• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.11a
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• pp.181-181
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• 2009

전자부품용 Pb-free sealing frit의 열팽창계수를 기판에 matching 시키기 위하여 음의 열팽창계수를 가지고 있는 $\beta$-Eucryptite, $\beta$-Spodumene를 합성하여 filler로 첨가하였다. 합성된 filler는 저온소성용 유리프리트의 높은 열팽창계수를 조절하기 용이하고, 유리프리트와 복합화 하여 소성하면 낮은 열팽창계수로 인한 우수한 열충격 저항성을 갖는다. Filler로써 $\beta$-Eucryptite, $\beta$-Spodumene의 결정성을 향상시키기 위해 $1250^{\circ}C$에서 5 시간 동안 유지하는 합성공정을 3회 반복 진행한 후 XRD를 사용하여 결정성을 분석하였고, TMA를 이용하여 filler 첨가량에 따른 유리프리트의 열팽장계수의 변화를 측정하였다. 또한, filler 입도와 함량에 따른 melting 특성을 분석하기 위해 Pill test를 진행하였으며, soda-lime glass 기판과의 접합면을 SEM을 사용하여 관찰하였다.

• Proceedings of the Optical Society of Korea Conference
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• 2002.07a
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• pp.42-43
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• 2002

고상 소결법으로 715iO$_2$＋11$Na_2$O＋10CaO＋3Er$_2$O$_3$＋5Yb$_2$O$_3$(all wt%) 조성의 스퍼터용 유리 타겟을 제조하여, RF 마그네트론 스퍼터에 의해 희토류 원소가 첨가된 광증폭기용 다성분계 sodium calcium silicate 유리박막을 제조하였다. 최적의 공정조건을 얻기 위해 RF-power, 공정압력, 기판온도를 변화시키면서 박막을 제조하여 RF-power 150W, 공정압력 4mtorr, 기판온도 50$0^{\circ}C$, 타겟-기판 거리 6cm에서 타겟의 손상이 심하지 않으면서, 1.4$mu extrm{m}$/h의 최고 증착율을 가지는 양질의 박막을 제조하였다. (중략)

• Journal of the Korean institute of surface engineering
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• v.33 no.2
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• pp.87-92
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• 2000

Transparent and electrical conducting tin oxide thin films were fabricated on soda lime silicate glass by thermal chemical vapour deposition technique. Thin films were deposition from mixtures of tetramethyltin (TMT) as a precursor, oxygen or oxygen containing ozone as an oxidant and 1,1,1,2-tetrafluoroethane as a doping material. Electrical properties of fabricated tin oxide films were changed depending on substrate temperature, and the amount of dopant. Resistivity of tin oxide films was reduced by doping fluorine or heat treatment. Thin films can be optimized at TMT flow rate of 8sccm, oxygen flow rate of 150sccm, 1,1,1,2-tetrafluoroethane floe rate of 300sccm and substrate temperature $380^{\circ}C$. In this conditions, the lowest resistivity of tin oxide films were $9$\times$10^{-4}$ $\Omega$cm.

• Journal of the Korean Ceramic Society
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• v.27 no.1
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• pp.67-73
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• 1990

The behavior of optical properties of ion exchanged glasses was investigated inthis study. The used glasses were soda-lime-silica glasses that were produced by float process. The coloring effect by Ag colloids is measrued by spectral transmittance, color coordinates, dominant wavelength and excitation purity resulting from silver ions exchange of glasses immersed into the mixed molten salt with AgNO3. Ion exchange coloring of glasses made it possible to obtain glasses with a range from yellow to brown, and transmittance was decreased with increasing the amount of Ag colloids which reduced from Ag+ions. Also, obtain from yellow to reddish brown with increasing purity by reheating treatment in air for ion exchanged glasses. The size of Ag colloids are 0.02~0.1${\mu}{\textrm}{m}$ with ion exchange conditions.

