• 한국자동차공학회논문집
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• 제3권1호
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• pp.1-12
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• 1995

Isothermal and thermal-mechanical fatigue characteristics of 12Cr heat resisting steel used for high temperature applications were investigated including hold time effects. Isothermal low cycle fatigue test at $600^{\circ}C$ and in-phase, out-of-phase thermal-mechanical fatigue test at 350 to $600^{\circ}C$ were conducted using smooth cylindrical hollow specimen under strain-control with total strain ranges from 0.006 to 0.015. Regardless of thermal-mechanical and isothermal fatigue tests, cyclic softening behavior was observed and much more pronounced in the thermal-mechanical fatigue tests with hold times due to the stress relaxation during the hold time. The phase difference between temperature and strain in thermal-mechanical fatigue tests resulted in significantly shorter fatigue life for out-of-phase compared to in-phase. The differences in fatigue lives were dependent upon the magnitudes of plastic strain ranges and mean stresses. During the hold time in the strain-controlled fatigue tests, the increase in the plastic strain range and the stress relaxation were observed. It appeared that the increase in plastic strain range per cycle and the introduction of creep damage made important contributions to the reduction of thermal-mechanical fatigue life with hold time, and the life reduction tendency was more remarkable in the in-phase than in the out-of-phase thermal-mechanical fatigue. Isothermal fatigue tests performed under the combination of fast and slow strain rates at $600^{\circ}C$ showed that the fatigue life decreased as the strain rate and frequency decreased,especially for the low strain ranges.

• Journal of Welding and Joining
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• 제16권6호
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• pp.35-43
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• 1998

In this paper, the fracture toughness evaluation of the various microstructures such as HAZ, F.L and W.M in weldment of TMCP steel which has the softening zone owing to high heat input welding was carried out by using of the small punch(SP) test. In addition, the fracture toughness with the specimen orientation of rolled TMCP steel was investigated by means of SP test and the crack opening displacement (COD) test and then was compared with that of conventional SM50YB steel. From the results of SP test for TMCP steel, it could be seen that the SP energy transition curves of three different orientation were shifted to higher temperature side in order of S, T and L. But the {TEX}$DBTT_{SP}${/TEX} of each orientation specimen did not show a lot of differences and were quite lower than those of conventional SM50YB steel. The mechanical properties of HAZ structure in weldment of TMCP steel such as hardness, SP energy at room temperature and -196$^{\circ}C$ and the upper shelf energy of SP energy transition curve were lower than those of base metal due to softening. The {TEX}$DBTT_{SP}${/TEX} of each microstructure in weldment of TMCP steel increased in order of HAZ, F.L and W.M against base metal, but all microstructures showed a quite lower {TEX}$DBTT_{SP}${/TEX} than those of SM50YB steel.

• 한국응용과학기술학회지
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• 제14권1호
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• pp.77-87
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• 1997

PFO(pyrolized fuel oil) and $C_{10}^{+}$ oil, which are the residual heavy oils form a NCC(naphtha cracking center), were heat-treated to produce the precursor-pitch for carbon materials. After PFO was initially distilled near $300^{\circ}C$ to separate the volatile matters recovering as high-quality fuel oil, the residuum of nonvolatile precursor-pitch was then thermally pyrolized in the temperature ranges from $350^{\circ}C$ to $450^{\circ}C$. Spinnable isotropic pitch with the softening point of $200^{\circ}C$ and the toluene insolubles of 36wt% was obtained at $365^{\circ}C$, and then was successfully spun through a spinneret(0.5mm diameter). After spinning, an isotropic carbon fiber of $25{\mu}m$ diameter was obtained via oxidation and craboniation procedures. Mesophase spherules began to be observed from the product pitch pyrolized at $400^{\circ}C$, and bulk mesophase with a flow texture was observed above $420^{\circ}C$. In the case of $C_{10}^{+}$ was the feed was polymerized in the presence $H_2SO_4$ at room temperature to increase the molecular weight and then heat-treated gradually up to $200{\sim}250^{\circ}C$. The products obtained with the softening point of $80{\sim}190^{\circ}C$ were carbonized at 500 and $1000^{\circ}C$ to examine the morphology.

