• Korean Journal of Materials Research
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• v.24 no.1
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• pp.53-59
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• 2014

The corrosion resistance of submerged entry nozzle (SEN) materials were investigated for high-class steel manufacturing. Composite samples were fabricated by mixing $ZrO_2$, $Al_2O_3$, MgO, mullite, spinel, and carbon. The raw materials were mixed with attrition milling, compacted in a uniaxial pressure of 200MPa and calcined at $1000^{\circ}C$ for 3 h in $N_2$ atmosphere. The bulk density and apparent porosity of the calcined samples were measured by the liquid displacement method in water using Archimedes's principle. The corrosion resistance of the samples were measured by cup test with mold powder at $1550^{\circ}C$ for 2 h. The microstructure and elemental analysis of samples were observed by scanning electron microscopy (SEM), energy dispersive spectrum (EDS), and X-ray diffraction pattern (XRD). The XRD result shows that the starting raw materials were crystalline phase. The microstructure of fabricated specimen was investigated before and after corrosion tests at $1000^{\circ}C$ and $1550^{\circ}C$ for 2h. $ZrO_2$-C composite showed good resistance in the slag corrosion test. Among the composite oxide materials, $ZrO_2-Al_2O_3$-C and $ZrO_2$-MgO-C showed better resistance than $ZrO_2$-C in the slag corrosion test. The diameter variation index of $ZrO_2$-C refractory was 16.1 at $1000^{\circ}C$ for 2 h. The diameter variation index of the $ZrO_2-Al_2O_3$-C refractory was larger than that of the $ZrO_2$-C refractory at $1550^{\circ}C$ for 2 h.

• Nuclear Engineering and Technology
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• v.48 no.1
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• pp.164-168
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• 2016

Lean duplex stainless steels with 0.087 wt.% gadolinium (Gd) were inert arc-melted and cast in molds of size $10mm{\times}10mm{\times}20mm$. The micro-hardnesses of the rolling direction (RD), transverse direction (TD) and short transverse (ST) direction were $258.5H_V$, $292.3H_V$, and $314.7H_V$, respectively. A 33% cold rolled specimen had the crystallographic texture that (100) pole was mainly concentrated to the normal direction (ND) and (110) pole was concentrated in the center of ND and RD. The corrosion potential and corrosion rate in artificial seawater and $0.1M\;H_2SO_4$ solution were in the range of $105.6-221.6mV_{SHE}$, $0.59-1.06mA/cm^2$, and $4.75-8.25mV_{SHE}$, $0.69-1.68mA/cm^2$, respectively. The friction coefficient and wear loss of the 0.087 w/o Gd-lean duplex stainless steels in artificial seawater were about 67% and 65% lower than in air, whereas the wear efficiency was 22% higher. The corrosion and wear behaviors of the 0.087 w/o Gd-lean duplex stainless steels significantly depended on the Gd phases.

• Transactions of the Korean Society of Mechanical Engineers
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• v.11 no.3
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• pp.376-385
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• 1987

In this study, the plane stress fracture toughness and Tearing modulus are investigated for various crack ratios using the J integral. To evaluate the J integral and Tearing modulus, both experiments and estimation are used. The thickness of the low carbon steel specimens that is used in the experiments is 3mm. The type of specimen that is considered in the study is center-cracked-tension one. The measurements of crack length are performed by unloading compliance method. In the estimation of crack parameters such as the J integral and load line displacement, the Ramberg and Osgood stress strain law is assumed. Then simple formulas are given for estimating the crack parameters from contained yielding to fully plastic solutions. Obtained results are as follows; (1) When the crack ratio is in the range of 0.500 - 0.701, the plane stress fracture toughness is almost constant regardless of crack ratios. (2) The fracture toughness (J$\_$c/) and Tearing modulus (T) obtained are J$\_$c/=28.51kgf/mm, T=677.7 for base metal, J$\_$c/=31.85kgf/mm, T=742.0 for annealed metal. (3) Simpson's and McCabe's formulas which consider crack growth in estimating J integral are shown more conservative J and lower T than Rice's and Sumpter's. (4) Comparison of the prediction with the actual experimental measurements by Simpson's formula shows good agreement.

