• Title/Summary/Keyword: specimen condition

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The effect of oxidation heat treatment on porcelain to metal bond strength (도재용착주조관용 비귀금속 합금의 사전 열처리가 도재-금속의 결합 강도에 미치는 효과)

  • Kim, C.Y.;Nam, S.Y.
    • Proceedings of the KOSOMBE Conference
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    • v.1997 no.05
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    • pp.43-46
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    • 1997
  • The interfacial bond strength and microstructural analysis of pre-heat treated porcelain-fused-metal (PFM) were investigated using a mechanical three-point bending tester and scanning electron microscope(SEM). Four kinds of heat treated samples were prepared as follows; A: heating $1200^{\circ}F\rightarrow1600^{\circ}F$, holding 1min, reheating $\rightarrow1850^{\circ}F$, hold 3min under vacuum, B: heating $1200^{\circ}F\rightarrow1600^{\circ}F$ holding 1min, reheating $\rightarrow1850^{\circ}F$ under vacuum condition, C: heating $1200^{\circ}F\rightarrow1600^{\circ}F$, holding 1min, reheating $\rightarrow1850^{\circ}F$, holding 3min in the air, repeat same heat treatment process under vacuum condition, D: heating $1200^{\circ}F\rightarrow1600^{\circ}F$, holding 1min, reheating $\rightarrow1850^{\circ}F$, holding 1min in the air. The three-point bending test results shows that the interfacial bond strength of specimen B and C were higher than that of A and B. The SEM study reveals that Specimen C shows the highest surface density.

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Evaluation on Basic Properties of Crushed Sand Mortar in Freezing-Thawing and Sulfate Attack (동결융해와 황산염의 복합작용을 받는 부순모래 모르타르의 기초 특성 평가)

  • Kim, Myeong-Sik;Baek, Dong-Il;Choi, Kang-Seok
    • Journal of Ocean Engineering and Technology
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    • v.23 no.5
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    • pp.54-60
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    • 2009
  • Exposed to various environments, concrete confronts degradation by a lot of physical and chemical reaction. Though so many experiments and theorizations on the single condition of concrete degradation have been carried out by constant studies, the truth for now is that there are few studies on the compound phenomenon of degradation related with marine environments. Accordingly, this study measured the degree of degradation in the change of external shape, the change of unit weight and compressive strength, ultrasonic velocity test, and the change of length, etc. after exposing the specimen of cement mortar to the environment between 0 cycle and the maximum of 300 cycles under the condition of aquatic curing, freezing and thawing, and compound degradation, using mineral admixture effective for concrete degradation as a binder. The result indicated that the case of adding mineral admixture showed greater resistance than that of using OPC only, and specifically, the specimen with the additive of slag powder and three component system showed very excellent resistance to freezing and thawing, and compound degradation.

A study of Tailored Blank Welding between dissimiliar materials and different thickness sheets by $CO_2$ Laser Beam ($CO_2$ 레이저빔에 의한 이종재질 및 이종두께의 Tailored Blank 용접에 관한 연구)

  • 황창선;김도훈;유병길;이경돈
    • Laser Solutions
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    • v.2 no.3
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    • pp.42-51
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    • 1999
  • This research was conducted as a fundamental study to apply tailored blank welding technique into automotive production process. The materials used in this study were 2.0mm thickness low carbon steel sheets and 1.2mm Zn-coated low carbon steel sheets. To ensure the reproducibility and to consider various factors, experiments were. conducted by applying Taguchi experimental method with 6 factors. Every welding process was repeated 3 times to offset the effect of uncontrolled factors. Elongation and LDH(Limited Dome Height)were measured to evaluate formability of specimens and Optical microscopy, XRD, SEM, and EDS analysis were performed to observe the microstructures and to determine the solidification mode in the weld. The elongation of specimen welded with optimum condition was 83% of base metal, and LDH was 84% of base metal. In case of laser treated specimen where Zn coating was removed, elongation was 85% of base metal, and LDH was 85% of base metal. In fusion zone, phases were consisted of quasi-polygonal ferrite, banitic ferrite, and martensite.

