• Title/Summary/Keyword: slip casting

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Analysis of Pore Structure for Porous Body with Coal Fly ash and Clay (석탄회-점토계 다공체의 기공구조 분석)

  • 이기강;박천주
    • Korean Journal of Crystallography
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    • v.9 no.1
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    • pp.64-70
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    • 1998
  • Porous body was prepared from coal fly ash 70 wt%0clay 30 wt% slip using DCC(Direct Coagulated Casting) method. Effect of the specific gravity of the slip on the pore size and distribution of the sintered body was examined by the SEM observation of microstructure and mercury porosimetry measurement of the pore size distribution. Average pore size of the porous sintered body was about 2.5μm for all slips with specific gravity of 1.55, 1.60 and 1.65g/cm3, respectively. Sintered body prepared from the slip of specific gravity of 1.60g/cm3 have the narrowest pore size distribution. slip of specific gravity of 1.55g/cm3 shows broader pore size distribution due to slow gellation process. Slip of specific gravity of 1.65g/cm3 required large amount of deflocculant and showed large variation of the viscosity with addition of coagulant which resulted in very unstable slip properties.

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Study on the Fabrication of Ceramic Core using a Gel-casting Process in Aqueous medium(I) : Gelation Behavior of Polydispered Ceramic Slip (수용액 매체에서 젤-케스팅 공정을 이용한 세라믹 코어 제조에 관한 연구(I) : 다성분계 분산 세라믹 슬립의 젤화 거동)

  • Kim, Jae-Won;Kim, Du-Hyeon;Kim, In-Su;Yu, Yeong-Su;Kim, Jae-Cheol;Jo, Chang-Yong
    • Korean Journal of Materials Research
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    • v.11 no.2
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    • pp.137-145
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    • 2001
  • A new process, gelcasting in aqueous medium, to fabricate complex-shaped ceramic core has investigated. The ceramic slurry, mixture of fused silica powder and additives such as zircon and cordierite, was electrosterically stabilizes. The slip was prepared by ball milling of polydispered ceramic suspension with monomer, dimer and dispersant. The rheological behavior of slip was evaluated by viscosity measurement. It was found that the high solid loading of polydispersed ceramic slip, which has low viscosity of 50vol%, is possible to obtained. The viscosity of the slip was significantly dependent upon the amount of polymer dispersant and the formulation of monomer and dimer. The green bodies were fabricated through casting and gelation at room temperature followed by drying at $25^{\circ}C$ for 48hrs under relative humidity of 80~85%. Crack-free green body was successfully fabricated through the above process.

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Effects of the Addition of Alumina on the Mechanical Properties of Cast Zirconia Sintered Body (주입성형한 지르코니아 소결체의 기계적 성질에 미치는 알루미나 첨가의 영향)

  • Lee, Dong-Yoon;Jo, Jun-Ho;Seo, Jeong-Il;Bae, Won-Tae
    • Journal of Technologic Dentistry
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    • v.34 no.2
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    • pp.113-119
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    • 2012
  • Purpose: Zirconia blocks for all ceramic dentures are divided into two groups. One is pre-heated block and the other is binder added block. In this study, the possibility of recycling the remained parts of binder added block after CAD/CAM machining with slip casting process was investigated. Methods: Owing to the binder added block contain large amount of organic matter, Binder burn-out was must be carried out before ball milling for preparing the casting slip. Binder burn-out was accomplished at $600^{\circ}C$ for 10 hours. Ball milling was performed with 5mm zirconia ball and 60mm polyethylene bottle. From 0% to 5% at 1% intervals of alumina was added to zirconia powder for preparing slip. Solid casting was achieved with plaster mold. Cast bodies were dried and sintered at $1,500^{\circ}C$ for 1 hour. Linear shrinkage, apparent porosity, water absorption, bulk density, and flexural strength were tested. Microstructures were observed by SEM, EDS and XRD analysis were executed. Results: Optimum slips for casting was prepared with 300g ball, 100g powder, and 180g distilled water. Cast body without alumina showed 26% of linear shrinkage, 6.07 of apparent density, and 470MPa of three point bend strength. On the other hand, as received zirconia block, which was sintered at the same conditions, showed 23% of linear shrinkage, 6.10 of apparent density, and 680MPa of three point bend strength. When 3% of alumina was added to zirconia, sintered body showed 23% of linear shrinkage, 6.10 of apparent density, and 780MPa of three point bend strength. SEM photomicrographs and EDS analysis showed alumina particles uniformly dispersed in zirconia matrix, and XRD analysis showed no phase transformation of tetragonal zirconia particles was occurred when alumina was added. Conclusion: According to the all of this experimental results, 3% of alumina added cast zirconia body showed excellent mechanical properties more than as received binder containing zirconia block.

Fabrication of Light Aggregates Using the Fly Ash-Clay Slurry

  • Seunggu Kang;Lee, Kigang;Kim, Jungwan
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.06a
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    • pp.81-86
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    • 1998
  • The light aggregates were fabricated by sintering green bodies made form the fly ash-clay alip. The content of fly ashes in the slip could be increased up to 70wt.% due to controlled rheological behavior of the slip, and the green body of uniform microstructure could be obtained by DCC(Direct Coagulation Casting)method. The apparent density, microstructure and compressive strength for sintered bodies fired at 1100∼1200$^{\circ}C$ were evaluated. The properties of light aggregates fabricated depend on slip density, particle behavior in the slip and sintering conditions. The sintered body prepared by firing a green body made from slip of density 1.60 at 1150$^{\circ}C$/2hr satisfied conditions of a light aggregate as apparent density of 1.49${\pm}$0.02 and compressive strength of 584${\pm}$62kg/$\textrm{cm}^2$.