• Korean Journal of Materials Research
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• v.25 no.8
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• pp.386-390
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• 2015

Fe-base superalloy powders with $Y_2O_3$ dispersion were prepared by high energy ball milling, followed by spark plasma sintering for consolidation. High-purity elemental powders with different Fe powder sizes of 24 and 50 mm were used for the preparation of $Fe-20Cr-4.5Al-0.5Ti-O.5Y_2O_3$ powder mixtures (wt%). The milling process of the powders was carried out in a horizontal rotary ball mill using a stainless steel vial and balls. The milling times of 1 to 5 h by constant operation (350 rpm, ball-to-powder ratio of 30:1 in weight) or cycle operation (1300 rpm for 4 min and 900 rpm for 1 min, 15:1) were applied. Microstructural observation revealed that the crystalline size of Fe decreased with an increase in milling time by cyclic operation and was about 15 nm after 3 h, forming a FeCr alloy phase. The cyclic operation had an advantage over constant milling in that a smaller-agglomerated structure was obtained. The milled powders were sintered at $1100^{\circ}C$ for 30 min in vacuum. With an increase in milling time, the sintered specimen showed a more homogeneous microstructure. In addition, a homogenous distribution of Y-compound particles in the grain boundary was confirmed by EDX analysis.

• Steel and Composite Structures
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• v.25 no.1
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• pp.79-92
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• 2017

Initial damage to a stud due to corrosion, fatigue, unexpected overloading, a weld defect or other factors could degrade the shear capacity of the stud. Based on typical push-out tests, a FEM model and theoretical formulations were proposed in this study. Six specimens with the same geometric dimensions were tested to investigate the effect of the damage degree and location on the static behavior and shear capacity of stud shear connectors. The test results indicated that a reduction of up to 36.6% and 62.9% of the section area of the shank could result in a dropping rate of 7.9% and 57.2%, respectively, compared to the standard specimen shear capacity. Numerical analysis was performed to simulate the push-out test and validated against test results. A parametrical study was performed to further investigate the damage degree and location on the shear capacity of studs based on the proposed numerical model. It was demonstrated that the shear capacity was not sensitive to the damage degree when the damage section was located at 0.5d, where d is the shank diameter, from the stud root, even if the stud had a significant reduction in area. Finally, a theoretical formula with a reduction factor K was proposed to consider the reduction of the shear capacity due to the presence of initial damage. Calculating K was accomplished in two ways: a linear relationship and a square relationship with the damage degree corresponding to the shear capacity dominated by the section area and the nominal diameter of the damaged stud. This coefficient was applied using Eurocode 4, AASHTO LRFD (2014) and GB50017-2003 (2003) and compared with the test results found in the literature. It was found that the proposed method produced good predictions of the shear capacity of stud shear connectors with initial damage.

• Journal of Sensor Science and Technology
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• v.8 no.3
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• pp.232-238
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• 1999

Single mode fiber optic interferometers using the Fabry-Perot configuration were embedded in a reinforced concrete structure. These interferometers investigated the character of phase shift and strain for internal loads. The 10 mm length of FFPI in the continuous length of single mode fiber (SMF) were produced with two pieces of SMF coated were $TiO_2$ dielectric film utilizing the fusion splicing technique. The fabricated fiber optic Fabry-Perot interferometer(FFPI) and the 6 mm length of steel bar were buried with specimen ($100{\times}100{\times}50\;mm^3$) which was made of concrete structure. The resin protects FFPI and fiber leads from squeezed concrete. Sensors at different point in the structure were multiplexed by TDM (Time Division Multiplexing) method and the deformation to the external loads at each point could be monitored simultaneously. The output signals were proportional to the external loads applied to the structure and the sensitivity of the sensors were $1.03^{\circ}/kg$ and $0.76^{\circ}/kg$ respectively.

