• 분석과학
• /
• 제6권4호
• /
• pp.359-362
• /
• 1993

원자흡수분광법으로 여러 원소를 동시분석시 최적 조건을 위하여 연료의 종류, 연료의 양 및 버너 높이의 변화에 대해 10가지 원소의 흡광도를 측정하였다. Air-$C_2H_2$를 연료로 과량을 사용하고, 버너 높이가 2mm일 때 최적 흡광도를 나타내었고, 이때 10가지 원소의 상대흡광도의 평균은 73%였다.

• 약학회지
• /
• 제39권2호
• /
• pp.148-152
• /
• 1995

For comparison between the compromised experimental condition and the best conditions for each element by flame atomic absorption spectrometer, the absorbances were measured with changing the burner height and HCL current. The optimum absorbance for simultaneous analysis of 6 elements was observed at 1 mA of HCL current and at 4 mm of burner height except Cr and Co. The stability of flame atomic absorption spectrometer on each element was found to be better than 5%. To investigated the accuracy of this instrument, POSCO RM-07 as a real sample was analysed at these compromised experimental conditions and found to be better than 0.04%.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2002년도 하계학술대회 논문집 A
• /
• pp.136-138
• /
• 2002

In this paper, we propose the analysis method of the Double Circuit Simultaneous Fault. To improve the accuracy and the promptness of the coontingency analysis, we reformed the Peterson method and extended the Sherman-Morrison equation. We also used the table of trigono -metric factor of Jacobian matrix before the fault, to compute the inverse matrix needed in the loadflow calculation.

• Archives of Pharmacal Research
• /
• 제11권1호
• /
• pp.45-51
• /
• 1988

The feature of resolution enhancement by derivative operation is linked to one of the multivariate analysis, which is multiple linear regression with two options, all possible and stepwise regression. Examined samples were synthetic mixtures of 5 vitamins, thiamine mononitrate, riboflavin phosphate, nicotinamide, pyridoxine hydrochloride and ascorbic acid. All components in mixture were quantified with reasonably good accuracy and precision. Whole data processing procedure was accomplished on-line by the development of three computer programs written in APPLESOFT BASIC language.

• Maxillofacial Plastic and Reconstructive Surgery
• /
• 제32권2호
• /
• pp.126-131
• /
• 2010

Objectives: This study is aimed to determine any differences in the postoperative stability between absorbable and titanium plate systems for fixation in orthognathic surgery with simultaneous maxillomandibular procedures especially including maxillary posterior impaction and advancement. Study Design: Forty patients with dentofacial deformities were randomly assigned into titanium (4 males and 6 females) and absorbable (17 males and 13 females) fixation group. All patients had undergone surgical alterations of maxilla with posterior impaction and advancement. A comparison study of the change in the maxillary position after the simultaneous surgery was performed with 1-day, 6-months postoperative lateral cephalograms compared to preoperative lateral cephalogram by tracing. Wilcoxon rank sum test was used for statistical analysis. Result: The position of the maxilla was stable after surgery and was not changed significantly from 1 day to 6 month after the simultaneous maxillomandibular surgery both in the experimental (absorbable plates) and control (titanium plates). Conclusion: This study suggests that application of absorable plating system in the fixation of maxillary segment in the simultaneous maxillomandibular procedures, leads to a predictable short-term postoperative skeletal stability comparable to the titanium plating system. Long term follow-up and further studies will be needed.

• 한국철도학회논문집
• /
• 제14권1호
• /
• pp.24-30
• /
• 2011

최저 안전율 또는 최대 파괴확률을 기반으로 하는 기존의 사면안정해석에 대하여, 지반물성과 해석모델이 갖는 고유 불확실성을 최소화하고, 사면안정해석에서 다양한 안정해석모델과 그에 따른 파괴형상을 반영할 수 있도록 다중 파괴모드에 대한 동시 파괴확률을 고려한 사면의 신뢰성해석기법을 제안하였다. 붕괴현장조사를 통하여 현장에서 가장 빈번하게 발생하는 파괴형식을 다파괴모드로 정의하였다. 동시 파괴확률의 산정에는 체계 신뢰성해석분야에서 최근 도입된 선형계획법에 의한 최적화를 이용하였으며, 이를 통하여 여러 가지 해석모델을 신뢰성 기반으로 동시에 고려하여 해석할 수 있다. 이 방법의 적용성 평가를 위하여 기존 문헌에서 나타난 제방에 대한 신뢰성해석 결과와 비교하였다. 다중 파괴모드에 대한 동시 파괴확률을 고려한 사면의 신뢰성 해석을 적용한 결과, 전체 시스템에 대한 대한 안정성을 정량적으로 산출할 수 있음을 확인하였다.

