• 제목/요약/키워드: shrinkage rate

검색결과 453건 처리시간 0.026초

Densification of Reaction Bonded Silicon Nitride with the Addition of Fine Si Powder - Effects on the Sinterability and Mechanical Properties

  • Lee, Sea-Hoon;Cho, Chun-Rae;Park, Young-Jo;Ko, Jae-Woong;Kim, Hai-Doo;Lin, Hua-Tay;Becher, Paul
    • 한국세라믹학회지
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    • 제50권3호
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    • pp.218-225
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    • 2013
  • The densification behavior and strength of sintered reaction bonded silicon nitrides (SRBSN) that contain $Lu_2O_3-SiO_2$ additives were improved by the addition of fine Si powder. Dense specimens (relative density: 99.5%) were obtained by gas-pressure sintering (GPS) at $1850^{\circ}C$ through the addition of fine Si. In contrast, the densification of conventional specimens did not complete at $1950^{\circ}C$. The fine Si decreased the onset temperature of shrinkage and increased the shrinkage rate because the additive helped the compaction of green bodies and induced the formation of fine $Si_3N_4$ particles after nitridation and sintering at and above $1600^{\circ}C$. The amount of residual $SiO_2$ within the specimens was not strongly affected by adding fine Si powder because most of the $SiO_2$ layer that had formed on the fine Si particles decomposed during nitridation. The maximum strength and fracture toughness of the specimens were 991 MPa and $8.0MPa{\cdot}m^{1/2}$, respectively.

후육 구상흑연주철의 이상흑연 제어 (Control of Abnormal graphite Structure in Heavy Section Ductile Cast Iron)

  • 이상목;신호철;신제식;문병문
    • 한국주조공학회지
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    • 제25권1호
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    • pp.40-50
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    • 2005
  • A series of heavy section ductile cast iron ingots with the cube length of 250mm were systematically investigated as functions of casting parameters of sand casting. Abnormal graphite formation was specially observed with the variation of Si content and Bi or Sb addition. Effects of chilling during casting and adaptation of riserless system were also examined, and proved to be effective for the prevention of both shrinkage and abnormal graphite such as chunky one. The formation of chunky graphite was effectively prevented by low Si content despite the promotion of pearlite matrix structure. The ferritic matrix was encouraged to form by high Si content and chunky graphite formation was effectively suppressed by the addition of Bi and Sb. Bi addition, however, was not good enough to control the microstructure owing to the sensitive cooling rate dependent inoculation behavior and relative low ability of nodulization. Sb addition, on the other hand, was proved to be effective for the microstructural control and enhancement of various mechanical properties such as strength, elongation, and impact energy. It may be suggested that optimized casting parameters should be applied to produce heavy section ductile cast iron with reliability.

Evaluation in Physiomechanical Characteristics of Carbonized Oriented Strand Board by Different Carbonizing Conditions

  • Lee, Min;Park, Sang-Bum;Lee, Sang-Min;Son, Dong-Won
    • Journal of the Korean Wood Science and Technology
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    • 제42권2호
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    • pp.163-171
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    • 2014
  • Environmental issues about indoor air quality have been increased and focused on volatile organic compounds (VOCs) caused cancer, asthma, and skin disease. Reducing VOCs has been attempted in many different methods such as using environmentally friendly materials and air cleaner or purifier. Charcoal is well known material for absorbing VOCs. Therefore, carbonized board from medium density fiberboard has been developed. We assumed that the source of carbonized boards can be any type of wood-based panels. In this study, carbonized boards were manufactured from oriented strand board (OSB) at 400, 600, 800, and $1000^{\circ}C$. Each carbonized OSB (c-OSB) was evaluated and determined physiomechanical characteristics such as exterior defects, dimensional shrinkage, modulus of elasticity, and bending strength. No external defects were observed on c-OSBs at all carbonizing conditions. As carbonizing temperature increased, less porosity between carbonized wood fibers was observed by SEM analysis. The higher rate of dimensional shrinkage was observed on c-OSB at $1000^{\circ}C$ (66%) than c-OSB at 400, 600, and $800^{\circ}C$ (47%, 58%, and 63%, respectively). The densities of c-OSBs were lower than original OSB, but there was no significant different among the c-OSBs. The bending strength of c-OSB increased 1.58 MPa (c-OSB at $400^{\circ}C$) to 8.03 MPa (c-OSB at $1000^{\circ}C$) as carbonization temperature increased. Carbonization temperature above $800^{\circ}C$ yielded higher bonding strength than that of gypsum board (4.6 MPa). In conclusion, c-OSB may be used in sealing and wall for decorating purpose without additional artwork compare to c-MDF which has smooth surface.

