• Title/Summary/Keyword: single-pass

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Crystal Structure of Fully Dehydrated Partially Cs+-Exchanged Zeolite X, Cs52Na40-X (The Highest Cs+-Exchanged Level Achieved by Conventional Method and Confirmation of Special Site Selectivity)

  • Bae, Myung-Nam
    • Bulletin of the Korean Chemical Society
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    • v.28 no.2
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    • pp.251-256
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    • 2007
  • The crystal structure of fully dehydrated partially Cs+-exchanged zeolite X, [Cs52Na40Si100Al92O384], a = 24.9765(10) A, has been determined by single-crystal X-ray diffraction techniques in the cubic space group Fd3 at 21 °C. The crystal was prepared by flow method for 5 days using exchange solution in which mole ratio of CsOH and CsNO3 was 1 : 1 with total concentration of 0.05 M. The crystal was then dehydrated at 400 °C and 2 × 10-6 Torr for 2 days. The structure was refined to the final error indices, R1 = 0.051 and wR2 (based on F2) = 0.094 with 247 reflections for which Fo > 4σ (Fo). In this structure, about fifty-two Cs+ ions per unit cell are located at six different crystallographic sites with special selectivity; about one Cs+ ion is located at site I, at the centers of double oxygen-rings (D6Rs), two Cs+ ions are located at site I', and six Cs+ ions are found at site II'. This is contrary to common view that Cs+ ions cannot pass sodalite cavities nor D6Rs because six-ring entrances are too small. Ring-opening by the formation of ?OH groups and ring-flexing make Cs+ ions at sites I, I', and II' enter six-oxygen rings. The defects of zeolite frameworks also give enough mobility to Cs+ ions to enter sodalite cavities and D6Rs. Another six Cs+ ions are found at site II, thirty-six are located at site III, and one is located at site III' in the supercage, respectively. Forty Na+ ions per unit cell are located at two different crystallographic sites; about fourteen are located at site I, the centers of D6Rs and twenty-six are also located at site II in the supercage. Cs+ ions and Na+ ions at site II are recessed ca. 0.34(1) A and 1.91(1) A into the supercage, respectively. In this work, the highest exchange level of Cs+ ions per unit cell was achieved in zeolite X by conventional aqueous solution methods and it was also shown that Cs+ ion could pass through the sixoxygen rings.

A case study on the conditions of direct transport for the preferential tariff treatment through Korea-EU FTA(Free Trade Agrement) (한.EU FTA하에서 협정관세적용을 위한 직접운송 요건의 충족여부에 관한 사례연구)

  • Han, Sang-Hyun
    • International Commerce and Information Review
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    • v.15 no.2
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    • pp.207-232
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    • 2013
  • FTA(Free Trade Agreement) of South Korea and European Union(EU) took effect from July 1, 2011. Korea signed a contract FTA with the European Union by first among Asian country, and Korea EU FTA is evaluated that it is wide, comprehensive and high level FTA. Therefore, Korea EU FTA will become FTA that dimension is high, and FTA fermentation with the European Union may activate the Korean economy through extension of export. By the way, in Korea EU FTA, the stipulations on import and export clearance system is different compared with other FTA. Therefore, exporter and importers should compare thoroughly on essential factor of origin standard and preferential tariff which is set in FTA Agreement. In this study, I analyzed 'conditions of direct transport' that is prescribed in article 13 of Korea EU FTA. Particular, I analyzed recently example of appeal for review that decision is made in the Korea Customs Service(KCS). Laying stress on counter measure of business, conclusion in this study is as following. First, companies must understand correctly a single consignment and a single transport document under Korea EU FTA. Second, companies must not analyze wrong 'conditions of direct transport'. Third, when simplicity transshipment or temporary custody is consisted, companies must secure documentary evidence as soon as possible. Fourth, in case goods pass third country, companies must understand uprightly 'a single consignment'. Finally, companies should keep in mind to truth that European Union and EFTA are different FTA.

