• Title/Summary/Keyword: single step

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Fabrication of PZT Film by a Single-Step Spin Coating Process

  • Oh, Seung-Min;Kang, Min-Gyu;Do, Young-Ho;Kang, Chong-Yun;Nahm, Sahn;Yoon, Seok-Jin
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.193-193
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    • 2011
  • To obtain ceramic films, the sol-gel coating technique has been broadly used with heat treatment, but crack formation tend to occur during heat treatment in thick sol-gel films. We prepared PZT thin films by sol-gel method with single-step spin coating process. The PZT solution have been synthesized using lead acetate ($Pb(CH_3COO)_2$), zirconium acetylacetonate ($Zr(OC_3H_7^n)_4$), and titanium diisopropoxide bis(acetylacetonate) 75wt% in isopropanol ($Ti(OC_3H_7^i)_2(OC_3H_7^n)_2$) as starting materials and n-propanol was selected as a solvent. The poly(vynilpyrrolidone) (PVP) was added with 0, 0.25, 0.5, 0.75, and 1 molar ratios to control viscosity of solution. We investigated influence of the viscosity on thickness, microstructure, and electrical properties of final PZT films. Thermo-gravimetric analysis and differential scanning calorimeter (TGA/DSC) was carried out from room temperature to $800^{\circ}C$ in order to measure pyrolysis temperature. Structural characteristics were analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Ferroelectric and dielectric properties were measured by RT66A (Radiant) and impedance analyzer (Agilent), respectively. The thicknesses of PZT films depended on incorporation of an excess amount of PVP. Finally, we obtained PZT films of good quality without crack formation via single-step spin coating.

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Test method for step-by-step construction of Autonomous station control system (자율분산 역 제어시스템 단계적 구축에 따른 테스트 방법)

  • Kim, Young-Hoon
    • Proceedings of the KSR Conference
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    • 2007.05a
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    • pp.1239-1243
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    • 2007
  • Autonomous Station Control System is automatic route control system of large-scale station. The system has flexibility of system step-by-step construction and expandability. A method of step-by-step construction for Autonomous Station Control System has system expansion and subsystem software expansion. The system has autonomous controllability and autonomous coordinability for system step by step construction. With property for a basis, each of subsystem communicates data field. Also, Each subsystem has its own management system, Autonomous Data Manager to manage itself and coordinate with the others. This paper make clear test method for Autonomous Station Control System expansion and software expansion. The first test method of system increasing construction is single station construction test. The second of method is connecting test the neighbor's Autonomous Station Control System. The third of method is connecting test the Autonomous Line Management System. Also, the test method of software expansion take the case of route control subsystem.

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Simulation of Containment Pressurization in a Large Break-Loss of Coolant Accident Using Single-Cell and Multicell Models and CONTAIN Code

  • Noori-Kalkhoran, Omid;Shirani, Amir Saied;Ahangari, Rohollah
    • Nuclear Engineering and Technology
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    • v.48 no.5
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    • pp.1140-1153
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    • 2016
  • Since the inception of nuclear power as a commercial energy source, safety has been recognized as a prime consideration in the design, construction, operation, maintenance, and decommissioning of nuclear power plants. The release of radioactivity to the environment requires the failure of multiple safety systems and the breach of three physical barriers: fuel cladding, the reactor cooling system, and containment. In this study, nuclear reactor containment pressurization has been modeled in a large break-loss of coolant accident (LB-LOCA) by programming single-cell and multicell models in MATLAB. First, containment has been considered as a control volume (single-cell model). In addition, spray operation has been added to this model. In the second step, the single-cell model has been developed into a multicell model to consider the effects of the nodalization and spatial location of cells in the containment pressurization in comparison with the single-cell model. In the third step, the accident has been simulated using the CONTAIN 2.0 code. Finally, Bushehr nuclear power plant (BNPP) containment has been considered as a case study. The results of BNPP containment pressurization due to LB-LOCA have been compared between models, final safety analysis report, and CONTAIN code's results.