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Viscosity Study to Optimize a Slurry of Alumina Mixed with Hollow Microspheres

  • Bukhari, Syed Zaighum Abbas;Ha, Jang-Hoon;Lee, Jongman;Song, In-Hyuck
    • Journal of the Korean Ceramic Society
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    • v.52 no.6
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    • pp.403-409
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    • 2015
  • Porous alumina ceramics are involved in many industrial applications due to the exceptional properties of these products. This study addresses the preparation of porous alumina ceramics using hollow microspheres as a pore-forming agent and slip casting as a green-body-forming technique. A uniform distribution of pores is a basic requirement of a porous material. This study investigates three different slurry systems, i.e., as-prepared alumina slurry, alumina slurry electrostatically dispersed by hydrochloric acid (HCl), and slurry dispersed by the commercial dispersant 'Darvan C-N'. At a low viscosity, the hollow microspheres in the slurry tend to float, which causes a non-uniform pore distribution. To avoid this phenomenon, the viscosity of the slurry was increased to the extent that the movement of hollow microspheres ceased in the slurry. As a result, a uniform pore distribution was achieved.

냉간압연가공시 Work roll 마멸과 Slip에 관한 연구

  • 전언찬;김순경
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1992.04a
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    • pp.274-278
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    • 1992
  • 냉간압연기술의 발달로 냉간압연기도 매우 다양하게 발달되었으며 냉간압연의 원자재인 열간압연재의 종류도 다양하다. 최근 열간압연가공시 회수율이 높은 연속주조재(Continuous casting strip)인 CC 재가 종전의 가공과정이 복잡하며 불량율이 높은 Ingot주조재(Ingot casting strip)인 IC 재 보다 생산비율이 점차 증대되어 냉간압연재료의 주종을 차지하고있다. CC재는 냉간압연가공시 IC재에 비해 Work roll 조도저하가 현저하게 크기 때문에 슬립(Slip)과 채팅(Charttering) 현상 등이 발생하여 압연가공성이 불안정 하게 되어 Work roll과 판표면에 손상이 생기게 되고, 압연가공시 Roll 사고 등의 문제가 발생하므로 Roll 마멸의 정도를 파악하여 Roll을 효과적으로 관리하므로써 Work roll과 판표면의 슬립현상 및 채터 링현상 등을 방지할 수 있다.

Characteristics of sintered fly ash-clay body prepared by slip processing and its applicability for foundation soils (슬립 공정으로 제조된 비산재-점토 계 소결체의 물성 및 기반재로의 적용특성)

  • Kang, Seung-Gu;Lee, Yeong-Saeng
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.6
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    • pp.271-276
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    • 2008
  • The civil engineering properties for the coal fly ash produced from a power plant mixed with sintered powders made from the fly ash-clay slip system were measured and its applicability for the foundation soils was investigated. The F-slip whose dispersion state is 'not good' and C-slip which is re-flocculated by adding a flocculant to a well-dispersed slip were fabricated and then sintered. The sintered body made from C-slip had more uniform microstructure than that of F-slip, therefore, the bulk density and compressive strength were improved. The civil engineering properties such as compression index, compressive strength, permeability coefficient of fly ash were improved by mixing $0.84{\sim}2\;mm$ powders obtained by crushing a sintered body made from C-slip. Therefore, the applicability of mixed powders composing of fly ash and sintered body made from C-slip was confirmed to foundation soils due to its improved civil engineering properties.

Microstructures and Drying of the Alumina Green Body by the Gel-Casting Method (Gel-Casting으로 제조한 알루미나 성형체의 건조와 미세구조)

  • 오창준;이홍림
    • Journal of the Korean Ceramic Society
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    • v.31 no.12
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    • pp.1467-1474
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    • 1994
  • The effects of the dispersion, drying, and binder burning-out on the green-microstructures of gelcasted alumina were studied. The slip consisting of 55 vol% alumina powder and 5 wt% organic materials was well-dispersed by adding 0.28 wt% polyelectrolyte polymer. Green bodies were dried at >85% relative humidity at room temperature. Green-microstructures were observed to be depended on the heating rate during binder burnout. Constant drying rate was not observed in drying process of gelcasted alumina. Sintered body showed its relative density higher than 99% when it was sintered at 1$600^{\circ}C$ for 2 hours.

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Neural Fuzzy Mold Level Control for Continuous Steel Casting

  • Lim, Chang-Gyoon;Kueon, Yeong-Seob;Kim, Yigon
    • International Journal of Fuzzy Logic and Intelligent Systems
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    • v.2 no.2
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    • pp.146-152
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    • 2002
  • Mold level control has been a major control task for continuous casting plants. The system involves nonlinearities such as stick-slip friction in the sliding gate, time-delay, friction force variations between molten steel and the inner wall of mold, and nozzle logging/unclogging. These complex problems should be solved to control mold level for steel cast. In this paper, we propose a neural fuzzy mold level control technique for solving these complex problems and give experiment studies to show the mold level control in continuous casting process.