• Nuclear Engineering and Technology
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• v.38 no.5
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• pp.405-410
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• 2006

Microstructural features and their related mechanical property changes in the 309L cladding and the heat affected zone (HAZ) of SA508 cl.3 steel were investigated through the use of TEM, tensile and small punch (SP) tests. The specimens were irradiated at 563 K up to the neutron fluences of $5.79{\times}10^{19}n/cm^2$ (>1MeV). The microstructure of the clad was mainly composed of a fcc ${\gamma}-phase$, a low percentage of bcc ${\delta}-ferrite$, and a brittle ${\sigma}-phase$. Along the weld fusion line there formed a heavy carbide precipitation with a width of $20{\sim}40{\mu}m$, showing preferential cracking during plastic deformation. The yield stress and ductile-to-brittle transition temperature (DBTT) of the irradiated clads increased. The origin of the hardening and the shift of the DBTT are discussed in terms of the irradiation-produced defect clusters of a fine size and brittle ${\sigma}-phase$.

• Journal of the korean Society of Automotive Engineers
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• v.10 no.2
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• pp.46-53
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• 1988

Effect of Notch Shape and Hardness Ratio on Characteristics of Impact Fracture in Dual Phase Steels. In this study, it is investigated the effect of notch shape and hardness ratio on the characteristics of impact fracture in dual phase steels. The impact test was carried out at the temperature range from -40.deg. C to room temperature with Instrumented Charpy Impact Tester. The main results obtained are as follows; 1, The maximum impact bending strength (.sigma.$_{max}$) increases with the tensile strength. Also, the impact energy depends on .sigma.$_{max}$. 2, In room temperature, the impact energy depends on crack-initiation energy (E$_{i}$) in case of the high hardness ratio (R=3.4), whereas depends on crack-propagation energy (E$_{p}$) in case of the low hardness ratio (R=1.8) and the dependence of crack-initiation energy of the impact characteristics decreases with increasing test temperature. These phenomena are result from the difficulty of cleavage facet formation.ion.ion.

• Corrosion Science and Technology
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• v.9 no.5
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• pp.209-215
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• 2010

To elucidate the effect of aging time on resistance to localized corrosion of hyper duplex stainless steel, a double-loop electrochemical potentiokinetic reactivation test a potentiodynamic anodic polarization test, a scanning electron microscope-energy dispersive spectroscope analysis, and a thermodynamic calculation were conducted. With an increase in aging time, sigma phases are precipitated much more than chi phases due to the meta-stable chi phase acting as a transition phase. As aging time at $850^{\circ}C$ increases, the corrosion resistance decreases owing to an increase in Cr, Mo and W depleted areas adjacent to the intermetallic phases such as sigma phases and chi phases.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.22 no.4
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• pp.178-182
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• 2012

The grain growth is very important because of its great influence on the various materials properties. Therefore, in this study, the effects of anisotropic grain boundary energy on grain growth in 2-D have been investigated with a large scale phase field simulation model on PC. A $2000{\times}2000$ grid system and the initial number of grains of about 73,000 were used in the computer simulation. The anisotropic ratio of grain boundary energy, ${\sigma}_{max}/{\sigma}_{min}$, has been varied from 1 to 3. As the anisotropy increased, the grain growth exponent, n, increased from 2.05 to 2.37. The grain size distribution showed a central plateau in the isotropic case, and was changed into no central plateau and the increasing population of very small grains in the anisotropic case, resulting from slowly disappearing grains. Finally, simulated microstructures were compared according to anisotropy.

• Journal of the Korean Society for Nondestructive Testing
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• v.24 no.1
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• pp.29-37
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• 2004

The effect of the substitution of Tungsten(W) for Molybdenum(Mo) on the creep behaviour of 22Cr-5Ni duplex stainless steel(DSS) has been investigated. Creep tests were carried out at $600^{\circ}C\;and\;650^{\circ}C$. Intermetallic ${\sigma}$ phase is precipitated during creep at $650^{\circ}C$, at which creep rupture time was much lower compared with at $600^{\circ}C$. The substitution of W for Mo in the duplex stainless steel was known to retard the formation of ${\sigma}$ phase. Minimum creep rate and creep rupture time, however, were hardly influenced by the substitution of 2wt.% W. An ultrasonic measurement for the creep specimens has been carried out for the evaluation of creep damage. The sound velocity increases propotionally with the increase of creep rupture time at $600^{\circ}C$ of creep temperature. On the contrary, the sound velocity decreases with the increase of rupture time at $650^{\circ}C$, which can be correlated with the microstructural evolution during creep.

