• Title/Summary/Keyword: small grain

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A Study on The Grain Boundary State of ${\alpha}-Fe_2O_3$ Thermistor by Frequency Properties (주파수 특성에 의한 ${\alpha}-Fe_2O_3$ Thermistor의 계면준위 해석)

  • Hong, H.K.;Kang, H.B.;Kim, B.H.;Choi, B.G.;Sung, Y.K.
    • Proceedings of the KIEE Conference
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    • 1990.07a
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    • pp.227-230
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    • 1990
  • The addition of titanium has come to produce an increase in the conductivity of ${\alpha}-Fe_2O_3$ and has been shown NTC ( negative temperature coefficient ) characteristics. Titanium enters the ${\alpha}-Fe_2O_3$ lattice substitutionally as $Ti^{4+}$,thus producing an $Fe^{2+}$ and maintaining the average charge per cation at three. Thus the $Fe^{2+}$ acts as a donor center with respect to the surrounding $Fe^{3+}$ ions. The sintering temperature, compacting pressure and sintering tire have an effect on the electrical properties. C-V and other properties have been measured on polycrystalline samples of ${\alpha}-Fe_2O_3$ containing small deviations from stoichiometry and small amounts of added Titanium. This measurment was made in the course of an investigation of the NTC mechanism in oxides whose cations have a partially filled d-level. C-V and frequency properties have been applied to the measurement of the trap barrier properties at the grain boundary. The double Schottky barrier at the grain boundary is the major cause of the NTC mechanism in NTC thermistor of ${\alpha}-Fe_2O_3$ containing N-type impurity.

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Grain Growth Revealed by Multi-wavelength Analysis of Non-axisymmetric Substructures in the Protostellar Disk WL 17

  • Han, Ilseung;Kwon, Woojin;Aso, Yusuke
    • The Bulletin of The Korean Astronomical Society
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    • v.45 no.1
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    • pp.59.2-59.2
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    • 2020
  • Disks around protostars are the birthplace of planets. The first step toward planet formation is grain growth from ㎛-sized grains to mm/cm-sized grains in a disk, particularly in dense regions. In order to study whether grains grow and segregate at the protostellar stage, we investigate the ALMA Band 3 (3.1 mm) and 7 (0.87 mm) dust continuum observations of the protostellar disk WL 17 in ρ Ophiuchus L1688 cloud. As reported in a previous study, the Band 3 image shows substructures: a narrow ring and a large central hole. On the other hand, the Band 7 image shows different substructures: a non-axisymmetric ring and an off-center hole. The two-band observations provide a mean spectral index of 2.3, which suggests the presence of mm/cm-sized large grains. Its non-axisymmetric distribution may imply dust segregation between small and large grains. We perform radiative transfer modeling to examine the size and spatial distributions of dust grains in the WL 17 disk. The best-fit model suggests that large grains (>1 cm) exist in the disk, settling down toward the midplane, whereas small grains (~10 ㎛) well mixed with gas are distributed off-center and non-axisymmetrically in a thick layer. The low spectral index and the modeling results suggest that grains rapidly grow at the protostellar stage and that grains differently distribute depending on sizes, resulting in substructures varying with observed wavelengths. To understand the differential grain distributions and substructures, we discuss the effects of the protoplanet(s) expected inside the large hole and the possibility of gravitational instability.

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Effects of Microstructures on the Toughness of High Heat Input EG Welded Joint of EH36-TM Steel (EH36-TM강의 대입열 EGW 용접부 저온 인성에 미치는 미세 조직의 영향)

  • Choi, Woo-Hyuk;Cho, Sung-Kyu;Choi, Won-Kyu;Ko, Sang-Gi;Han, Jong-Man
    • Journal of Welding and Joining
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    • v.30 no.1
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    • pp.64-71
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    • 2012
  • The characteristics of high heat input (342kJ/cm) EG (Electro Gas Arc) welded joint of EH36-TM steel has been investigated. The weld metal microstructure consisted of fine acicular ferrite (AF), a little volume of polygonal ferrite (PF) and grain boundary ferrite (GBF). Charpy impact test results of the weld metal and heat affected zone (HAZ) met the requirement of classification rule (Min. 34J at $-20^{\circ}C$). In order to evaluate the relationship between the impact toughness property and the grain size of HAZ, the austenite grain size of HAZ was measured. The prior austenite grain size in Fusion line (F.L+0.1 mm) was about $350{\mu}m$. The grain size in F.L+1.5 mm was measured to be less than $30{\mu}m$ and this region was identified as being included in FGHAZ(Fine Grain HAZ). It is seen that as the austenite grain size decreases, the size of GBF, FSP (Ferrite Side Plate) become smaller and the impact toughness of HAZ increases. Therefore, the CGHAZ was considered to be area up to 1.3mm away from the fusion line. Results of TEM replica analysis for a welded joint implied that very small size ($0.8\sim1.2{\mu}m$) oxygen inclusions played a role of forming fine acicular ferrite in the weld metal. A large amount of (Ti, Mn, Al)xOy oxygen inclusions dispersed, and oxides density was measured to be 4,600-5,300 (ea/mm2). During the welding thermal cycle, the area near a fusion line was reheated to temperature exceeding $1400^{\circ}C$. However, the nitrides and carbides were not completely dissolved near the fusion line because of rapid heating and cooling rate. Instead, they might grow during the cooling process. TiC precipitates of about 50 ~ 100nm size dispersed near the fusion line.

