• Journal of the Korean Society for Heat Treatment
• /
• v.27 no.2
• /
• pp.72-78
• /
• 2014

Isothermal transformation behavior of a 10% Cr heat resistant steel fabricated by centrifugal casting process was investigated. Normalized specimen at $1100^{\circ}C$ for 1 hour was isothermally annealed at temperature range between $600^{\circ}C$ and $700^{\circ}C$ with various time. The annealed specimen had eutectoid structure which was generated along austenitic grain boundary during isothermal annealing. Areal fraction of eutectoid structure increased up to 25% after holding at $700^{\circ}C$ for 20 hours. It was observed that austenitic matrix was transformed to ferrite structure and fine $M_{23}C_6$ carbides with increase of annealing time. Time-temperature-transformation diagram of the centrifugally cast 10% Cr steel with 0.18 wt% C was plotted based on the results of isothermal transformation behavior.

• Proceedings of the Korean Nuclear Society Conference
• /
• 1996.05c
• /
• pp.79-84
• /
• 1996

Small punch test was performed on CF8 duplex stainless steel aged at 370 and 400$^{\circ}C$ up to 5,000 h to evaluate the degree of the thermal aging embrittlement. At room temperature, the SP load-displacement curve was in a similar shape to those of ferritic steels and had a good reproducibility in spite of two-phase structure. The aging heat treatment resulted in a slight increase of the yield strength. As test temperature was lowered, the SP load showed a sudden drop followed by serrations before the SP specimen was fractured, resulting from the cracking of ferrite phase. The extent of thermal embrittlement was assessed in terms of the SP energy. Aging treatment at higher temperature led to a larger shift in the transition temperature and the corresponding change in the fracture mode. The main cause of the degradation was the embrittlement of ferrite phase. Additionally the phase boundary separation profoundly contributed to the degradation of the specimen aged at 400$^{\circ}C$.

• Journal of the Korean Ceramic Society
• /
• v.28 no.7
• /
• pp.561-567
• /
• 1991

Submicron ${\alpha}-SiC$ powder with $Al_2O_3$ addition was hot-pressed under the controlled heating and pressurizing schedule. $SiO_2$ layer on ${\alpha}-SiC$ powder was effective for the sintering of ${\alpha}-SiC$ powder when $Al_2O_3$ was used as an additive. Applying of pressure under the controlled schedule accelerated the rearrangment of SiC grains, yielding 98% of theoretical density of SiC even at $1900^{\circ}C$. Flexural strength of the specimen containing 2 wt% $Al_2O_3$ was increased as increasing the hot-pressing temperature up to $2050^{\circ}C$ and maximum value was 800 MPa, while the flexural strength of the specimen containing 10 wt% $Al_2O_3$ was decreased as increasing the hot-pressing temperature above $2000^{\circ}C$ due to the formation of continuous grain boundary phase. Fracture toughness of the specimens was in the range of $3.5~4.5\;MNm^{-3/2}$ regardless of the amount of $Al_2O_3$ addition.

• Journal of the Korean Ceramic Society
• /
• v.37 no.2
• /
• pp.152-157
• /
• 2000

Si3N4/SiC nanocomposite ceramics containing 5 wt%dispersed SiC particles were prepared by gas-pressure-sintering at 200$0^{\circ}C$ under nitrogen atmosphere. SiC particles with average sizes of 0.2 and 0.5${\mu}{\textrm}{m}$ were used, and the effect of the SiC particle size on the microstructure was investigated. The addition of SiC particles effectively suppressed the growth of the Si3N4 matrix grains. The effect of grain growth inhibition was higher in the nanocomposites dispersed with fine SiC. SiC particles were dispersed uniformly inside Si3N4 matrix grains and on grain boundaries. When the fine SiC particles were added, large fraction of the SiC particles was trapped inside the grains. On the other hand, when the large SiC particles were added, most of the SiC particles were located on grain boundaries. Typically, the fraction of SiC particles located at grain boundaries was higher in the specimen prepared from $\beta$-Si3N4 than in the specimen prepared from $\alpha$-Si3N4.

• Korean Journal of Materials Research
• /
• v.26 no.11
• /
• pp.583-589
• /
• 2016

In this study, recrystallization behaviors in the two-phase (${\alpha}+{\gamma}$) region of micro-alloyed steels such as Base, Nb, TiNbV and CAlN were investigated in terms of flow stress, microstructure and associated grain boundary characteristics. The flow stress of all specimens reached peak stress and gradually decreased, which means that recrystallization or recovery of proeutectoid deformed ferrite and recovery or transformation to ferrite of deformed austenite occurred by thermal activation. The precipitation of carbide or nitride via the addition of micro-alloying elements, because it reduced prior austenite grain size upon austenitization, promoted transformation of austenite to ferrite and increased flow stress. The strain-induced precipitation under deformation in the two-phase region, on the other hand, increased the flow stress when the micro-alloying elements were dissolved during austenitization. The recrystallization of the Nb specimen was more effectively retarded than that of the TiNbV specimen during deformation in the two-phase region.

