• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1997년도 제25회 춘계학술대회
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• pp.53-61
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• 1997

The effect of sintering condition on tribological behavior in the Cu-base sintered friction materials was studied through pin-on-disk type wear tester. Especially, the experiment was focused on making a comparative study between presstwed sintering and pressureless sintering. Pressureless sintering process showes more stable friction coefficient and lower wear rate than pressure sintering process. This result is related to pore size and density of pore in the sintered materials.

• 한국결정성장학회지
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• 제25권1호
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• pp.6-12
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• 2015

율속제어소결은 소결 공정 중 실시간으로 측정되는 시편의 팽창/수축거동을 이용해 일정한 수축거동을 하도록 로의 파워를 조정하는 소결방법으로, 온도를 조절하기 위해 로의 파워를 제어하는 일반적인 소결에 비해 시편의 소결 과정을 세밀히 제어할 수 있으며, 특히 소결공정의 최적화를 이룰 수 있는 장점이 있다. 본 연구에서는 탄화붕소의 소결에 율속 제어소결을 적용해 각 공정변수의 조절에 따른 소결온도 및 입자성장의 변화를 조사하여 그 상관관계를 규명하고 이를 기존의 이론에 맞추어 해석함으로써 율속제어소결을 어떻게 소결공정 최적화에 이용할 수 있는지 그 가능성을 알아보았으며 이를 통해 향후 미지 소재의 소결공정에 율속제어공정을 어떻게 적용할 수 있는지 고찰해 보았다.

• 한국분말재료학회지
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• 제11권1호
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• pp.55-59
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• 2004

TiNi bodies were produced from (Ti＋Ni) powder mixture by spark-plasma sintering procerg. The sintering behavior was investigated through the measurement of change in density, densification rate, phase analysis and microstructure. Irrespective of heating rate, sintered bodies with above 97％ relative density could be obtained. TiNi with B2 structure was confirmed as the major phase and $Ti_2Ni,\;TiNi_3$, unreacted Ti, Ni as the second phase. Increase in heating rate suppressed a formation of intermediate phase during sintering process. Increase in holding time at sintering temperature led to a compositional homogenization.

• 한국분말재료학회지
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• 제8권1호
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• pp.61-69
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• 2001

Spark-Plasma Sintering(SPS) is one of the new sintering methods which takes advantages both inconventional pressure sintering and electric current sintering. It is known that SPS is very effective for the densification of hard-to-sinter materials like refractory metals, intermetallic compounds, glass and ceramics without grain growth. However, a clear explanation for sintering mechanism and an experimental evidence for the formation of weak plasma during SPS are not given yet. In this study, fundamental study on sintering behavior and mechanism of SPS was investiged. For this study, various spherical Fe powders were prepared such as as-received, as-reduced, and as-oxidized and then sintered by SPS facility. In order to confirm the surface cleaning effect during SPS neck region and fracture surface of sintered body was observed and analyzed by SEM/EPMA. Densification behavior was analyzed from the data of deflection along the pressure axis. Some specimens were additionally produced by Hot Pressing and the results were compared with those of SPS.

• 한국분말재료학회지
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• 제5권2호
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• pp.89-97
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• 1998

Sintering behavior of nanostructured(NS) W-Cu powders prepared by mechanical alloying (MA) was investigated as a function of sintering temperature. MA NS W-2owt%Cu and W-3owt%Cu composite powders with the crystal size of 20-30 nm were annealed at 90$0^{\circ}C$, and thermal characteristics of those powders were investigated by DSC. Sintering behavior of MA NS W-Cu composite powders was investigated during the solid-state sintering and the Cu-liquid phase sintering. The new nanosintering phenonenon of MA W-Cu powders at solid-state sintering temperature was suggested to explain the W-grain growth in the inside of MA powders. The sintering densification of MA NS W-Cu powders was enhanced at Cu melting temperature by arrangement of MA powders, i.e., the first rearrangement of MA powders was occurred, and then the rearrangement of W-grains in the sintered parts was also took place during liquid-phase sintering, i.e., the second rearrangement was happened. Due to the double rearrangement process of MA NS W-Cu powders, the high sintered density with more than 96%o was obtained and the fine and high homogeneous state of W and Cu phases was achieved by sintering at 1200 $^{\circ}C$.