• 대한기계학회논문집
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• 제18권5호
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• pp.1192-1202
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• 1994

Fatigue behavior and life prediction were presented for thermal-mechanical and isothermal low cycle fatigue of 12Cr forged steel used for high temperature applications. In-phase and out-of-phase thermal-mechanical fatigue test at 350 to 600.deg. C and isothermal low cycle fatigue test at 600.deg. C were conducted using smooth cylindrical hollow specimen under strain-control with total strain ranges from 0.006 to 0.015. Cyclic softening behavior was observed regardless of thermal-mechanical and isothermal fatigue tests. The phase difference between temperature and strain in thermal-mechanical fatigue resulted in significantly shorter fatigue life for out-of-phase than for in-phase. The difference in fatigue lives was dependent upon the magnitudes of inelastic strain ranges and mean stresses. Increase in inelastic strain range showed a tendency of intergranular cracking and decrease in fatigue life, especially for out-of-phase thermal-mechanical fatigue. Thermal-mechanical fatigue life prediction was made by partitioning the strain ranges of the hysteresis loops and the results of isothermal low cycle fatigue tests which were performed under the combination of slow and fast strain rates. Predicted fatigue lives for out-of-phase using the strain range partitioning method showed an excellent agreement with the actual out-of-phase thermal-mechanical fatigue lives within a factor of 1.5. Conventional strain range partitioning method exhibited a poor accuracy in the prediction of in-phase thermal-mechanical fatigue lives, which was quite improved conservatively by a proposed strain range partitioning method.

• 한국식품저장유통학회지
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• 제24권6호
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• pp.727-733
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• 2017

상온($25^{\circ}C$)과 저온($-1^{\circ}C$)에서 modified atmosphere packaging(MAP)를 이용한 '상감둥시' 감의 탈삽처리를 통하여 각 온도에서 PE 필름의 적정 두께를 구명하고자 하였다. 60(상온에서만 사용), 80, 100, 115, $130{\mu}m$ 두께의 PE 필름을 이용하여 낱개 진공포장 후 각각 상온과 저온에서 탈삽하였다. 상온에서 탈삽은 필름 두께가 두꺼울수록 속도가 빠른 경향이었으나 모든 처리구에서 두께에 관계없이 5일 만에 식용이 가능한 상태로 탈삽되었다. 경도는 모든 처리구에서 비교적 높게 유지되었다. 과육갈변(top flesh browning)과 부패는 20일에 발생되었으며 과피흑변(peel blackening)과 과정부연화(style-end softening)는 적정 두께에서 거의 문제 되지 않았다. 상온 MAP 탈삽의 적정 PE 필름 두께는 $80-100{\mu}m$로, 이 두께에서 5일만에 탈삽되어 10일까지 상품성을 유지한 유통이 가능한 것으로 판단되었다. 저온에서의 탈삽도 필름 두께가 두꺼울수록 속도가 빨랐으며 50일경에 두께에 관계없이 완전히 탈삽되었다. 경도는 필름 두께에 따른 큰 차이는 없었으나 두꺼울수록 높은 경향을 보였다. 과육갈변과 부패는 필름 두께와 관계없이 모든 처리구에서 90일까지 발생되지 않았다. 과피흑변과 과정부연화는 90일에 발생되었으며 115와 $130{\mu}m$ 두께에서 이취가 발생되었다. 저온 MAP 탈삽의 적정 PE 필름 두께는 $80-100{\mu}m$로, 이 두께에서 50일만에 탈삽되어 80일까지 상품성을 유지한 유통이 가능한 것으로 판단되었다

• 분석과학
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• 제9권2호
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• pp.179-191
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• 1996

초내열 718 합금의 고온 변형 거동을 이해하기 위하여 rotating grade의 718 합금을 이용하여 온도 $927{\sim}1066^{\circ}C$, 변형속도 $5{\times}10^{-4}{\sim}5{\times}10^0sec^{-1}$ 범위에서 진변형량 0.7까지 압축실험을 수행하였다. 최대 유동 응력은 변형 속도가 증가하고 시험 온도가 감소함에 따라 증가하였다. 변형 속도 $5{\times}10^{-1}sec^{-1}$을 제외한 대부분의 설험 조건에서 가공 연화현상이 관찰되었다. 가공 연화는 저온, 고변형 속도에서는 주로 동적 회복 및 변형 쌍정에 의해 일어나는 반면 고온, 저변형 속도 조건에서는 동적 재결정에 의해 발생하였으며 $5{\times}10^{-1}sec^{-1}$의 변형 속도 조건에서는 동적 재결정된 결정 입자들의 재가공 경화에 의해 가동 경화현상이 나타났다. 변형 속도 감도(m)는 변형 속도가 낮은 경우에는 0.3 정도로서 주로 동적 재결정에 의해 변형 거동이 나타남을 반영하였으며 고변형 속도에서는 0.1 정도로서 동적 회복과 변형 쌍정의 발생으로 718 합금의 변형이 이루어짐을 알 수 있었다.

