• Title/Summary/Keyword: spray forming

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Development of Spray Thin Film Coating Method using an Air Pressure and Electrostatic Force (공압과 정전기력을 이용한 스프레이 박막 코팅 기술 개발)

  • Kim, Jung Su;Kim, Dong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.6
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    • pp.567-572
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    • 2013
  • In many electro-devices, the vacuum process is used as the manufacturing process. However, the vacuum process has a problem, it is difficult to apply to a continuous process such as a R2R(roll to roll) printing process. In this paper, we propose an ESD (electro static deposition) printing process has been used to apply an organic solar cell of thin film forming. ESD is a method of liquid atomization by electrical forces, an electrostatic atomizer sprays micro-drops from the solution injected into the capillary with electrostatic force generated by electric potential of about several tens kV. The organic solar cell based on a P3HT/PCBM active layer and a PEDOT:PSS electron blocking layer prepared from ESD method shows solar-to-electrical conversion efficiency of 1.42% at AM 1.5G 1sun light illumination, while 1.86% efficiency is observed when the ESD deposition of P3HT/PCBM is performed on a spin-coated PEDOT:PSS layer.

Spray Characteristics of Gas-centered Swirl Coaxial(GCSC) Injector in High Pressure Condition (고압환경에서의 기체-액체 분사기 분무 특성 연구)

  • Kim, Jong-Gyu;Han, Yeoung-Min;Bae, Tae-Won;Choi, Hwan-Seok;Yoon, Young-Bin
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2010.11a
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    • pp.5-8
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    • 2010
  • The GCSC injectors studied in this paper are those applied to the combustion chamber of staged combustion engines. Liquid fuel is injected through tangential holes along the outer wall of the GCSC injector forming a swirling sheet and oxygen rich gas generated by a preburner enters axially through the center orifice of the injector to form a gaseous jet. The spray characteristics of GCSC injectors under ambient/high pressure conditions and the effect of recess on spray characteristics have been examined in this paper. These results are expected to be used as fundamental data to develop of a staged combustion engine.

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fabrication of Ceramic Tape By Ultrasonic Spray (초음파 분무를 이용한 세라믹 테이프의 성형)

  • 윤정한;박양수;심수만;이해원
    • Journal of the Korean Ceramic Society
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    • v.36 no.6
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    • pp.625-631
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    • 1999
  • Ceramic tapes were fabricated by ultrasonically spraying slurries of monodispersed spherical and alumina powders. Effects of slurry compositions on tape forming were investigated. A relatively fast rate of solvent evaporation caused pores and cracks to be formed. A good chemical affinity between solvent and binder gave rise to binder separation resulting in inhomogeneous distribution of binder. Defect-free silica tapes with uniform distribution of particle packing and the binder were obtained from the solvent having a low chemical affinity and a slow evaporation rate and containing appropriate amounts of the binder and the plasticizer. Tape thickness could be controlled by adjusting solids loadings and slurry feed rates. It was possible to fabricate a tape in 15 $\mu\textrm{m}$ thickness from 7 vol% alumina slurry.

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High Temperature Deformation Behavior of Rapid-Solidification Processed Al-18Si Alloy (급냉응고된 과공정 Al-Si합금의 고온변형특성에 관한 연구)

  • 김성일
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2000.04a
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    • pp.183-186
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    • 2000
  • The high temperature deformation behavior of spray-formed Al-19wt%Si-1.87wt%Mg-0.085wt.%Fe alloy was studied by torsion testing in the strain rate range of 0.001-1 sec-1 and in the temperature range of 300-500 $^{\circ}C$. The relationship between stress temperature and strain rate is expressed using the Power law. the behavior of dynamic recrystallization is showed in 300-35$0^{\circ}C$, 1-0.1sec-1 and the behavior of dynamic recovery is showed in 450-50$0^{\circ}C$, 0.01-0.001sec-1 The size of Si particles is mall when the temperature is low and the strain rate is high. The strain rate sensitivity(m) and the apparent activation energy(Q) indicate the dependence on strain rate and temperature for flow stress respectively. The hot ductility is high when m is high and Q is low. The maps of strain rate sensitivity and apparent activation energy suggest the optimum processing conditions.

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A Study on the characteristics of microstructure, hardness and wear of rapidly solidified AI-20Si-5Fe-2Ni materials (급냉응고 AI-20Si-5Fe-2Ni 합금의 조직, 경도 및 마모특성에 관한 연구)

  • 이상용;이정환;이영선;신평우
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1996.10a
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    • pp.157-165
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    • 1996
  • Characteristics of microstructure, hardness and wear of two AI-20Si-5Fe-2Ni materials produced by powder metallurgy and spray forming respectively were studied at temperatures up to 560$^{\circ}C$. Above 300$^{\circ}C$, the microstructure of powder processed alloy became inhomogenous, whereas the spray formed alloy showed homogeneous microstructures. Hardness of both alloys was increased between 300$^{\circ}C$~490$^{\circ}C$ in both alloy. It was interpreted that increase in hardness was mainly related to the formation of stable and fine intermetallic phase from metastable one. It was showed that hoogenity of microstructure in the rapidliy soldified affected directly wear property.