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The Volume Resistivity properties due to the Curing Condition of Silicone Gel for Power Semiconductor (실리콘 젤의 경화조건에 따른 체적고유저항 특성)

  • Song, Byung-Gi;Cho, Kyung-Soon;Shin, Jong-Yeol;Kim, Lee-Doo;Hong, Jin-Woong
    • Proceedings of the KIEE Conference
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    • 1997.11a
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    • pp.270-272
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    • 1997
  • In order to a study on the electrical properties of silicone gel due to the curing condition, the volume resistivity test is researched. For experiment, we have made up several samples of different curing temperature and time such as 1[H], 2[H] at 125[$^{\circ}C$], 150[$^{\circ}C$], 160[$^{\circ}C$], 170[$^{\circ}C$], 180[$^{\circ}C$]. A measurement of volume resistivity using the VMG-1000 highmegohm meter is recorded after 10 minutes when the each voltage, and DC 500[V] and 1000[V] is applied. A coaxial cylindrical liquid electrode to measure volume resistivity of specimen is used, and its geometric capacitance is 2[pF]. As a result of the experiment, the electrical properties of specimen cured at 170[$^{\circ}C$] for 2[H] is superior.

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A Study on the Minimum Scheme of Burr Generation on Working Condition and Specimen Shape for in the Pure Aluminium(A1050) (순알루미늄(A1050)의 가공조건과 시험편 형상에 따른 버어생성의 최소화에 관한 연구)

  • 이광영;서영백;박흥식;전태옥
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.10
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    • pp.34-40
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    • 1998
  • The burr produced on piece part edges in machining operations must be removed for most parts to function effectively. Although considerable cost have been expended in improving deburring methods, little energy has been applied toward minimizing burrs. This study has been carried out to prevent the burrs produced on pure aluminium under various working condition and specimen shape in turning operations. The computer image processing system was used for measurement of size of burr, such as burr length, burr depth and burr area. The size of burr showed a decreasing tendency with the increase of rake angle and side cutting angle but it increased rapidly with the increase of depth of cut and the cutting speed has no effect on size of burrs. The size of burr rapidly decreased with the increase of edge angle and burrs are not occurred if edge angle is over 80$^{\circ}$.

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Development of Fuel Rod Fretting Wear Tester (핵연료봉 프레팅마멸 시험기 개발)

  • 김형규;하재욱;윤경호;강흥석;송기남
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.11a
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    • pp.245-251
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    • 2001
  • A fretting wear tester is developed for experimental study on the fuel fretting problem of light water reactor. The feature of the developed tester is it can simulate the existence of gap between spring and fuel rod as well as different contacting force including the just-contact condition (0 N on the contact). Used are a servo-motor, an eccentric cylinder and lever mechanism for driving system. A spacer grid cell is constituted with four strap segments (each segment has a spring). This fretting wear tester can also be used as a fatigue tester of a spacer grid spring with the frequency of more than 10 Hz. It is required to simulate the frequency of the vibrating fuel rod due to flow-induced vibration in a reactor. In fretting wear test, up to two span-length of a fuel cladding tube can be accommodated. A specimen of cladding tube of one span-length is specially designed, which can be extended for two-span test. For .fatigue test, a device for clamping the spring fixture is installed additionally, Presently, the tester is designed for the condition of air environment and room temperature. The variation of the reciprocal distance is measured to check the stability of input force, which will be exerted to the cladding (for fretting wear. test) and the spring (for fatigue test) specimen.

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Unique local deformations of the superelastic SMA rods during stress-relaxation tests

  • Ashiqur Rahman, Muhammad;Rahman Khan, Mujibur
    • Structural Engineering and Mechanics
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    • v.22 no.5
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    • pp.563-574
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    • 2006
  • This paper studies mechanical behavior of the superelastic shape memory alloy (SMA) rods in terms of local deformations and time via tensile loading-unloading cycles for both ends fixed end constraints. Besides the unique stress induced martensitic transformation (SIMT), SMA's time dependent behavior when it is in mixed-phase condition upon loading and unloading, also need careful attention with a view of investigating the local deformation of the structural elements made of the same material. With this perspective, the so-called stress-relaxation tests have been performed to demonstrate and investigate the local strains-total strains relationships with time, particularly, during the forward SIMT. Some remarkable phenomena have been observed pertaining to SIMT, which are absent in traditional materials and those unique phenomena have been explained qualitatively. For example, at the stopped loading conditions the two ends (fixed end and moving end of the tensile testing machine) were in fixed positions. So that there was no axial overall deformation of the specimen but some notable increase in the axial local deformation was shown by the extensometer placed at the middle of the SMA specimen. It should be noted that this peculiar behavior termed as 'inertia driven SIMT' occurs only when the loading was stopped at mixed phase condition. Besides this relaxation test for the SMA specimens, the same is performed for the mild steel (MS) specimens under similar test conditions. The MS specimens, however, show no unusual increase of local strains during the stress relaxation tests.