플라스마 디스플레이 패널의 격벽용 BaO-B2O3-ZnO-P2O5계의 HNO3를 이용한 에칭 특성 (HNO3 Etching Properties of BaO-B2O3-ZnO-P2O5 System of Barrier Ribs in PDP)

  • 전재삼;김재명;김남석;김형순
    • 한국재료학회지
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    • 제16권4호
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    • pp.235-240
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    • 2006
  • We investigated the effect of ZnO filler on the microstructure of $BaO-B_2O_3-ZnO-P_2O_5$ glass system to find an etching mechanism of barrier ribs. The sintering behavior of composites heated in the temperature range $560-600^{\circ}C$ was studied by volumetric shrinkage rate and microstructure. The etching test was carried out in $HNO_3$ solution at $50^{\circ}C$ for 10 min. The volumetric shrinkage of sintered sample decreased with the increased firing temperature because of the formation of two crystals. Glass and ZnO filler react forming the $BaZn_2(PO_4)_2$ crystal phases during the sintering process. Etching phenomenon of sintered samples by $HNO_3$ showed that the $BaZn_2(PO_4)_2$ crystal phase was strongly leached compared to glass matrix, crystal phases and fillers. Therefore, the control of interface by condition of sintering is so important to achieve etching effect in barrier ribs.

기계편용 장식사 니트소재의 물성 및 감성 평가 (Physical and Hand Properties of the Knitted Fabrics From Machine Knitting Fancy Yarns)

  • 박기윤;박명자
    • 한국의상디자인학회지
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    • 제10권2호
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    • pp.125-138
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    • 2008
  • For physical and hand property evaluation of fabrics, the knitted fabrics from 11 types of machines knitting fancy yarns, boucle (M1), knot (M2), snarl (M3), and slub (M4), tamtam (M5), tubular (M6), fur 1 (M7), bead (M8), fur 2 (M9), fur 3 (M10), and ladder (M11) yarns, were prepared with 7-10 G plain stitch. Washing test and pilling test had also been carried out. For hand properties by objective sensibility evaluation, 17 items of sir mechanical properties using KES-FB (Kawabata Evaluation System) had been measured. Then hand values of knitted fabrics were calculated with a calculation formula, namely KN-402-KT. Finally the total hand values were obtained through KN-301-WINTER. As a result of physical properties and objective evaluation for machines knitting fancy fabrics, most of them shrank in the direction of wale and course after the washing test, in which their shrinkage rate had a maximum of 3.5%. Therefore, the washing test indicated that the shrinkage ratio of knitted fabrics had a minor change. The results of the pilling test are mostly 4-5th grade, and all of the machines knitting fancy fabrics showed good results in the pilling resistance. In hand properties and objective sensibility evaluation, twisted fancy yarns, such as boucle (M1), knot (M2), snarl (M3), and slub (M4), were superior to bonding rigidity (B) and shear rigidity (G). The surface property between course and wale differs in all samples and course direction is tougher than wale direction. FUKURAMI (fullness and softness) of all samples have high values, besides NUMERI (smoothness) of tamtam (M5) and boucle (M1), which were rather good. Most samples except fur 1 (M7) had low KOSHI (stiffness) value. The total hand value (THV) of twisted yarns was low. This study proves that manufacturers, who plan knitting yarn products and knit fashion, can apply these data to develop machines knitting yarns and knits that fit the consumers' demands.