A Study on the Performance of Flat-plate Solar Air Collector and its Application to Grain Drying (평면식 태양열집열기를 이용한 곡물 건조개선에 관한 연구)

  • 민영봉;최규홍
    • Journal of Biosystems Engineering
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    • v.3 no.2
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    • pp.114-125
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    • 1978
  • The use of petroleum fuels in grain drying causes problems of high cost and management. To solve these problems, it is required to study on soLar energy as an alternative to petroleum fuels for grain drying. The purposes of this study were to find out the optimum received area and air flow rate of a flat-plate solar air collector for grain drying and to assess its effects on grain drying with a small grain bin. The results of this study are summarized as follows ; 1. The calculated optimum tilt angles of the collector in the summer and autumn drying seasons were 20 and 50 degress, respectively, in suwon area. 2. The outlet temperature of the collector was $36^\circ C$ on the daily average with the maximum of $36^\circ C$ at 12:00 o clock. Solar radiation on the collector surface was 1.04 ly( 1 langley = 1 cal/$cm^2$) per minute on the daily average and 1.30 ly per minute on the maximum at 11:00am. The thermal efficiency of the collector was 62.4 percent on the daily average, and the air flow-rate per unit receiving are was 1.03 $m^3$/min/$m^2$.4. The calculated optimum receiving area and the air flow-rate per unit cubic volume for paddy in autumn drying season was 2 $m^2$ and 2$m^3$/min , respectively. 5. not significantly difference in the collector efficiency was appeared between the rotating and fixed type of solar collector. 6. For drying of wheat with 0.6 meter of the depth in the bin, approximately 9 hours were required to reduce the moisture content from 21.6% to 13% with air follow rate of 5 $m^3$/min an initial moisture per cubic meter of wheat and with air temperature of $52^\circ C$. 7. In the drying test of rough rice with a turning operation in a grain bin approximately 21 hours were required to reduced the moisture from 21% to 14.5% with airflow rate of 2 $m^3$/min per cubic meter of rice and the air temperature of $43.5^\circ C$. 8. Over-drying at the bottom and less -drying at the top of the grain mass was resulted from the high -temperature of drying air which was obtained from the flat-plate solar collector in this test. An appropriate operation should be prepared for the uniform moisture of the grain in the bin.

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Effects of Mg and Cu Additions on Superplastic Behavior in MA Aluminum Alloys

  • Han, Chang-Suk;Jin, Sung-Yooun;Bang, Hyo-In
    • Korean Journal of Materials Research
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    • v.28 no.8
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    • pp.435-439
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    • 2018
  • MA Al alloys are examined to determine the effects of alloying of Mg and Cu and rolling on tensile deformation behavior at 748 K over a wide strain rate range($10^{-4}-10^3/s$). A powder metallurgy aluminum alloy produced from mechanically alloyed pure Al powder exhibits only a small elongation-to-failure(${\varepsilon}_f$ < ~50%) in high temperature(748 K) tensile deformation at high strain rates(${\acute{\varepsilon}}=1-10^2/s$). ${\varepsilon}_f$ in MA Al-0.5~4.0Mg alloys increases slightly with Mg content(${\varepsilon}_f={\sim}140%$ at 4 mass%). Combined addition of Mg and Cu(MA Al-1.5%Mg-4.0%Cu) is very effective for the occurrence of superplasticity(${\varepsilon}_f$ > 500%). Warm-rolling(at 393-492 K) tends to raise ${\varepsilon}_f$. Lowering the rolling-temperature is effective for increasing the ductility. The effect is rather weak in MA pure Al and MA Al-Mg alloys, but much larger in the MA Al-1.5%Mg-4.0%Cu alloy. Additions of Mg and Cu and warm-rolling of the alloy cause a remarkable reduction in the logarithm of the peak flow stress at low strain rates (${\acute{\varepsilon}}$< ~1/s) and sharpening of microstructure and smoothening of grain boundaries. Additions of Mg and Cu make the strain rate sensitivity(the m value) larger at high strain rates, and the warm-rolling may make the grain boundary sliding easier with less cavitation. Grain boundary facets are observed on the fracture surface when ${\varepsilon}_f$ is large, indicating the operation of grain boundary sliding to a large extent during superplastic deformation.