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Ground Altitude Computation Algorithm using Laser Altimeter and GPS for UAV Automatic Take-off and Landing (레이저 고도계 및 GPS를 이용한 무인기의 자동이착륙용 지면고도계산 알고리듬 설계)

  • Cho, Sangook;Choi, Keeyoung;Kim, Sung-Su
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.41 no.1
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    • pp.54-60
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    • 2013
  • This paper presents a ground altitude determination algorithm using a laser altimeter and GPS for automatic take-off and landing of UAV. The characteristics of the laser altimeter was analyzed in ground tests and a low-pass filter was designed to reduce the effect of signal interruption due to reflectivity problem. The paper shows that a single sensor cannot measure ground altitude appropriately in terms of reliability and accuracy. To complement shortcomings of the laser altimeter, the linear Kalman filter was designed using DGPS vertical speed. Designed filter was validated and tuned through the steps of simulation, ground test and flight test. It was confirmed that the accuracy for automatic landing is achievable.

A Study on the Parallel Multiplier over $GF(3^m)$ Using AOTP (AOTP를 적용한 $GF(3^m)$ 상의 병렬승산기 설계에 관한 연구)

  • Han, Sung-Il;Hwang, Jong-Hak
    • Journal of IKEEE
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    • v.8 no.2 s.15
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    • pp.172-180
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    • 2004
  • In this paper, a parallel Input/Output modulo multiplier, which is applied to AOTP(All One or Two Polynomials) multiplicative algorithm over $GF(3^m)$, has been proposed using neuron-MOS Down-literal circuit on voltage mode. The three-valued input of the proposed multiplier is modulated by using neuron-MOS Down-literal circuit and the multiplication and Addition gates are implemented by the selecting of the three-valued input signals transformed by the module. The proposed circuits are simulated with the electrical parameter of a standard $0.35{\mu}m$CMOS N-well doubly-poly four-metal technology and a single +3V supply voltage. In the simulation result, the multiplier shows 4 uW power consumption and 3 MHzsampling rate and maintains output voltage level in ${\pm}0.1V$.

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Gas and particle removal characteristics of a novel electrostatic precipitation type air cleaner using an activated carbon filter as an electrode (활성탄 섬유 필터를 전극으로 활용한 정전 방식의 공기정화장치의 가스 및 입자 제거 특성 분석)

  • Lim, Gi-Taek;Kim, Yong-Jin;Han, Bangwoo;Woo, Chang Gyu;Shin, Weon Gyu;Kim, Hak-Joon
    • Particle and aerosol research
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    • v.14 no.1
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    • pp.9-16
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    • 2018
  • We have developed an electrostatic precipitation (ESP) type air cleaner for indoor air quality and investigated its performances regarding CADR (Clean air delivery rate), single-pass efficiency and gas removal efficiency. The ESP air cleaner used an ACF (Activated carbon fiber) filter for gas removal and the ACF as a high voltage electrode for particle removal. The ESP air cleaner was tested in a chamber with the volume of $1m^3$ regarding CADR and gas removal efficiency. The applied CADR area of the ESP was $1.8m^2$. Gas removal efficiency was tested with 3 gases (Acetaldehyde, Acetic acid, Ammonia). As the results of the gas removal efficiency, the ESP air cleaner shows the removal efficiencies of 90, 98 and 85% for acetaldehyde, acetic acid and ammonia, respectively.