Calcined Condition and Characteristic of Cu-Ni-Zn Ferrite Powder Made by Thermal Decomposition of Organic Acid Salt (유기산염 열분해법으로 합성한 Cu-Ni-Zn 페라이트분말의 특성과 하소조건)

  • 정재우
    • Journal of Powder Materials
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    • v.2 no.1
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    • pp.29-35
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    • 1995
  • In this study the calcined condition and characteristic of Cu-Ni-Zn ferrite powder were investigated. The Cu-Ni-Zn ferrite powder has been synthesized by the thermal decomposition of the organic acid salt. This process did not require a strict pH control and provided the uniform composition and fine powder with about 0.3 $\mu\textrm{m}$. The XRD diffraction pattern of this powder showed about 50% spinel phase. The optimum calcination was found to be done at $700^{\circ}C$ for one hour. After the calcination, the amount of spinel increased to 90%. The distribution of the particle size showed bimodal peaks, one was about 0.5 $\mu\textrm{m}$ and the other was about 20 $\mu\textrm{m}$. The large particles of 20 $\mu\textrm{m}$ were the agglomeration of fine Particles. The mean Particle size of the powder was about 0.4 $\mu\textrm{m}$. The powder was compacted under 100 MPa pressure and sintered at 1100~ $1250^{\circ}C$ for one hour in air. The density of ferrites specimen was a function of the sintering temperature. The higher the temperature, the denser the ferrite. The maximum relative density of the sintered ferrite was about 93% at $1250^{\circ}C$. The grain size of sintered specimen at $1200^{\circ}C$ was 5 $\mu\textrm{m}$ and homogeneous.

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A Study of Environment & Bullet-Proof Capability Test Method for KLTV's Transparent Armour (한국형 전술차량 방탄유리 환경 및 방호력 시험 적용 기법 연구)

  • Park, Jinwon;Park, Youngchan;Kim, Seonjin
    • Journal of the Korea Institute of Military Science and Technology
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    • v.21 no.1
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    • pp.69-73
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    • 2018
  • Korean-peacekeeper's transparent armors in Iraq showed delamination, cracking and clouding a decade ago. And there were also similar deterioration recurrences in KLTV during the operational test a few years ago. Also, the differences between operational capability & lab Bullet-proof test condition, and insufficiency of military protection spec resulted in incomplete bullet-proof results. Moreover, although so many ground weapon systems have been developed, there were not secure test & evaluation codes to verify transparent armoured glasses equal to advanced-overseas products. So in this study, first, environmental test codes were established that all tests should be carried out as the application of only one specimen with newly adopted thermal shock test instead of completing each test with different one. Second, protection standards were integrated through the analysis of global developed country's specifications and reinforced as adding to the real mock-up condition if vehicle's glasses are smaller than standard specimen. Hereby, by applying to test-codes which including actual operational & vehicular conditions, the gap between development test and operational environment was minimized.

Piezoelectric properties ofPbTi$O_3$ system ceramics for hydrophone (하이드로폰용 PbTi$O_3$계 세라믹스의 압전특)

  • 유주현;홍재일
    • The Transactions of the Korean Institute of Electrical Engineers
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    • v.44 no.4
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    • pp.479-482
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    • 1995
  • In this study, to improve sintering condition, anisotropic properties ( $k_{t}$/ $k_{p}$) of electromechanical coupling coefficient and piezoelectric constant $d_{h}$ and $g_{h}$, Mn $O_{2}$ impurity was added to the (P $b_{0.76}$C $a_{0.24}$)[( $Co_{1}$2/ $W_{1}$2/)$_{0.04}$ $Ti_{0.96}$] $O_{3}$ ceramics for application to hydrophone devices. Electromechanical coupling coefficients of the specimen with 1.5 [mol%] Mn $O_{2}$ sintered at 1150.deg. C were $k_{t}$=49% and $k_{p}$ = O, which exibited the highest value in piezoelectric anisotropic properties (kt/kp). Without relations with sintering temperature, the highest value of hydrostatic piezoelectric constant $d_{h}$ & $g_{h}$ were shown at the specimen with 1.5 [mol%] Mn $O_{2}$. Accordingly, the best addition amount of Mn $O_{2}$ was 1.5 [mol%] and proper sintering temperature was 1150.deg. C. Hydrostatic piezoelectric constant values of $d_{h}$=64.52[10$^{-12}$ C/N], $g_{h}$=35.92[10$^{-3}$ Vm/N] in the above condition were effectiely extended for hydrophone applications.pplications.ons.

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