Study on the Soil Compaction (흙의 다짐에 관한 연구(I))

  • 강문묵
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.11 no.4
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    • pp.1783-1790
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    • 1969
  • It is one of the most economical method of soil stabilization works to compact soil, which increases soil density artificially. Compaction effort is to lessen void of soils, and consequently its aim is to enlarge friction and cohesion force, and reduce permeability of soil. Factors in compaction effort are moisture content, grain size, grain size distribution, physical properties, compaction method and temperature of soils etc. The results obtained in this study on the effects that grain size, gradation and physical properties influence upon compaction effort for 20 samples under the constant compaction method, are summarized as follows: 1. The bigger the maximum dry density is, the smaller the optimum moisture content is, on the other hand, the smaller the maximum dry densityis, the bigger the optimum moisture content is, ingeneral. 2. The coarser the grain size is, the bigger the maximum dry density is, and the optimum moisture content becomes small, and dry density-moisture content curve has the sharp peak, generally. Also, the finer the grain size is the smaller the maximum dry density is, and the optimum moisture content shows the big value, and dry density-moisture content curve has the dull peak. 3. The maximum dry density shows the biggest value on the sample to be about 15% of particles finer than No. 200 sieve. The more the percent passing of No. 10 sieve increase, the smaller the maximum dry density is. Soils which have uniformity coefficient less than 5 in particles larger than 0.074mm hardly show dry density-moisture content curve. 4. There is a relation which is ramax=2.3948-0.0376 Wopt between the maximum dry density and the optimum moisture content, namely, the maximum dry density is increased in proportion to decrease of the optimum moisture content. 5. There are relations to be the straight lines which the maximum dry density decrease, on the other hand, the optimum moisture content increase in accordance with enlargement of Atterberg Limit(LL, PL, PL) in compacted soils.

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Program Development for Material Degradation Evaluation Using Grain Boundary Etching Method (입계부식법을 이용한 열화도 평가 프로그램 개발)

  • Yu, Hyo-Seon;Baek, Seung-Se;Na, Seong-Hun;Kim, Jeong-Gi;Lee, Hae-Mu
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.7
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    • pp.1064-1072
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    • 2001
  • It is very important to evaluate material degradation like temper and carbide embrittlements to secure the reliable and efficient operational conditions and to prevent brittle failure in service. The extent of material deterioration can be accurately evaluated by mechanical test such as impact test or creep test. But it is almost impossible to sample a large specimen from in-service plants. Thus, the material degradation evaluation by a non-destructive method is earnestly required. Recently the non-destructive test technique which uses the grain boundary etching characteristics owing to the variation of material structures has been proposed. However the program for material degradation evaluation using the grain boundary etching method(GEM) in Windows 98 domain doesnt be developed now. The aims of this paper are to develop the program and to complete the new master curve equations for the evaluation of material degradation on in-serviced high temperature components.

Study on the Conditioning of Brown Rice (I) -Property variation and predicted model of brown rice after Conditioning- (현미 조질에 관한 연구 (I) -조질 후 현미의 물성 변화와 예측모델-)