The Disruption of Saccharomyces cerevisiae Cells and Release of Glucose 6-Phosphate Dehydrogenase (G6PDH) in a Horizontal Dyno Bead Mill Operated in Continuous Recycling Mode

  • Mei Chow Yen;Ti Tey Beng;Ibrahim Mohammad Nordin;Ariff Arbakariya;Chuan Ling Tau
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.10 no.3
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    • pp.284-288
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    • 2005
  • Baker's yeast was disrupted in a 1.4-L stainless steel horizontal bead mill under a continuous recycle mode using 0.3 mm diameter zirconia beads as abrasive. A single pass in continuous mode bead mill operation liberates half of the maximally released protein. The maximum total protein release can only be achieved after passaging the cells 5 times through the disruption chamber. The degree of cell disruption was increased with the increase in feeding rate, but the total protein release was highest at the middle range of feeding rate (45 L/h). The total protein release was increased with an increase in biomass concentration from 10 to $50\%$(w/v). However, higher heat dissipation as a result of high viscosity of concentrated biomass led to the denaturation of labile protein such as glucose 6-phosphate dehydrogenase (G6PDH). As a result the highest specific activity of G6PDH was achieved at biomass concentration of $20\%$(ww/v). Generally, the degree of cell disruption and total protein released were increased with an increase in impeller tip speed, but the specific activity of G6PDH was decreased substantially at higher impeller tip speed (14 m/s). Both the degree of cell disruption and total protein release increased, as the bead loading increased from 75 to $85\% (v/v)$. Hence, in order to obtain a higher yield of labile protein such as G6PDH, the yeast cell should not be disrupted at biomass concentration and impeller tip speed higher than $20\%(w/v)$ and 10 m/s, respectively.

Paleomagnetic Study of the Lower Ordovician Formations in the North Eastern Okcheon Zone (옥천대 북동부에 분포하는 하부 고생대층에 대한 고지자기 연구)

  • Min, Kyung Duck;Lee, Youn Soo;Hwang, Suk Yeon
    • Economic and Environmental Geology
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    • v.26 no.3
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    • pp.395-401
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    • 1993
  • Lower Ordovician rock samples were collected from 23 sites located at the Okcheon non-metamorphic zone, near Taeback and Yeongweol areas, southern part of the Korean Peninsula. A characteristic magnetic component was obtained from four sites. This stable direction ($Dm=-19.4^{\circ}$, $Im=24.1^{\circ}$) which is carried by hematite of very high temperature $679^{\circ}C$), successfully pass both of reversal test and paleopole reliability test, and is regarded as a primary direction. The remagnetized components can be divided into three on the basis of their characteristic directions and magnetic minerals. The first which is carried by hematite, magnetite and pyrrhotite, is widely found at the whole sites. It shows syn- or post-tectonic remagnetization according to strongly negative fold test and distribution between Mesozoic and present field directions. The second, in situ, is distinguishable from the present field direction. After bedding correction, it is identical to Late Triassic to Early Jurassic direction. Its magnetic carrier is considered to be a single component hematite, which may be acquired by pre-tectonic CRM in the Okcheon orogenic zone. The third, which is carried by magnetite and hematite, is characterized by stable reversed direction. These minerals may be acquired by the thermal or chemical process in unknown period. Paleopole position is $169.2^{\circ}E$ in longitude and $59.9^{\circ}S$ in latitude, which indicates that the study area was located at $12.6^{\circ}S$ in paleo-latitude and belonged to northern end of the Gondwana in Early Ordovician.

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Analysis of Genes Expressed during Pepper-Phytophthora capsici Interaction using EST Technology (EST기법을 이용한 고추와 고추역병균간의 상호작용에서 발현되는 유전자들의 분석)

  • Kim, Dongyoung;Lee, Jong-Hwan;Choi, Woobong
    • Journal of Life Science
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    • v.24 no.11
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    • pp.1187-1192
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    • 2014
  • Pepper, consumed as a typical spice food around world, is mainly cultivated in warm countries, including Korea, China, and Mexico. Phytophthora capsici is a pathogen on several economically important crops, including pepper. The oomycete attacks the roots, stems, leaves, and fruit of the host plants. To understand the molecular mechanisms underlying development of the disease, the genes expressed during pepper-P. capsici interaction were explored by analyzing expressed sequence tags (ESTs). A cDNA library was constructed from total RNA extracted from pepper leaves challenged with P. capsici for three days, resulting in an early stage of symptom development for comparable interaction. A comprehensive analysis of single-pass sequencing of 5,760 randomly selected cDNA clones extracted 5,148 high-quality entries for contig assembly, which generated 2,990 unigenes. A homology search of the unigenes with BLASTX resulted in 2,409 matches, of which 606 showed classified functional catalogs.

