• 제목/요약/키워드: sublimation method

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AlN 단결정 성장에 관한 도가니 형태의 의존성에 관한 연구 (A study on the dependance of crucible dimension on AlN single crystal growth)

  • 인경필;강승민
    • 한국결정성장학회지
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    • 제25권1호
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    • pp.1-5
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    • 2015
  • AlN 단결정의 특별한 용도로 이를 개발하기 위한 노력이 전 세계적으로 매우 활발하게 이루어지고 있다. 이러한 AlN을 기반으로 하는 자외선 LED는 생활, 의학, 자동자 등에 유용한 용도로서 살균, 정화, 경화 및 분석 등 분야에 이용된다. 이에 실험을 통해 PVT법으로 카본 도가니를 사용하여 AlN 단결정을 성장시켰으며 실험 중 3가지 형태의 도가니를 이용하여 성장에 미치는 영향을 분석하였으며, 그 온도 조건은 $1900{\sim}2100^{\circ}C$이고 실험 압력으로는 1~200 Torr였다. 그 결과, 높이가 높은 형태의 도가니를 사용할 경우 증발량은 기준 형태보다 증가 하는데 그쳤다. 반면, 넓은 형태의 도가니는 더욱 많은 증발양의 증가를 보였으며, 기준 형태에 비하여 훨씬 안정하다는 것을 알았다. 또한, 제한된 크기의 도가니를 이용한 PVT법에서의 도가니 형태의 변화에 따른 결과는 성장률에 따른 최적 조건, 성장 결정의 품질변화 및 성장 조건 안정성에 영향을 주는 것을 알았다.

터빈 블레이드 말단과 슈라우드 사이의 간극변화에 따른 슈라우드에서의 열/물질전달 특성 (Heat/Mass Transfer Characteristics on Shroud with Turbine Blade Tip Clearances)

  • 이동호;최종현;조형희
    • 대한기계학회논문집B
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    • 제25권3호
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    • pp.414-421
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    • 2001
  • The present study is conducted to investigate the local heat/mass transfer characteristics on the shroud with blade tip clearances. The relative motion between blade and shroud has little influence on the overall heat transfer characteristics, except some local effects. Therefore, the relative motion between the blade and shroud is neglected in this study. A naphthalene sublimation method is employed to determine the detailed local heat/mass transfer coefficients on the surface of the shroud. The tip clearance is changed from 0.66% to 2.85% of the blade chord length. The flow enters the gap between the blade tip and shroud at the pressure side due to the pressure difference. Therefore, the heat/mass transfer characteristics on the shroud are changed significantly from those with endwall. At first, high heat/mass transfer occurs along the profile of blade at the pressure side due to the entrance effect and acceleration of the gap flow. Then, the heat/mass transfer coefficients on the shroud increase along the suction side of the blade because tip leakage vortices are generated and interact with the main flow. The results show that the heat/mass transfer characteristics are changed largely with the gap distance between the tip of turbine blade and the shroud.

새로운 가이드 튜브를 통한 6H-SiC 단결정의 직경 확장에 관한 연구 (The Diameter Expansion of 6H-SiC Single Crystals by the Modification of Inner Guide Tube)

  • 손창현;최정우;이기섭;황현희;최종문;구갑렬;이원재;신병철
    • 한국전기전자재료학회논문지
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    • 제21권9호
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    • pp.795-800
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    • 2008
  • A sublimation method using the SiC seed crystal and SiC powder as the source material is commonly adopted to grow SiC bulk single crystal. However, it has proved to be difficult to achieve the high quality crystal and the process reliability because SiC single crystal should be grown at very high temperature in closed system. The present research was focused to improve SiC crystal quality grown by PVT method through using the new inner guide tube. The new inner guide tube was designed to prevent the enlargement of polycrystalline region into single crystalline region and to enlarge the diameter of SiC single crystal. The 6H-SiC crystals were grown by conventional PVT process. The seed adhered on seed holder and the high purity SiC source materials are placed on opposite side in sealed graphite crucible surrounded by graphite insulation. The SiC bulk growth was conducted around 2300 $^{\circ}C$ of growth temperature and 50 mbar in an argon atmosphere of growth pressure. The axial thermal gradient across the SiC crystal during the growth was estimated in the range of 15${\sim}$20 $^{\circ}C$/cm.

출력장치의 인쇄특성을 고려한 모니텅상의 컬러교정 (A Studyt on the soft-proofing method on Monitor using characteristics of printing device)

  • 송경철;강상훈
    • 한국인쇄학회:학술대회논문집
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    • 한국인쇄학회 2000년도 춘계 학술발표회 논문집
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    • pp.45-55
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    • 2000
  • Recently, as the prepress mainstream is changed to the digital wolkflow, various digital proofing systems such as high price dye sublimation printers and low price ink jet printers are widely used in printing industry. Generally, CRT monitors are also often used as a soft proofing device for hard-copy image output. However, displayed color image on CRT monitor does not match to the actual color printing sheets. Because, the color space of CRT monitor used RGB color space, and it is differ with printing device color space, CMY. Therefore, proper color compensations are needed to match the colors between hard-copy proofs on the printing device and soft copy proofs on the monitor. For the proper compensation, we used LUT and gamut mapping method for color space transformation between device dependent color space and device independent color space, vis a vis. This paper shows the application method and the usefulness of CRT monitor for the soft-copy proofing using the output characteristics of printing device.