• 한국수산과학회지
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• 제51권5호
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• pp.499-509
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• 2018

This study optimized the bone-softening and fishy odor-reducing process for mackerel Scomber japonicus products using response surface methodology (RSM). The RSM showed that the optimum concentrations of doenjang and citric acid for reducing the fishy odor in bone-softened mackerel were 11.8% and 0.04%, respectively, and the optimum immersion time was 52.2 min. The estimated overall acceptance, salinity, and acidity of the products under these optimum conditions were 7.7 points, 1.1%, and 202.6 mg/100 g, respectively, which were similar to the actual measured values of $7.6{\pm}1.2$ points, $1.0{\pm}0.1%$ and $203.2{\pm}3.8mg/100g$. Moreover, the heating temperature and time for bone-softening based on RSM were $107.3^{\circ}C$ and 4.4 h, respectively. The estimated hardness and proportion of skin removed from the product under the optimal conditions were $161.5g/cm^2$ and 0.09%, respectively, which were also similar to the actual measured values of $171.1{\pm}12.6g/cm^2$ and $0.10{\pm}0.02%$. The optimum bone-softening and fishy odor-reducing process for mackerel consisted of the following steps: thawing (${\leq}10^{\circ}C$, 8 h), filleting, washing/dewatering, immersing in an 11.8% doenjang -0.04% citric acid solution for 52 min, washing/dewatering, heating ($107.3^{\circ}C$, 4.4 h), freezing, depanning, internal and external packaging, and X-ray detection treatment.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2002년도 춘계학술발표대회 논문집
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• pp.69-72
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• 2002

The high temperature deformation behavior of SiCp/2124Al composite and 2124Al alloy was investigated by hot compression test in a temperature ranged $400~475^{\circ}C$ over a strain rate ranged $10^{-3}~1s^{-1}$. The billets of 2124Al alloy and SiCp/2124Al composite were fabricated by vacuum hot pressing process. The stress-strain curve during high temperature deformation exhibited a peak stress, and then the flow stress decreased gradually into a steady state stress with increasing the strain. It was found that the flow-softening behavior was attributed to the dynamic recovery, local dynamic recrystallization and dynamic precipitation during the deformation. The precipitation phases were identified as S' and S by TEM diffraction pattern. Base on the TEM inspection, the relationship between the Z-H parameter and subgrain size was found based on the experiment data. The dependence of flow stress on temperature and strain rate could be formulated well by a hyperbolic-sinusoidal relationship using the Zener-Hollomon parameter.

• 한국표면공학회지
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• 제16권1호
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• pp.3-9
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• 1983

The change of the hardness and yield strength depending upon the electrolysis conditions was investigated for Watts and bright nickel electrodeposits. The hardness of Watts nickel electrodeposits decreased with increasing current density in the range of 1-15A/Am2, while it increased with increasing bath temperature. The hardness of bright nickel deposits increased noticebly in comparison with that of Watts nickel electro-deposits. The hardness and the yield strength of the bright nickel electrodeposits increased considerably with decreasing current density and the highest value was obtained at the lowest current density (1A/dm2), while they decreased noticebly at the bath temperature of 80$^{\circ}C$ in comparison with that of 40-60$^{\circ}C$. The change of the hardness and the yield strength of bright nickel electrodeposits depending upon the electrolysis conditions could be mainly attributed to the variation of organic additives codeposited in the electrodeposits. The recrystallizatioin temperature(50% softening temperature) of the Wattss and the bright nickel electro-deposits was 520-280$^{\circ}C$ and 350-410$^{\circ}C$ respectively and then the recystallization temperature of bright nickel deposits was lower than that of the Watts nickel electrodeposits.

• Carbon letters
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• 제2권3_4호
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• pp.182-191
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• 2001

Quinoline insoluble formed by the heat treatment was hot-pressed near its softening point. The green body was stabilized in the temperature range of $300{\sim}400^{\circ}C$ and subsequently carbonized below $1300^{\circ}C$ in an argon atmosphere. The behaviors of QI formation was examined with varying the heat treatment temperature and the lapse of time of the sample carbonized at various temperatures. And the mechanical property, corrosion resistance, and friction behavior were also measured optimum content of mesophase pitch ensured a dense structure and high $LC_{(002)}$ value, which resulted in high mechanical properties, good corrosion resistance, and low-stable friction behavior.