  • 한충수;연광석;강태환;전홍영;고학균
    • Journal of Biosystems Engineering
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    • v.26 no.1
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    • pp.39-46
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    • 2001
  • This research conducted to investigate the variation of the moisture content, crack ratio, and hardness of the whole and cracked brown rice after conditioning at the initial moisture content of 13, 14, and 15% with time lapse. The conditioning was conducted by increasing the moisture content of the sample to 0.4 and 0.8%. For basic information and conditioning characteristics for the development of a conditioning machine for the brown rice, predicted models of above three properties were developed using a nonlinear regression analysis of SAS with Gauss-Newton, Gradient, and DUD methods. Results of this research could be summarized as follows. 1. No moisture variation occurred after 0.5 hour conditioning. 2. The increasement of the crack ratio was 7.6 and 17.5% with the sample increased the moisture content of 0.4 and 0.8%, respectively, after 8 hours conditioning. 3. The hardness of the conditioned whole grain of the brown rice decreased 0.82 and 1,000kg$\_$f/ with the sample increased moisture content 0.4 and 0.8%, respectively, after 8 hours conditioning with respect to the non-conditioned sample. 4. The hardness of the conditioned cracked grain of the brown rice decreased 0.54 and 0.81kg$\_$f/ with the sample increased moisture content 0.4 and 0.8%, respectively, after 8 hours conditioning with respect to the non-conditioned sample. The hardness of the broken grain was about 0.81∼1.88kg$\_$f/ lower than whole grain. 5. The moisture content variation, increasing rate of the crack ratio, and hardness of the cracked and whole grain was predicted as a negative exponential function. 6. Each predicted model with the nonlinear regression analysis, which was very accurate and had a very small amount of sum of square of error between experimental value and predicted value, which could be used for predicting the physical variation after conditioning.

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An Experimental Study on the Structural Characteristics of Reinforced Concrete Beams Containing Oyster Shells (굴패각을 사용한 철근콘크리트 보의 특성에 관한 실험적 연구)

  • Lee, Sang-cheol;Woo, Song-gyu;An, Yong-deok;Jun, Hak-su;Koo, Hae-shik
    • KIEAE Journal
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    • v.7 no.5
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    • pp.135-142
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    • 2007
  • This is an experimental study on the structural characteristics of reinforced concrete beams using of the oyster shells as a substitute fine aggregate of concrete. In this study, the main factors consist of the grain sizes and the percentage of substitution of oyster shells to fine aggregate in the equal water cement ratio. The results of the study showed as followed. The initial load value of them represented similar constant within 10% of the maximum load value in each test beam. But the maximum load value and the ultimate load value decreased with increased grain size and the rate of substitution. As the grain size of oyster shells became smaller, the load values of them were somewhat higher. The deflection among deformation properties of reinforced concrete beams with oyster shells represented typical curves like that of normal reinforced concrete. In the deformation of steel and concrete, the deformation was proportionated to the load till yield point and from yield point until approaching the ultimate load point. One type was typical curve of the load and the deformation and the other type irregularly was changed to very small deformation for the load increase centering around load axis. After the analyzing structural behaviors and the properties of reinforced concrete test beams with oyster shells, the most excellent grain size of oyster shells represented 1.0mm and less or 5.0mm and less with taking uniformly, and the percentage of practicable substitution of them to fine aggregate was about 30%.

Hydrogen Embrittlement Resistance and Diffusible Hydrogen Desorption Behavior of Multipass FCA Weld Metals (다층 FCA 용착금속의 수소취성 저항성 및 확산성 수소 방출 거동)

  • Yoo, Jaeseok;Xian, Guo;Lee, Myungjin;Kim, Yongdeok;Kang, Namhyun
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.112-118
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    • 2013
  • In this study, constant loading test (CLT) was performed to evaluate the hydrogen embrittlement resistance for multipass FCA weld metals of 600MPa tensile strength grade. The microstructures of weld metal-2 having the smallest carbon equivalent (Ceq=0.37) consisted of grain boundary ferrite and widmanstatten ferrite in the acicular ferrite matrix. The weld metal-1 having the largest Ceq=0.47, showed the microstructures of grain boundary ferrite, widmanstatten ferrite and the large amount of bainite (vol.%=19%) in the acicular ferrite matrix. The weld metal-3 having the Ceq=0.41, which was composed of grain boundary ferrite, widmanstatten ferrite, and the small amount of bainite (vol.%=9%) in the acicular ferrite matrix. Hydrogen desorption spectrometry (TDS) used to analyze the amount of diffusible hydrogen and trapping site for the hydrogen pre-charged specimens electrochemically for 24 hours. With increasing the current density of hydrogen pre-charging, the released amount of diffusible hydrogen was increased. Furthermore, as increasing carbon equivalent of weld metals, the released diffusible hydrogen was increased. The main trapping sites of diffusible hydrogen for the weld metal having a low carbon equivalent (Ceq=0.37) were grain boundaries and those of weld metals having a relatively high carbon equivalent (Ceq: 0.41~0.47) were grain boundaries and dislocation. The fracture time for the hydrogen pre-charged specimens in the constant loading test was decreased as the carbon equivalent increased from 0.37 to 0.47. This result is mainly due to the increment of bainite that is vulnerable to hydrogen embrittlement.