Comparison of Spatio-temporal Gait Parameters between Paretic and Non-paretic Limb while Stepping over the Different Obstacle's Heights in Subjects with Stroke (편마비 환자의 장애물 높이에 따른 마비측과 비마비측 하지의 시공간적 보행변수 비교)

  • Han, Jin-Tae
    • Journal of the Korean Society of Physical Medicine
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    • v.9 no.1
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    • pp.69-74
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    • 2014
  • PURPOSE: The aim of this study is to compare the spatio-temporal gait parameters between paretic and non-paretic limb while stepping over the different obstacle's heights in subjects with stroke. METHODS: Nine subjects with stroke were participated in this study. Subjects were asked to step over obstacles with a different height. 8 camera motion analysis system(Motion Analysis Corporation, Santa Rosa, USA) was used to measure spatio-temporal parameters. The two way repeated measurement ANOVA was used to compare spati-temporal gait parameters between paretic and non-paretic limbs while stepping over a different obstacle's height(0cm, 10cm, 20cm). RESULTS: Step width, velocity, single supoort time, and double support time were not different among obstacle's height(p>0.05) but stride length, step length, and cadence were significantly different(p>0.05). In stride length, cadence, and double support time, the interactions between obstacle's heights and limbs were not different(p>0.05) but it was significantly different in velocity, step length, and single support time(p<0.05). Velocity, stride length, cadence, and double support times were not different between paretic limb and non-paretic limb(p>0.05) but step length and single support times were significantly different between paretic limb and non-paretic limb(p<0.05). CONCLUSION: These results show that there are differences with spatio-temporal gait parameters among obstacle's heights and between paretic and non-paretic limb during obstacle crossing in subjects with stroke.

A Combination Strategy for Construction of Peptide-β2m-H-2Kb Single Chain with Overlap Extension PCR and One-Step Cloning

  • Xu, Tao;Li, Xiaoe;Wu, You;Shahzad, Khawar Ali;Wang, Wei;Zhang, Lei;Shen, Chuanlai
    • Journal of Microbiology and Biotechnology
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    • v.26 no.12
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    • pp.2184-2191
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    • 2016
  • The time-consuming and high-cost preparation of soluble peptide-major histocompatibility complexes (pMHC) currently limits their wide uses in monitoring antigen-specific T cells. The single-chain trimer (SCT) of peptide-${\beta}2m$-MHC class I heavy chain was developed as an alternative strategy, but its gene fusion is hindered in many cases owing to the incompatibility between the multiple restriction enzymes and the restriction endonuclease sites of plasmid vectors. In this study, overlap extension PCR and one-step cloning were adopted to overcome this restriction. The SCT gene of the $OVA_{257-264}$ peptide-$(GS_4)_3-{\beta}2m-(GS_4)_4-H-2K^b$ heavy chain was constructed and inserted into plasmid pET28a by overlap extension PCR and one-step cloning, without the requirement of restriction enzymes. The SCT protein was expressed in Escherichia coli, and then purified and refolded. The resulting $H-2K^b/OVA_{257-264}$ complex showed the correct structural conformation and capability to bind with $OVA_{257-264}$-specific T-cell receptor. The overlap extension PCR and one-step cloning ensure the construction of single-chain MHC class I molecules associated with random epitopes, and will facilitate the preparation of soluble pMHC multimers.

Hydrogen Post-annealing Effect of (Pb0.72,La0.28)Ti0.93O3 Films Fabricated by Pulsed Laser Deposition (펄스레이저 증착법으로 제작된(Pb0.72,La0.28)Ti0.93O3박막의 수소후열처리에 관한 전기적 특성 연구)

  • 한경보;전창훈;전희석;이상렬
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.3
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    • pp.190-194
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    • 2003
  • Dielectric thin films of (P $b_{0.72}$,L $a_{0.28}$) $Ti_{0.93}$ $O_3$ (PLT(28)) have been deposited on Pt(111)/Ti/ $SiO_2$/Si(100) substrates in-situ by pulsed laser deposition using different annealing and deposition Processes. We have investigated the effect of hydrogen annealing on the ferroelectric properties of PLT thin films and found that the annealing process causes the diffusion of hydrogen into the ferroelectric film resulting in the destruction of polarization. We have tried to form the film by a two-step deposition process In order to improve electrical property. Two-step process to grow PLT films was adopted and verified to be useful to enlarge the grain size of the film and to reduce the leakage current characteristics. Structural properties and electrical properties including dielectric constant, ferroelectric characteristics, and leakage current of PLT thin films were shown to be strongly influenced by grain size. The film deposited by using two-step Process including pre-annealing treatment has a strongly(111) orientation. However, the films deposited by using single -step process with hydrogen annealing process show the smallest grain size. The film deposited by using two-step process including pre-annealing treatment shows the leakage current density of below 10$^{-7}$ A/c $m^2$ for the field of smaller than 100 kV/cm. However, the films deposited by using single-step process with hydrogen annealing process and pre-annealing process show worse leakage current density than the film deposited by using two-step process including pre-annealing treatment.tment.