• Journal of Astronomy and Space Sciences
• /
• 제32권1호
• /
• pp.33-38
• /
• 2015

Forbush Decreases (FD) are transient, sudden reductions of cosmic ray (CR) intensity lasting a few days, to a week. Such events are observed globally using ground neutron monitors (NMs). Most studies of FD events indicate that an FD event is observed simultaneously at NM stations located all over the Earth. However, using statistical analysis, previous researchers verified that while FD events could occur simultaneously, in some cases, FD events could occur non-simultaneously. Previous studies confirmed the statistical reality of non-simultaneous FD events and the mechanism by which they occur, using data from high-latitude and middle-latitude NM stations. In this study, we used long-term data (1971-2006) from middle-latitude NM stations (Irkutsk, Climax, and Jungfraujoch) to enhance statistical reliability. According to the results from this analysis, the variation of cosmic ray intensity during the main phase, is larger (statistically significant) for simultaneous FD events, than for non-simultaneous ones. Moreover, the distribution of main-phase-onset time shows differences that are statistically significant. While the onset times for the simultaneous FDs are distributed evenly over 24-hour intervals (day and night), those of non-simultaneous FDs are mostly distributed over 12-hour intervals, in daytime. Thus, the existence of the two kinds of FD events, according to differences in their statistical properties, were verified based on data from middle-latitude NM stations.

• 한국정밀공학회:학술대회논문집
• /
• 한국정밀공학회 2012년도 추계학술대회 논문집
• /
• pp.629-630
• /
• 2012

• 천문학회보
• /
• 제39권2호
• /
• pp.80.1-80.1
• /
• 2014

We made simultaneous surveys of 22 GHz water and 44 / 95 GHz methanol masers toward 299 high-mass protostellar objects using the Korea VLBI Network (KVN) 21-m telescope. The sources were selected from the catalog of Red MSX Source (RMS) survey. Initial selection of the sample present high-mass protostellar objects in an evolutionary phase prior to ultra-compact HII regions, which have bolometric luminosities > $10^3L_{\odot}$ but are not associated with any radio continuum emission. After the follow-up work of ongoing RMS survey, final samples contains 56 sources classified as HII regions. We performed a simultaneous survey of 22 GHz water and 44 GHz methanol masers in 2011 and then conducted a simultaneous survey of 22 GHz water and 44 / 95 GHz methanol masers in 2012. The primary scientific goals of these surveys are to investigate the relationship among the three masers and to explore the relationship between each maser and the central star or the parental dense core. The detection rates of two epochs are 42% and 38% for water, 25% and 26% for 44 GHz methanol, and 23% (2012 only) for 95 GHz methanol masers. We performed a statistical analysis on subsample associated with a large data found in literature. In this poster, we will the preliminary data analysis results and discuss the implications.

• Natural Product Sciences
• /
• 제27권4호
• /
• pp.264-273
• /
• 2021

Simultaneous quantification of multiple marker compounds in herbal medicine by high performance liquid chromatography (HPLC) analysis is still a challenge due to the complexity in various parameters to be considered and co-existing multi-components. As a case study, a reliable HPLC method for simultaneous quantification of paeoniflorin from Paeoniae Radix and decursin from Angelicae Gigantis Radix in various commercial herbal medicine was developed based on analytical quality by design (AQbD) strategy. As a first step, risk assessment was performed to select the critical method parameters (CMPs) which were decided as organic mobile phase ratio and column oven temperature. In order to evaluate the effect of the CMPs on critical method attributes (CMAs) of peak resolution and tailing, central composite design (CCD) was employed. The final chromatographic conditions were optimized as follows: column- C₁₈, 4.6 × 250 mm, 5 ㎛ particle size; mobile phase- A: acetonitrile, B: 0.1% acetic acid water; detection wavelength- 235 nm for paeoniflorin, 325 nm for decursin; column oven temperature- 25℃; flow rate- 1.0 mL/min; gradient mobile phase system as Time (min) : % A, 0:14, 25:14, 30:50, 60:50, 61:100, 65:100, 66:14, 75:14. The method was successfully validated according to the International Conference on Harmonization (ICH) guidelines and piloted for ten commercial herbal medicines.