• Journal of the Korean Society for Heat Treatment
• /
• v.9 no.3
• /
• pp.212-218
• /
• 1996

To clarify the influence of precipitation microstructure and inclusion on the monotonic tensile fracture behaviors in 2090 alloy aged at $180^{\circ}C$, the detailed measurement of hardness, tensile strength, elongation and the observation of scanning electron micrography, transmision electron micrography have been carried out. The transgranular shear ductile fracture has been observed in specimen quenched after solution treatment at $500^{\circ}C$ for 45min. While the under-aged specimen was fractured in both transgranular shear ductile and intergranular fracture mode, the fracture mode of peak-aged and over-aged alloy was predominantly intergranular fracture. The fracture behavior of each ageing condition was influenced by the change of precipitation microstructural features. In the case of peak-aged and over-aged alloys, the coarse and heterogeneous slip band caused by both shearable nature of the ${\delta}^{\prime}(Al_3Li)$ precipitates and PFZ along the high angle grain boundary aid the localization of deformation, resulting in low energy intergranular fracture. It was also estimated that the fractured T-type intermetallic phases (inclusion) and the equilibrium ${\delta}$(AlLi) phases which were formed at grain boundaries palyed an important role in promoting intergranular fracture mode.

• Journal of the Korean Society for Heat Treatment
• /
• v.19 no.3
• /
• pp.163-169
• /
• 2006

Fretting is a kind of surface degradation mechanism observed in mechanical components and structures. The fretting damage decreases into 50-70% of the plain fatigue strength. The connecting rod for automobile has been used in special environments and various loading conditions. Failure of connecting rod in automotive engine may cause catastrophic situation. In this study, we investigated the fatigue characteristic of connecting rod material for an automobile. Fatigue life is defined as the number of cyclic stress to failure by regular cyclic stress. Fatigue life of C70S6 specimen was obtained from 134,000 to 147,000 cycles. Fatigue limit showed 432MPa by normal fatigue test. The other hands, it was 96MPa in the case of fretting fatigue test. It was extremely lower than that of a normal fatigue test. From observation of fracture surface, it was confirmed that the fatigue crack was initiated at the boundary of a specimen and bridge pad.

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2007.04a
• /
• pp.129-132
• /
• 2007

In this study, for the establishment of the performance evaluation methods of repair material and method for reinforced concrete structure and the quality control standards of durability recovery method, the quantitative exposure data by exposure experiment under the coastal and normal atmosphere environment is accumulated and analyzed. Investigating and evaluating the result of exposure experiment during 54 months of exposure age under the coastal and normal atmosphere environment, Micro crack, swelling and spatting of surface coating material, crack of repair boundary parts and the great potential difference between repair part and non-repair part were somewhat generated. And the result shown that exposure specimen of coastal environment had lower electrode potential than exposure specimen of normal atmosphere environment.

• Korean Journal of Materials Research
• /
• v.10 no.11
• /
• pp.725-731
• /
• 2000

Recrystallization behaviors of cold-worked and $\beta$-quenched Zr-Zn alloys were investigated by the microhardness tests and microscopic examinations. The recrystallization of the $\beta$-quenched alloys was retarded in comparison with that of the cold-worked alloys, suggesting that the stored energy of the cold-worked alloys is larger than that of the $\beta$-quenched alloys. Although initial hardness for the cold-worked and the $\beta$-quenched specimens had an equal value, the recrystallization behaviors were observed to be quite different. Based on the transmission electron microscope(TEM) studies, it was suggested that the recrystallization of the cold-worked specimen would have occurred by subgrain coalescence while that of $\beta$-quenched specimen by strain-induced grain boundary migration.

• Smart Structures and Systems
• /
• v.22 no.6
• /
• pp.663-673
• /
• 2018

In this study, the effect of particle size on the cracks propagation and coalescence or cracking pattern of the edge notched disc specimens are investigated. Firstly, calibration of PFC3D was performed using Brazilian experimental test output. Then micro parameters were used to build edge notched disc specimen. The horizontal wall of the assembly is let to move downward with a standard low speed of 0.016 m/s. The numerical results show that the tensile cracks are dominant failure pattern for the modeled discs. These tensile cracks initiate from the pre-existing notch tip and propagate parallel to the loading direction then interact with the upper boundary of the modeled specimen. As the size of the balls (ball diameter) decrease the number of tensile cracks increase. The tensile fracture toughness of the samples also decreases as the particle size increases. Understanding the crack propagation and crack coalescence phenomena in brittle materials such as concretes and rocks is of paramount importance in the stability analyses for engineering structures such as rock slopes, underground structures and tunneling.