• Magazine of the Korean Society of Agricultural Engineers
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• v.31 no.2
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• pp.66-81
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• 1989

The characteristics of resilient modulus(Mr) which dominates the life of pavement and the design of pavement were investigated on the test specimens which were cement treated and non-treated of the three different soil types. The results are summarized as follows : 1. The resilient modulus was decreased by increasing the cyclic deviator stress ($\sigma$d) , especially the resilient modulus was gradually decreased or sometimes increased when the value of ad was greater than 0.75- 1. 0kg/cm$^2$. 2. The resilient modulus was increased by increasing the homogeneous confined stress ($\sigma$do) and such phenomena were distinct on the coarse soils. 3. The resilient modulus was increased by increasing the ratio of confined stress(Kc), and this phenomena were eminent on the coarse soils too, and the higher permanent strain was showed by increasing the value of Kc. 4. In the drained cyclic triaxial compression test, the value of ad, Kc, and (Oho) was introduced by the following interrelated equations which were similar to the Mr model of Cole. Kcn/Mr=K1(J$_2$/ $\tau$oct)K2 ............. (coarse soli) Mcn/Mr=K3($\sigma$dp/ $\tau$f)k4 ...............(fine soils) 5. The stress path was not much affected by the value of Mr, however, moisture content, dry desity, and contant of fines affected the value of Mr. 6. In the soil-cement specimens, the resilient compression strain($\varepsilon$d) was decreased by the increment of the $\sigma$ho, and Mr was decreased by increasing the $\sigma$d 7. In the flexible pavement. the cement treated layer should be designed not to fail by the fatigue before the designed traffic load, and actually the pavement could cover the traffic load to a certain extent under the post-crack phase, therefore farther studies on this phenomena' are required in the design analysis. 8. The finite element computer program (ANALYS) was used for displacement analysis of pavement containing the cement-treated layer, The result showed that the program used for this analysis was proved to be usable.

• Korean Journal of Metals and Materials
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• v.50 no.10
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• pp.735-743
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• 2012

The aim of this study was to analyze the effect of the cooling rate after heat treatment on the microstructure and mechanical properties of 2507 duplex stainless steels. Heat treatment was carried out at $1050^{\circ}C$ for 1 hr, followed by controlled cooling. The cooling rates were $175.6{\times}10^{-3}^{\circ}C/s$, $47.8{\times}10^{-3}^{\circ}C/s$, $33.3{\times}10^{-3}^{\circ}C/s$, $16.7{\times}10^{-3}^{\circ}C/s$, $11.7{\times}10^{-3}^{\circ}C/s$, $5.8{\times}10^{-3}^{\circ}C/s$ and $2.8{\times}10^{-3}^{\circ}C/s$, which resulted in variations of the microstructure, such as the fractional change of the ferrite phase and sigma phase formation. Fatigue, hardness, impact and tensile tests were performed on the specimens with different cooling rates. The precipitation of the ${\sigma}$ phase caused a hardness increase and a sharp decrease of toughness and tensile elongation. The fatigue limit of the sample with a cooling rate of $5.8{\times}10^{-3}^{\circ}C/s$ was 26 MPa higher than that of the sample with a cooling rate of $175.6{\times}10^{-3}^{\circ}C/s$. Our observations of the fracture surface confirmed that the higher fatigue resistance of the specimen with a cooling rate of $5.8{\times}10^{-3}^{\circ}C/s$ was caused by the delay of the fatigue crack growth, in addition to higher yield strength.

• Proceedings of the KWS Conference
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• v.43
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• pp.174-176
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• 2004

The duplex stainless clad vessel with 38m & over thickness shall be performed to PWHT based on the ASME code. In this case, it is well-known that precipitators such as carbides and sigma($\sigma$) phase are formed at gram boundary between ferrite and austenite phase. Therefore, a weld test for simulating this situation has been planned and performed by 3309LMo71-1 for barrier layer and E2209Tl-1 for 2nd & over layer and then carried out to investigate the overlaid weld metal. Based on the test results, it could be concluded that PWHT should be carried out after the completion of 1st(barrier) layer and then 2 & over layer should be applied.

• Proceedings of the KIEE Conference
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• 2005.10b
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• pp.436-438
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• 2005

본 논문에서는 전력선 위상 측정을 위해 A/D 변환기 및 위상계측 연산장치를 집적한 하이브리드 센서칩의 구현 기법을 제시하였다. 개발한 위상계측 연산장치는 recursive sliding-DFT에 기반하였으며 곱셈기의 시분할 공유 구조를 사용하여 칩의 구현 면적을 최소화 하였다. 60Hz의 전력선 신호를 중심주파수로 하는 AD 변환장치는 sigma-delta ADC를 기반으로 하여 8-bit 정밀도를 제공하며 아날로그부의 구현을 최소화하도륵 설계하였다. 설계한 하이브리드 센서칩은 컴퓨터 시뮬레이션 및 FPGA 구현을 통해 동작을 검증하였으며, 검증 완료후 $0.35{\mu}m$ CMOS 공정기술로 구현하였다. 전력선 위상을 측정하기 위해 구현된 4채널 하이브리드 센서 칩의 설계면적은 $5{\times}5m^2$ 의 약 20%정도를 차지하였다.

• Proceedings of the KWS Conference
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• 2004.05a
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• pp.156-158
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• 2004

The microstructural evolution in a 304 stainless steel weld during FSW was examined. The SZ and TMAZ showed typical dynamically recrystallized and recovered microstructures, respectively, The microstructural observation revealed that sigma phase was formed at the advancing side of the stir zone. A possibility was suggested that the rapid formation of the sigma phase is related to the transformation of austenite to delta-ferrite in the stir zone, from introduction of high strain and dynamic recrystallization during FSW.