A STUDY ON THE FRACTURE OF DENTAL AMALGAM (치과용 아말감의 파절에 관한 연구)

  • Huh, Hyeon-Do;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.9 no.1
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    • pp.101-106
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    • 1983
  • It was the purpose of this study to investigate the fracture mode of dental amalgam by observing the crack propagation, and to relate this to the microstructure of the amalgam. Caulk 20th Century Regular, Caulk Spherical, Dispersalloy, and Tytin amalgam alloys were used for this study. After each amalgam alloy and Hg measured exactly by the balance was triturated by the mechanical amalgamator (Capmaster, S.S. White), the triturated mass was inserted into the cylindrical metal mold which was 4 mm in diameter and 12 mm in height and was pressed by the Instron Universal Testing Machine at the speed of 1mm/min with 120Kg. The specimen removed from the mold was stored in the room temperature for a week. This specimen was polished with the emery papers from #100 to #200 and finally on the polishing cloth with 0.06${\mu}Al_2O_3$ powder suspended in water. The specimen was placed on the Instron testing machine in the method similar to the diametral tensile test and loaded at the crosshead speed of 0.05mm/min. The load was stopped short of fracture. The cracks on the polished surface of specimen was examined with scanning electron microscope (JSM-35) and analyzed by EPMA (Electron probe microanalyzer). The following results were obtained. 1. In low copper lathe-cut amalgam, the crack went through the voids and ${\gamma}_2$ phase, through the ${\gamma}_1$ phase around the ${\gamma}$ particles. 2. In low copper spherical amalgam, it was observed that the crack passed through the ${\gamma}_2$ and ${\gamma}_1$ phase, and through the boundary between the ${\gamma}_1$ and ${\gamma}$ phase. 3. In high copper dispersant (Dispersalloy) amalgam, the crack was found to propagate at the interface between the ${\gamma}_1$ matrix and reaction ring around the dispersant (Ag-Cu) particles, and to pass through the Ag-Sn particles. 4. In high copper single composition (Tytin) amalgam, the crack went through the ${\gamma}_1$ matrix between ${\eta}$ crystals, and through the unreacted alloy particle (core).

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An Efficient Approach for Single-Pass Mining of Web Traversal Sequences (단일 스캔을 통한 웹 방문 패턴의 탐색 기법)

  • Kim, Nak-Min;Jeong, Byeong-Soo;Ahmed, Chowdhury Farhan
    • Journal of KIISE:Databases
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    • v.37 no.5
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    • pp.221-227
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    • 2010
  • Web access sequence mining can discover the frequently accessed web pages pursued by users. Utility-based web access sequence mining handles non-binary occurrences of web pages and extracts more useful knowledge from web logs. However, the existing utility-based web access sequence mining approach considers web access sequences from the very beginning of web logs and therefore it is not suitable for mining data streams where the volume of data is huge and unbounded. At the same time, it cannot find the recent change of knowledge in data streams adaptively. The existing approach has many other limitations such as considering only forward references of web access sequences, suffers in the level-wise candidate generation-and-test methodology, needs several database scans, etc. In this paper, we propose a new approach for high utility web access sequence mining over data streams with a sliding window method. Our approach can not only handle large-scale data but also efficiently discover the recently generated information from data streams. Moreover, it can solve the other limitations of the existing algorithm over data streams. Extensive performance analyses show that our approach is very efficient and outperforms the existing algorithm.