• The Journal of the Korea Contents Association
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• v.13 no.9
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• pp.392-399
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• 2013

The purpose of this study is to identify the manufacturing possibility of non-cement mortar using blast furnace slag and alkali accelerator. In this experimental study, the blast furnace slag which is the by-product of the steel industry substitute for cement, and the potassium hydroxide(KOH), calcium hydroxide ($Ca(OH)_2$) and sodium hydroxide(NaOH) as stimulus were added to each specimen. And the analysis on reaction property of non-cement mortar was conducted by measurement such as flexural and compressive strength, XRD, EDS and SEM. From the test results, it can be founded that $SiO_2$ and CaO included in the blast furnace slag are released and make the calcium silicate hydrate like the hydration reaction of the cement. Also, the continued study is need to reduce emission of $CO_2$ because of major content in filed of the building construction.

• Journal of the Korea institute for structural maintenance and inspection
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• v.24 no.3
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• pp.104-111
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• 2020

The purpose of this study is to investigate the flexural behavior and plastic hinge of reinforced concrete-ECC composite beams. Ordinary portland cement was used as a binder, and high volume fly ash was also used to improve the properties of ECC. An ECC designed in this study showed high tensile strain capacity of 3.0%. Three types of beams were manufactured according to the replacement length of concrete with ECC. From the bending tests, it was found that load-bearing capacity as well as ductility of beam increased with an increase in the replacement length of concrete with ECC. Curvature ductility and plastic hinge length of beam were also increased.

• Journal of Welding and Joining
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• v.10 no.3
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• pp.63-72
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• 1992

The joining methods of ceramics to metals which can be expected to obtain high temperature strength are mainly classified into the solid-state diffusion bonding method and the active brazing method. Between these two, the solid-state diffusion bonding method is given attentions as substituting method for active brazing method due to being capable of obtaining higher bonding strength at high temperature and accurate bonding. In this paper, the solid-state diffusion bonding of $Al_{2}$O$_{3}$ ceramics to Ni-Cr-Mo alloy steel (SNCM21) using insert metal was carried out. The insert metal employed in this study was experimentally home-made, Ag-Cu-Ti alloy. Influence of several bonding parameters of $Al_{2}$O$_{3}$SNCM21 joint was quantitatively evaluated by bonding strength test, and microstructural analyses at the interlayer were performed by SEM/EDX. From above experiments, the optimum bonding condition of the solid-state diffusion bonding of $Al_{2}$O$_{3}$/SNCM21 using Ag-Cu-Ti insert metal was determined. Futhermore, high temperature strength and thermal-shock properties of $Al_{2}$O$_{3}$/SNCM21 joint were also examined. The results obtained are as follows. 1. The maximum bonding strength was obtained at the temperature of 95% melting point of insert metal. 2. The high temperature strength of $Al_{2}$O$_{3}$/SNCM21 joint appeared to bemaximum value at test temperature 500.deg.C and the bonding strength with increasingtemperature showed parabolic curve. 3. The strength of thermal-shocked specimens was far deteriorated than those of as-bonded specimens. Especially, water-quenched specimen after heated up to 600.deg. C was directly fractured in quenching.

• Korean Journal of Optics and Photonics
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• v.1 no.1
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• pp.46-51
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• 1990

Laser plasma was generated by a 1GW iodine photodissociation laser ($\lambda$=1.315$\mu\textrm{m}$, E=12.7J) whose output beam was focused on a molybdenum target surface. The experiment was conducted in a vacuum chamber under 1D-sTorr and several tens of laser shooting were necessary for sufficient exposure for the PBS resist of 111m thickness. Aluminium was coated on the top of the resist by 0.1$\mu\textrm{m}$ thickness which acts as an X-ray filter to cut off the visible and the ultraviolet lights. A bio-specimen was put directly on the aluminium coated resist and located at a distance of 3 cm from the X-ray source. The replicas of a steel mesh, spider's web. and a red blood cell were obtained by this technique and were observed by Nomarski microscope and SEM. The limitation of its resolution is determined by the X-ray source size and Fresnel diffraction effect, and its theoretical prediction is well matched with the experimental results. In this experiment, a resolution better than 0.1$\mu\textrm{m}$ could be obtained. ained.