• Journal of the Korean Ceramic Society
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• v.24 no.4
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• pp.335-342
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• 1987

There were several numbers of studies on chemically strengthening glass. Most of them were strengthened in molten salt bath below transformation range of glass. Apart from them, this study used solution hydration technique by Autoclave. After determining proper concentration of AgNO3 salt solution, experimental condition varied from 4hrs to 16hrs at relatively low temperature (180, 200, 220$^{\circ}C$). The results showed that the Soda-Lime-Silica glass could be strengthened by diffusion mechanism without influence of water above 15% salt solution. Because of Ag+ ion penetration in glass surface, yellow color appeared and decreased transmittance at visible range. Modulus of rupture was increased with the amount of exchange and brittleness was decreased.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.04a
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• pp.195-198
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• 2005

The role of elastic/plastic mismatch on the contact crack initiation is investigated for designing desirable surface-coated asymmetric layered composites. Various layered composites such as $Si_3N_4$ ceramics on $Si_3N_4+BN$ composite, soda-lime glass on various substrates with different elastic modulus for the analysis. Spherical indentation is conducted for producing contact cracks from the surface or interface between the coating and the substrate layer. A finite element analysis of the stress fields in the loaded layer composites enables a direct correlation between the damage patterns and the stress distributions. Implications of these conclusions concerning the design of asymmetric layered composites indicate that the elastic modulus mismatch is one of the important parameter for designing layered composite to prevent the initiation of contact cracks.

• Transactions of the Korean Society of Mechanical Engineers
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• v.14 no.1
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• pp.130-137
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• 1990

Thermal shock stress intensity factor for an edge-cracked plate subjected to thermal shock is obtained from Bueckner's weight function method. It is shown that thermal shock stress intensity factor has maximum values with variation of time and crack length and that there is most dangerous crack length. By comparing thermal shock stress intensity factor with fracture toughness, the fracture time and critical temperature difference due to thermal shock are determined theoretically. Under constant thermal shock temperature difference, and increase of crack length is shown to increase fracture time. The theoretical fracture time is compared with experimental value measured by acoustic emission method with soda lime glass.

• Journal of the Korean Vacuum Society
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• v.4 no.1
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• pp.32-39
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• 1995

SnO2/AI/Ag/AI/SnO2층 구조로 이루어진 열처리 가능한 열선반사막을 직류 스퍼터링법에 의해 soda-lime silicate 유리위에 형성시켰다. 이 코팅유리를 $650^{\circ}C$에서 열처리하면 가시광선 투과율 85%이상, plasma wavelength 970nm 이하를 얻을 수 있었다. 따라서 이 구조의 막은 유리 곡가공에 견디는 열적 안정성을 나타내었으며, 코팅유리의 열처리에 따른 전기적 특성 및 열적 안정성은 각각 Ag와 AI층의 두께에 의존하였다.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.11a
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• pp.122-122
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• 2003

In recent years, there has been increasing interest in quasi one-dimensional nanostructural systems, because of their numerous potential applications in various areas, such as materials sciences, electronics, optics, magnetism and energy storage. Specifically, zinc oxide (ZnO) is recognized as one of the most promising oxide semiconductor materials, because of its good optical, electrical, and piezoelectrical properties. The ZnO nanorods were synthesized using vapor-solid (VS) mechanism on soda lime glass substrate without the presence of metal catalyst. ZnO nanorods were prepared thermal evaporation of a Zn powder at 500. As-fabricated ZnO nanorods had an average diameter and length of 40nm and 3$\mu\textrm{m}$. Transmission electron microscopy revealed that the ZnO nanorods were single crystalline with the growth direction perpendicular to the (101) lattice plane. The influences of reaction time on the formation of the ZnO nanorods were investigated. The Photoluminescence measurements showed that the ZnO nanorods had a strong ultraviolet emission at around 380nm and a green emission at around 500nm.

• Journal of the Korean Ceramic Society
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• v.31 no.9
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• pp.957-968
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• 1994

Manufacturing process of porous glass by the filler method was studied. Commercial soda-lime-silicate glass powder was mixed with inorganic salt as the filler such as KCl, K2SO4, Na2SO4. Sintering shrinkages of mixed powders with the variation of sintering temperature were compared, and the effects of the fillers to shrinkages of mixed powder were increased in the order of Na2SO4${\mu}{\textrm}{m}$ of pore diameter were manufactured when the filler sizes 100~200 ${\mu}{\textrm}{m}$. The open pore volume of porous glass is determined by the quantity of filler and porous glasses having open pore volume between 30 and 70 vol% are available. Available sintering temperature range for preparation of porous glass is from the softening temperature of the glass powder to eutectic melting temperature of DTA curve of mixed powder.