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치아 와동의 복합레진 수복시 음향방출의 시간적 발생 특성 (Time-Based Characteristics of Acoustic Emission During Dental Composite Restoration)

  • 구자국;최낙삼
    • 대한기계학회논문집A
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    • 제35권2호
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    • pp.169-174
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    • 2011
  • 제 1 급 와동이 모사된 비관통형 치아 시편에 수복된 복합레진의 중합 수축시 발생하는 AE 신호를 실시간으로 검출한 후 이를 분석하였다. 시간대별 발생 분포를 살펴보면, 광조사 초기에 중합 수축이 급격히 진행되는 제 I 구간에서 AE event 가 많이 관찰되었다. 제 I구간 후 AE event 발생 빈도가 낮아져 AE 가 별로 관찰되지 않은 제II구간이 있었는데, AE 신호의 발생이 적은 PMMA 는 치아에 비해 구간이 길었으며 AE 검출이 잦았던 스테인리스스틸 모형은 제 II 구간이 짧았다. AE 활성도를 나타내는 구간 특성은 수복재와 와동의 계면부에서 일어나는 균열의 발생빈도를 나타내는 것으로 사료되며 젤화점 직후의 제I 구간에서 AE 가 집중적으로 관측되는 바, 수복재와 와동 사이의 갭 형성은 바로 젤화점 직후에 만들어졌음을 가리킨다. 신호의 최대 진폭은 25-45dB 이었고 1 차 중심 주파수는 100-200kHz 와 240-400kHz 영역의 신호들이 발생하였으며 이는 레진이나 접착층의 파괴에 해당하였다.

Reassessment of viscoelastic response in steel-concrete composite beams

  • Miranda, Marcela P.;Tamayo, Jorge L.P.;Morsch, Inacio B.
    • Structural Engineering and Mechanics
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    • 제81권5호
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    • pp.617-631
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    • 2022
  • In this paper the viscoelastic responses of four experimental steel-concrete composite beams subjected to highly variable environmental conditions are investigated by means of a finite element (FE) model. Concrete specimens submitted to stepped stress changes are also evaluated to validate the current formulations. Here, two well-known approaches commonly used to solve the viscoelastic constitutive relationship for concrete are employed. The first approach directly solves the integral-type form of the constitutive equation at the macroscopic level, in which aging is included by updating material properties. The second approach is postulated from a rate-type law based on an age-independent Generalized Kelvin rheological model together with Solidification Theory, using a micromechanical based approach. Thus, conceptually both approaches include concrete hardening in two different manners. The aim of this work is to compare and analyze the numerical prediction in terms of long-term deflections of the studied specimens according to both approaches. To accomplish this goal, the performance of several well-known model codes for concrete creep and shrinkage such as ACI 209, CEB-MC90, CEB-MC99, B3, GL 2000 and FIB-2010 are evaluated by means of statistical bias indicators. It is shown that both approaches with minor differences acceptably match the long-term experimental deflection and are able to capture complex oscillatory responses due to variable temperature and relative humidity. Nevertheless, the use of an age-independent scheme as proposed by Solidification Theory may be computationally more advantageous.

회수수를 사용한 3성분계 경량 골재 모르타르의 공학적 특성에 관한 실험적 연구 (An Experimental Study on the Engineering Characteristics of Ternary Lightweight aggregate Mortar Using Recycling Water)