Zeros and Step Response Characteristics in LTI SISO Systems with Complex Poles (복소극점을 갖는 선형시불변 단일입출력 시스템의 영점과 계단응답 특성)

  • Lee, Sang-Yong
    • Journal of Institute of Control, Robotics and Systems
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    • v.16 no.4
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    • pp.313-318
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    • 2010
  • This paper deals with the relationship between zeros and step response of the second and third order LTI (Linear Time Invariant) SISO (Single-Input and Single-Output) systems with complex poles. Although it has been known that the maximum number of local extrema is less than the number of zeros in the system with only real poles[8], some cases with complex poles are shown in this paper to have many local extrema. This paper proposes monotone nondecreasing conditions and describes the relationship between the transient response and the number of local extrema in step response with each region of zeros.

Design of Low-Input-Voltage Step-Up Converter for Single Fuel Cell (단일 연료전지 셀을 위한 저입력 전압 승압 컨버터의 설계)

  • Lim, Jeong-Gyu;Park, Jin-Ju;Chung, Se-Kyo
    • Proceedings of the KIPE Conference
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    • 2010.07a
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    • pp.152-153
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    • 2010
  • This paper presents the design of a low-input-voltage step-up converter. Such circuits can be useful for single fuel cell to generate less than 0.7V. Important issues to design it are physical volume, efficiency and start-up method. In this paper, we propose a step-up converter with a simple start-up circuit. The operation of proposed circuit is presented and the experimental results are provided to verify the feasibility of the proposed technique.

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High-Efficiency Power Conditioning System for Grid-Connected Photovoltaic Modules

  • Choi, Woo-Young;Choi, Jae-Yeon
    • Journal of Power Electronics
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    • v.11 no.4
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    • pp.561-567
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    • 2011
  • This paper presents a high-efficiency power conditioning system (PCS) for grid-connected photovoltaic (PV) modules. The proposed PCS consists of a step-up DC-DC converter and a single-phase DC-AC inverter for the grid-connected PV modules. A soft-switching step-up DC-DC converter is proposed to generate a high DC-link voltage from the low PV module voltage with a high-efficiency. A DC-link voltage controller is presented for constant DC-link voltage regulation. A half-bridge inverter is used for the single-phase DC-AC inverter for grid connection. A grid current controller is suggested to supply PV electrical power to the power grid with a unity power factor. Experimental results are obtained from a 180 W grid-connected PV module system using the proposed PCS. The proposed PCS achieves a high power efficiency of 93.0 % with an unity power factor for a 60 Hz / 120 Vrms AC power grid.

Dyeing of Cotton/Polyester Blends with Disperse Dyes in the Presence of DMDHEU/PEG (DMDHEU/PEG와 분산염료를 이용한 면/폴리에스테르 혼방직물의 염색)

  • 김은아;유효선
    • Journal of the Korean Society of Clothing and Textiles
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    • v.24 no.7
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    • pp.1025-1034
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    • 2000
  • Cotton differs from polyester in physical and chemical properties. When cotton/polyester blends are dyed, water-soluble dyes are generally used for cotton and disperse dye for polyester. Thus, two bath or one bath-two step dyeing process are usually accepted. These processes consume more energy and cost compared to a single step process. To save energy and cost, a single step dyeing and finishing is carried out with disperse dyes in the presence of a crossslinking agent. K/S values of the dyed fabrics were determined to examine the dyeing property of cotton, cotton/polyester, polyester fabrics dyed with disperse dyes in the presence of DMDHEU/PEG. The concentration of DMDHEU, molecular weight and concentration of PEG, curing time and curing temperature were varied.

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