수명 예측을 하였다.

• Restorative Dentistry and Endodontics
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• 제18권1호
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• pp.1-26
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• 1993

The purpose of this study was to investigate the effect of acid etching on the surface appearance and fracture toughness of five glass ionomer cements. Five kinds of commercially available glass ionomer cements including chemical curing filling type, chemical curing lining type, chemical curing metal reinforced type, light curing tilling type and light curing lining type were used for this study. The specimens for SEM study were fabricated by treating each glass ionomer cement with either visible light curing or self curing after being inserted into a rubber mold (diameter 4mm, depth 1mm). Some of the specimens were etched with 37% phosphoric acid for 0, 15, 30, 60, go seconds, at 5 minutes, 1 hour and 1 day after mixing of powder and liquid. Unetched ones comprised the control group and the others were the experimental groups. The surface texture was examined by using scanning electron microscope at 20 kV. (S-2300, Hitachi Co., Japan). The specimens for fracture toughness were fabricated by curing of each glass ionomer cement previously inserted into a metal mold for the single edge notch specimen according to the ASTME399. They were subjected to a three-point bend test after etching for 0, 30, 60, and 90 seconds at 5 minutes-, 1 hour-and 1 day-lapse after the fabrication of the specimens. The plane strain fracture toughness ($K_{IC}$) was determined by three-point bend test which was conducted with cross-head speed of 0.5 mm/min using Instron universal testing machine (Model No. 1122) following seven days storage of the etched specimens under $37^{\circ}C$, 100% humidity condition. Following conclusions were drawn. 1. In unetched control group, crack was present, but the surface was generally smooth. 2. Deterioration of the surface appearance such as serious dissolving of gel matrix and loss of glass particles occured as the etching time was increased beyond 15 s following Immediate etching of chemical curing type of glass ionomer cements. 3. Etching after 1 h, and 1 d reduced surface damage, 15 s, and 30s etch gave rough surface appearance without loss of glass particle of chemical curing type of glass ionomer cements. 4. Light curing type glass ionomer cement was etched by acid, but there was no difference in surface appearances according to various waiting periods. 5. It was found that the value of plane stram fracture toughness of glass ionomer cements was highest in the light curing filling type as $1.79\;MNm^{-1.5}$ followed by the light curing lining type, chemical curing metal reinforced type, chemical curing filling type and chemical curing lining type. 6. The value of plane stram fracture toughness of the chemical curing lining type glass ionomer cement etched after 5 minutes was lower than those of the cement etched after 1 hour or day or unetched (P < 0.05). 7. Light curing glass ionomer cement showed Irregular fractured surface and chemical curing cement showed smooth fractured surface.

• Restorative Dentistry and Endodontics
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• 제24권1호
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• pp.156-165
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• 1999

The purpose of this study was to evaluate the effect of surface treatments on the shear bond strength between new and old composites. Circular cavities prepared on the center of acrylic resin mold and the prepared cavities were filled with composite resin. They randomly assigned into control group and 8 groups according to the difference in surface treatments of old composites; Control group: no surface treatment, Group 1: surface treated with #120 SiC paper & bonding agent, Group 2: surface treated with #400 SiC paper & bonding agent, Group 3: surface treated with #120 SiC paper, 32% $H_3PO_4$ & bonding agent, Group 4: surface treated with #400 SiC paper, 32% $H_3PO_4$ & bonding agent, Group 5: surface treated with #120 SiC paper, primer & bonding agent, Group 6: surface treated with #400 SiC paper, primer & bonding agent, Group 7: surface treated with #120 SiC paper, 32% $H_3PO_4$, primer & bonding agent, Group 8: surface treated with #400 SiC paper, 32% $H_3PO_4$, primer & bonding agent. New composites were applicated on the old composites of experimental groups. The shear bond strengths for the experimental specimen were measured and the results were analyzed by using one way ANOVA. The observations of surface morphology after SiC paper roughening and debonded surface morphology after shear bond strength test were done by SEM. The results were as follows; 1. Shear bond strengths for specimens roughened with #120 SiC paper matching with the particle size of coarse diamond bur were significantly higher than those for the specimens with #400 SiC paper(P<0.05). By SEM, the surface of the specimens roughened with #120 SiC paper was more irregular than the specimens with #400 SiC paper. 2. Shear bond strengths for specimens treated with 32% $H_3PO_4$ etchant, primer, bonding resin were significantly higher than those for specimens treated with 32% $H_3PO_4$ and bonding resin(P<0.05). 3. Shear bond strengths for the specimens treated with 32% $H_3PO_4$ etchant and bonding resin were significantly higher than those for specimens treated with only bonding resin(P<0.05). There was no remarkable change of surface morphology after 32% $H_3PO_4$ etching. 4. It was possible to observe mixed fracture patterns (the cohesive fracture of old composite and the adhesive fracture between old and new composite) in the specimens roughened with #120 SiC paper, but almost adhesive fracture in the specimens roughened with #400 SiC paper.