• 한국분말재료학회지
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• 제7권2호
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• pp.93-101
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• 2000

In order to clarify the enhanced sintering behavior of nanostructured(NS) W-Cu powder prepared by mechaincal alloying, the sintering behavior during heating stage was analysed by a dilatometry with various heating rates. The sintering of NS W-Cu powders was characterized by the densification of two stages, having two peaks in shrinkage rate curves. The temperature at which the first peak appear was much lower than Cu melting point, and dependent on heating rate. On the basis of the shrinkage rate curves and the microstructural observation, the coupling effect of nanocrystalline W-grain growth and the liquid-like behavior of Cu phase was suggested as a possible mechanism for the enhanced sintering of NS W-Cu powder in the state.

• 한국분말재료학회지
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• 제21권1호
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• pp.7-15
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• 2014

This study investigated the densification behavior of rhenium alloys including W-25 wt.%Re and Re-2W-1Ta (pure Re) during sintering. The dilatometry experiments were carried out to obtain the in-situ shrinkage in $H_2$ atmosphere. The measured data was analyzed through shrinkage, strain rate and relative density, and then symmetrically treated to construct the linearized form of master sintering curve (MSC) and MSC as a well-known and straightforward approach to describe the densification behavior during sintering. The densification behaviors for each material were analyzed in many respects including apparent activation energy, densification parameter, and densification ratio. MSC with a minimal set of preliminary experiments can make the densification behavior to be characterized and predicted as well as provide guideline to sinter cycle design. Considering the results of linearized form and MSC, it was confirmed that the W-25 wt.%Re compared to Pure Re is more easily densified at the relatively low temperature.

• 한국분말재료학회지
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• 제10권1호
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• pp.40-45
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• 2003

Sintering behavior of 2xxx series Al alloy was investigated to obtain full densification and sound microstructure. The commercial 2xxx series Al alloy powder. AMB2712, was used as a starting powder. The mixing powder was characterized by using particle size analyzer, SEM and XRD. The optimum compacting pressure was 200 MPa, which was the starting point of the "homogeneous deformation" stage. The powder compacts were sintered at $550~630^{\circ}C$ after burn-off process at $400^{\circ}C$. Swelling phenomenon caused by transient liquid phase sintering was observed below $590^{\circ}C$ of sintering temperature. At $610^{\circ}C$, sintering density was increased by effect of remained liquid phase. Further densification was not observed above $610^{\circ}C$. Therefore, it was determined that the optimum sintering temperature of AMB2712 powder was $610^{\circ}C$.}C$.

• 한국분말재료학회지
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• 제1권2호
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• pp.190-197
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• 1994

The densification behavior during a sintering of M2 and T15 grade high speed steel powder compacts was reported. Sintered densities over 98% theoretical were achieved by a liquid phase sintering in vacuum for both grades. The optimum sintering temperature range where full densification could be achieved without excessive carbide coarsening and incipient melting was much narrower in M2 than in T15 grade. The sintering response was mainly affected by the type of carbides present. The primary carbides in M2 were identified as $M_6C$ type whereas those in T15 were MC type which provides wider sintering range. The addition of elemental carbon up to 0.3% lowered the optimum sintering temperature for both grades, but had little effect on expanding the sintering range and sintered structure.

• 한국분말재료학회지
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• 제17권2호
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• pp.154-159
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• 2010

In this study, the sintering behavior of (Nd, Dy)-Fe-B powder which fabricated by strip-casting was investigated with various sintering temperatures and holding times. The relative density over 99% could be obtained by both sintering at $1070^{\circ}C$ for 1h and sintering at $970^{\circ}C$ for 20h. The grain growth was observed in sintered specimen at $1050^{\circ}C$ compared to one at $970^{\circ}C$. The isothermal sintering process below $1000^{\circ}C$ led to suppress grain growth showing the improved magnetic properties. The phase transformation of Nd-rich was confirmed by X-ray diffraction pattern.