  • 이재인;배성호;김지환;최세진
    • 한국건설순환자원학회논문집
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    • 제10권1호
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    • pp.48-55
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    • 2022
  • 본 연구는 콘크리트의 운반 과정 중 발생하는 레미콘 회수수의 재활용율 증대 및 온실가스 저감을 위한 연구의 일환으로 회수수를 배합수 및 인공경량골재 프리웨팅수로 사용하고 고로슬래그 미분말 및 플라이애시를 시멘트 대체재로 사용한 3성분계 경량 골재 모르타르의 공학적 특성을 검토하였다. 이를 위해 3성분계 경량 골재 모르타르의 플로우, 기건단위질량, 압축강도, 건조수축, 중성화 깊이, 염화물 이온 침투 저항성을 측정하였으며 측정 결과 회수수를 사용할 경우 높아진 알칼리도에 의해 시멘트계 재료들의 반응성이 높아졌으며 3성분계 배합과 함께 사용할 경우 고로슬래그 미분말 15 %, 플라이애시를 5 % 사용할 시 모르타르의 압축강도 및 내구특성 향상에 긍정적인 것으로 나타났다.

Preparation and Performance of Aluminosilicate Fibrous Porous Ceramics Via Vacuum Suction Filtration

  • Qingqing Wang;Shaofeng Zhu;Zhenfan Chen;Tong Zhang
    • 한국재료학회지
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    • 제34권1호
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    • pp.12-20
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    • 2024
  • This study successfully prepared high-porosity aluminosilicate fibrous porous ceramics through vacuum suction filtration using aluminosilicate fiber as the primary raw material and glass powder as binder, with the appropriate incorporation of glass fiber. The effects of the composition of raw materials and sintering process on the structure and properties of the material were studied. The results show that when the content of glass powder reached 20 wt% and the samples were sintered at the temperature of 1,000 ℃, strong bonds were formed between the binder phase and fibers, resulting in a compressive strength of 0.63 MPa. When the sintering temperatures were increased from 1,000 ℃ to 1,200, the open porosity of the samples decreased from 89.08 % to 82.38 %, while the linear shrinkage increased from 1.13 % to 10.17 %. Meanwhile, during the sintering process, a large amount of cristobalite and mullite were precipitated from the aluminosilicate fibers, which reduced the performance of the aluminosilicate fibers and hindered the comprehensive improvement in sample performance. Based on these conditions, after adding 30 wt% glass fiber and being sintered at 1,000 ℃, the sample exhibited higher compressive strength (1.34 MPa), higher open porosity (89.13 %), and lower linear shrinkage (5.26 %). The aluminosilicate fibrous porous ceramic samples exhibited excellent permeability performance due to their high porosity and interconnected three-dimensional pore structures. When the samples were filtered at a flow rate of 150 mL/min, the measured pressure drop and permeability were 0.56 KPa and 0.77 × 10-6 m2 respectively.

식품의 건조 및 수축특성에 관한 연구 - 2. 다시마의 건조 및 수축특성에 영향을 미치는 인자 - (Drying and Shrinking Characteristics of Food 2. Influencing Factors in Drying and Shrinking Characteristics of Sea Tange)

  • 조덕제;허종화;정수열
    • 한국수산과학회지
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    • 제21권1호
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    • pp.16-20
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    • 1988
  • 다시마의 건조와 수축특성을 알기위한 기초자료를 얻고자 건조중인 다시마의 건조 및 수축특성에 미치는 채취부위, 공기의 온도, 상대습도 및 풍속의 영향에 관하여 실험한 결과를 요약하면 다음과 같다. 1) 다시마의 열풍건조과정은 항률건조 기간이 없이 바로 감률건조기가 나타났으며 이것은 다시 감률건조 1단계 및 2단계로 구분되었다. 2) 두께가 얇은 선단부가 기부보다 수축이 더 많이 되었으며 공기의 온도 $50^{\circ}C$, 상대습도 $30\%$, 유속 0.4m/s의 일정한 건조 조건하에서 다시마의 선단부, 중간부 및 기부를 120분까지 건조하였을 경우 수축율은 각각 $57.5\%,\;54.0\%,\;42.7\%$이었다. 3) 상대습도가 낮은것은 높은것에 비해 건조속도 및 수축속도는 빨랐으나 함수률 $20\%$까지 건조하였을 경우 수축율은 오히려 상대습도가 높은것이 증가하였다.

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