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Evaluation of Friction Shear Factor By the Lubricating Methods in Warm Forging (온간 단조에서 윤활 분사 방법에 따른 마찰 상수값의 평가)

  • 정덕진;김동진;김병민
    • Transactions of Materials Processing
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    • v.10 no.4
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    • pp.319-328
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    • 2001
  • Quantitative evaluation of the tribological conditions at the tool-workpiece interface in metal forming is usually accomplished by the ring compression test. This paper describes an experimental investigation into friction factor under warm forming conditions according to the lubricants and the lubricating methods using the ring compression test. Four different lubricants, two water based graphite and two oil based graphite lubricants, and three different lubricating methods were applied in the experiments. Calibration curves with the friction shear factor were obtained using FEM analysis and verified by the experimental results. The influence of lubricant and lubricating methods on friction are discussed. In the ring compression test, the lower friction factor got to spray the oil based lubricant on die and billet in warm forging temperature.

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Structural Design and Characterization of a Channel-forming Peptide

  • Krittanai, Chartchai;Panyim, Sakol
    • BMB Reports
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    • v.37 no.4
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    • pp.460-465
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    • 2004
  • A 16-residue polypeptide model with the sequence acetyl-YALSLAATLLKEAASL-OH was derived by rational de novo peptide design. The designed sequence consists of amino acid residues with high propensity to adopt an alpha helical conformation, and sequential order was arranged to produce an amphipathic surface. The designed sequence was chemically synthesized using a solid-phase method and the polypeptide was purified by reverse-phase liquid chromatography. Molecular mass analysis by electro-spray ionization mass spectroscopy confirmed the correct designed sequence. Structural characterization by circular dichroism spectroscopy demonstrated that the peptide adopts the expected alpha helical conformation in 50% acetonitrile solution. Liposome binding assay using Small Unilamellar Vesicle (SUV) showed a marked release of entrapped glucose by interaction between the lipid membrane and the tested peptide. The channel-forming activity of the peptide was revealed by a planar lipid bilayer experiment. An analysis of the conducting current at various applied potentials suggested that the peptide forms a cationic ion channel with an intrinsic conductance of 188 pS. These results demonstrate that a simple rational de novo design can be successfully employed to create short peptides with desired structures and functions.

Phytochemical compounds and quality characteristics of spray-dried powders with the blanching condition and selected forming agents from pressed extracts of Ligularia fischeri leaves (블랜칭 처리 및 부형제 종류에 따른 곰취 착즙액 분무건조 분말의 phytochemical 성분 및 품질특성)

  • Kim, Jae-Won;Park, In-Kyung;Youn, Kwang-Sup
    • Food Science and Preservation
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    • v.20 no.5
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    • pp.659-667
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    • 2013
  • This study was performed to determine the effects of the blanching condition (immersion ratio 1:15 (w/v) for 3 min at $95^{\circ}C$, and solution containing 1% sodium chloride) and selected forming agents (dextrin DE=10, dextrin DE=20, ${\beta}$-cyclodextrin; each forming agents added 5%) on the phytochemical compounds and quality characteristics of Ligularia fischeri leaves. The moisture was not affected by the forming agent. The color of a, b and chroma values were low in the blanching treatment groups and were significantly lowest with ${\beta}$-cyclodextrin (CD). The polyphenol and flavonoid contents in the blanching treatment groups were higher than those in the non-blanching-treatment group. The ascorbic acid content was higher in the non-blanching-treatment group and was significantly highest in the group treated with dextrin (DE=10) whereas the blanching treatment groups showed lower dehydroascorbic acid content than the non-blanching-treatment group. The water absorption was higher in the non-blanching-treatment group and was significantly highest in the group treated with CD. The water solubility in the blanching treatment groups treated with dextrin (DE=20) and CD was higher than that in the blanching treatment group treated with DE=10. The total chlorophyll and chlorophyll a and b contents were high in the blanching treatment group treated with CD, and for the total carotenoid contents, the same tendency as that seen with the chlorophyll content was observed. With regard to the particle diameter, those in the blanching treatment groups were lower than that in the non-blanching-treatment group and was significantly lowest in the blanching treatment groups treated with DE=20 and CD. The result of SEM observation showed that the spray-dried powders in blanching treatment groups treated with the DE=20 and CD forming agents had uniform particle distribution.

Fabrication Method of OPV using ESD Spray Coating (ESD 스프레이를 이용한 OPV 제작 기법)

  • Kim, Jungsu;Jo, Jeongdai;Kim, Dongsoo
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.06a
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    • pp.84.2-84.2
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    • 2010
  • PEMS (printed electro-mechanical system) is fabricated by means of various printing technologies. Passive and active components in 2D or 3D such as conducting lines, resistors, capacitors, inductors and TFT, which are printed with functional materials, can be classified in this category. And the issue of PEMS is applied to a R2R process in the manufacturing process. In many electro-devices, the vacuum process is used as the manufacturing process. However, the vacuum process has a problem: it is difficult to apply toa continuous process as a R2R printing process. In this paper, we propose an ESD (electro static deposition) printing process has been used to apply an organic solar cell of thin film forming. ESD is a method of liquid atomization by electrical forces, anelectrostatic atomizer sprays micro-drops from the solution injected into the capillary, with electrostatic force generated by electric potential of about tens of kV. ESD method is usable in the thin film coating process of organic materials and continuous process as a R2R manufacturing process. Therefore, we experiment the thin films forming of PEDOT:PSS layer and Active layer which consist of the P3HT:PCBM. The result of experiment, organic solar cell using ESD thin film coated method is occurred efficiency of about 1.4%. Also, the case of only used to ESD method in the active layer coating is occurred efficiency of about 1.86% as the applying a spin coating in the PEDOT:PSS layer. We can expect that ESD method is possible for continuous process to manufacture in the organic solar cell or OLED device.

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