• Journal of Welding and Joining
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• 제5권2호
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• pp.53-59
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• 1987

The effect of applied stress, current density and heat-treatment after welding on the time to fracture, fracture behavior was investigated by the method of constant load tensile testing under catholic charging with hydrogen in E.B. welded 250,300 Grade 18% Ni Maraging steel sheet. The main results obtained are as follows: 1. All specimen showed the characteristic delayed failure and the time to fracture showed decreasing tendency with the increase in current density and applied stress. 2. Hydrogen embitterment susceptibility of notched specimen after solution-treatment and aging after welding was more increased than that of aged smooth specimen and as welded specimen. 3. Fracture surface showed a typical intergranular fracture on the border, a dimple pattern in the center of specimen and some quasi-cleavage fracture between the intergranular and the dimple.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2000년도 춘계학술발표대회 논문집
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• pp.20-25
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• 2000

In order to study the impact fracture behavior of brittle materials, a steel-ball-impact experiment was Performed. Five kinds of materials were used in this study : soda-lime glass plates, glass/epoxy prepreg-one layer-bonded and unbonded glass plates, glass/epoxy prepreg-three layers-bonded and unbonded glass plates. Fracture patterns, the maximum stress and absorbed fracture energy were observed according to various impact velocities 40-120m/s. With increasing impact velocity, ring crack, cone crack, radial crack and lateral crack took place in the interior of glass plates. The generation of such cracks was largely reduced with glass/epoxy prepreg coating. Consequently, it is thought that the characteristics of the dynamic Impact fracture behavior could be evaluated using the absorbed fracture energy and the maximum stress measured at the back surface of glass plates.

• 소성∙가공
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• 제3권2호
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• pp.167-177
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• 1994

Most of bulk metal forming processes may be limited by ductile fracture such as surface or internal cracks developing in the workpiece. It is important to identify the conditions within the deforming workpiece which may lead to fracture, and then it is possible to modify the forming processes to produce sound and reliable product. This paper suggests the scheme to simultaneously accomplish prediction of fracture initiation and analysis of deformation in metal forming processes. The Cockcroft-Latham criterion which is successfully applied to a variety of loading situations is used in the present investigation to estimate whether fracture occurs during the deformation process. The numerical predictions and experimental results of two types of metal forming process are compared, axisymmetric extrusion and simple upsetting. The proposed scheme has successfully predicted the fracture initiation found experimentally.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2002년도 추계학술대회 논문집
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• pp.812-815
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• 2002

The shape of K-R curve for an ideally brittle material is flat because the surface energy is an unvaried material property. However, the K-R curve can take on a variety of shapes when nonlinear material behavior accompanies fracture. By the way, a general metallic material is nonlinear, structural steel is such. Therefore, the J-R curve form J-integral value instead of K parameters can be used to evaluate elastic-plastic materials with flaws in terms of ductile fracture that can be significant to design. In this paper, R-curve behaviors form K and J parameter is considered for the precise assessment of fracture analysis, in case of JS-SS400 steels.