스퍼터링 법에 의한 BSCCO 단결정 성장의 부착 계수 향상 (Enhanced sticking coefficient in the BSCCO single crystal grown by the sputtering method)

  • 천민우;양승호;박용필
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.585-586
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    • 2005
  • BSCCO thin films were fabricated by an ion beam sputtering method with an ultra-low growth rate, and sticking coefficients of the respective elements are evaluated. The sticking coefficient of Bi element in BSCCO film formation was observed to show a unique temperature dependence; it was almost a constant value of 0.49 below about $730^{\circ}C$ and decreased linearly over about $730^{\circ}C$. In contrast, Sr and Ca, displayed no such remarkable temperature dependence. This behavior of the sticking coefficient was explained consistently on the basis of the evaporation and sublimation processes of Bi2O3. It is considered that the liquid phase of the bismuth oxide plays an important role in the Bi 2212 phase formation in the co-deposition process.

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공기분사식 제상장치 개발에 관한 실험적 연구 (Experimental Study for Development of Air Eject Defrost Equipment)

  • 한인근;김창영;김재돌;윤정인
    • 대한기계학회논문집B
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    • 제25권3호
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    • pp.277-284
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    • 2001
  • One of the problems in a refrigerator operation is the frost formation on a cold surface of the evaporator. The frost layer is formed by the sublimation of water vapor when the surface temperature is below the freezing point. This frost layer is usually porous and formed on the cold surface of the evaporator. The frost layer on the surface of a evaporator will make side effect such as thermal resistance. However, these important factors have not been used in determining the defrosting period. Therefore, the proper defrosting operation period based on the new defrosting method is very important, and make a comparison between conventional method like electric defrost and new method in compression work, evaporation pressure, evaporation temperature.

컬러교정인쇄에 대한 룩업테이블의 적용방법에 관한 연구 (A Study on the Application Method of Look-up Table to Color Proofing Systems)

  • 송경철;강상훈
    • 한국인쇄학회지
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    • 제18권1호
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    • pp.35-45
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    • 2000
  • Recently, as the prepress mainstream is changed to the digital workflow, various digital proofing systems such as high price dye sublimation printers and low price ink jet printers are widely used in printing industry. However, most of the digital proofing devices have lower resolution than analog proofing systems and differ with actual color presses in the color gamuts. Therefore, proper color compensations are needed for digital color proofing in order to match colors between the proofs and the press sheets. This study shows the application method of Look-up Table to the digital color proofer of Rainbow, the analog proofer of Matchprint-II, and an actual offset press is effective on the color compensations.

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부분 모델을 이용한 접촉하중을 받는 코팅층이 있는 부재의 열적/기계적 응력해석 (Thermo-Mechanica1 Stress Analyses of Part with Coated Layer under Contact Load Using Partial Model)

  • 권영두;김석삼;신세현;추상우
    • Tribology and Lubricants
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    • 제18권3호
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    • pp.228-234
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    • 2002
  • Generally, space structures are subjected to severe situations, such as, sublimation, strong evaporation of lubricants, thermal stresses, high temperature gradients, irradiation, impacts by microscopic meteorites, and other factors. Recent]y, various kinds of coatings are applied to the parts under heavy contact stresses, in order to insure long wear-free lives and/or reduce friction coefficients. In space structures, molybdenum disulfide is using frequently. Moreover TiN, Al$_2$O$_3$, PTFE(Poly Tetra Fluor Ethylene) are introduced recently for space structure. In this part we are going to apply the partial model method, developed in reference[11] to analyze part with coated layer. In referencer[l1], we compute the reasonable size of partial model and aspect ratio. Using these data, we analyze the structures coated with TiN, Al$_2$O$_3$, PTFE under contact load, temperature and crack model . Beside, we consider the stress analysis under time dependent load and transient thermal effect.

컬러인쇄공정에 대한 룩업테이블의 적용방법에 관한 연구 (A Study on the Application Method of Look-up Table to Color Printing Process)

  • 송경철;강상훈
    • 한국인쇄학회:학술대회논문집
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    • 한국인쇄학회 2000년도 추계 학술 발표회 논문집
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    • pp.17-28
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    • 2000
  • Recently, as the prepress mainstream is changed to the digital workflow, various digital proofing systems such as high price dye sublimation printers and low price ink jet printers are widely used in printing industry. However, most of the digital proofing devices have lower resolutions than analog proofing systems and differ with actual color presses in the color gamuts. Therefore, proper color compensations are needed for digital color proofing in order to match color between the proofs and the press sheets. In this paper, we used 3-dimensional look-up table(LUT) and tetrahedral interpolation method for the color space conversion between the device independent color space(CIEXYZ or Lab) and the device dependent color space(CMY) to reduce the color differences between the original copy and digital color proofs and the press sheets.

유기 분자빔 성막법을 이용한 $\alpha$-Sexithieny1 박막의 성장 및 특성 연구 (A study on the growth and characterization of $\alpha$ -Sexithienyl thin films by OMBD(Organic Molecular Beam Deposition) technique)

  • 박용인;박주강;권오관;김영관;최종선;신동병;손병청;강도열
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1996년도 추계학술대회 논문집
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    • pp.187-190
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    • 1996
  • Conducting polymers have band structures similar to those of inorganic semiconductors such as silicon. Several electronic devices have been constructed with conjugated polymers, mainly Schottky diodes and Metal-Insulator-Semiconductor Field-Effect Transistors (MISFET's). Organic semiconductor has been reported as active materials in MISFET's.$^{1.4}$ In our laboratory, $\alpha$-Sexithiencyl ($\alpha$-6T) has been synthesized and purified by sublimation method. In this study, thin films of $\alpha$-Sexithienyl were prepared on various substrates in ultra-high vacuum chamber by vacuum evaporation method, so called OMBD(Organic Molocular Beam Deposition).$^{7.9}$ The $\alpha$-Sexithienyl thin films were deposited with various deposition conditions. The crystalline structure, and molecular orientation of these films have being studied by using UV/Vis. spectroscopy and X-Ray Diffractometry.

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