• 제목/요약/키워드: sessile drop method

검색결과 30건 처리시간 0.01초

Glycerol dimethacrylate를 포함한 고습윤성 안의료용 고분자의 중합 및 특성 (Polymerization and Characterization of Ophthalmic Polymer Containing Glycerol dimethacrylate with High Wettability)

  • 조선아;김태훈;성아영
    • 대한화학회지
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    • 제55권2호
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    • pp.283-289
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    • 2011
  • 본 연구는 glycerol dimethacrylate를 교차결합제인 EGDMA(ethylene glycol dimethacrylate)와 HEMA(2-hydroxyethyl methacrylate), MMA(methyl methacrylate), MA(methacrylic acid) 그리고 개시제인 AIBN(azobisisobutyronitrile)과 함께 공중합 하였다. 생성된 고분자의 물리적 특성을 측정한 결과, 함수율 22~32%, 굴절률 1.442~1.463, 가시광선 투과율 90.0~90.5% 그리고 접촉각의 경우 56~$65^{\circ}$ 범위의 분포를 나타내었다. 또한 sessile drop method에 의한 공중합체의 접촉각을 측정한 결과 glycerol dimethacrylate의 함량이 증가할수록 9.89~$18.99^{\circ}$ 감소한 결과를 보였다. 본 실험결과로 볼 때 생성된 공중합체는 습윤성이 높은 안의료용 렌즈 재료로 사용될 수 있을 것으로 판단된다.

귀금속(금, 은)-유리계의 젖음성과 부착성 (Wettability and Adhesion of Noble Metal (Au, Ag)-Glass Systems)

  • 김종희
    • 한국세라믹학회지
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    • 제32권4호
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    • pp.405-412
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    • 1995
  • In order to estimate the wettability of the borosilicate glasses with different composition on the noble metals of gold and silver, the measurements of the contact angle between the solid and the liquid were made at various temperatures and holding times using the sessil-drop method. The wetting behavior and the adhesion of the phases were strongly influenced by the thermal or the physical characteristics of the materials. The dependence of wetting angle ($\theta$) on the holding time (t) could be represented by the relation of $\theta$=a.tb, whereby the wettability of the systems was quantitatively compared. Also with increasing content of borosilicate glass in the glass-gold matrix composite, the tensile strength was decreased whereas the elastic modulus was increased.

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레벨셋 기법을 이용한 전기습윤 현상의 동적 거동에 대한 해석 (ANALYSIS OF ELECTROWETTING DYNAMICS WITH CONSERVATIVE LEVEL SET METHOD)

  • 박준권;홍지우;강관형
    • 한국전산유체공학회:학술대회논문집
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    • 한국전산유체공학회 2009년 추계학술대회논문집
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    • pp.84-87
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    • 2009
  • Electrowetting is a versatile tool to handle tiny droplets and forms a backbone of digital microfluidics. Numerical analysis is necessary to fully understand the dynamics of electrowetting, especially in designing electrowetting-based devices, such as liquid lenses and reflective displays. We developed a numerical method to analyze the general contact-line problems, incorporating dynamic contact angle models. The method is based on the conservative level set method to capture the interface of two fluids without loss of mass. We applied the method to the analysis of spreading process of a sessile droplet for step input voltages and oscillation of the droplet for alternating input voltages in electrowetting. The result was compared with experimental data. It is shown that contact line friction significantly affects the contact line motion and the oscillation amplitude. The pinning process of contact line was well represented by including the hysteresis effect in the contact angle models.

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나노섬유의 특성분석을 위한 레이저 접촉각 측정기의 효율성 연구 (Feasibility Study of Laser Contact Angle Measurement for Nano-fiber Characterization)

  • 신경인;안선훈;김성훈
    • 한국의류학회지
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    • 제27권5호
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    • pp.554-559
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    • 2003
  • A newly developed contact angle measurement instrument by laser beam projection allows for rapid and direct determination of contact angles. The instrument may have a possibility to characterize newly developed nano-fibers. When the laser beam impinges on an edge of an interface of liquid and solid, projected beam were split across and made two straight lines on a tangent screen. From the result, it could measure the contact angle directly by reading the angle between two split beams. The purpose of this study was to prove reliability and reproducibility of the contact angle measurement instrument by laser beam projection compare to the conventional one by microscope through the comparative experiment and questionnaire. Test samples were selected by consideration of hydrophilic and hydrophobic, such as nylon 6 and polypropylene, respectively. The laser contact angle measurement has accurate, fast and convenient method to measure contact angle, and it can be a unique method to characterize nano-fibers.

타이타늄 표면 처리 특성에 따른 젖음성에 관한 연구 (Wettability of titanium implants depending upon surface properties)

  • 한영수;신상완
    • 대한치과보철학회지
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    • 제47권1호
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    • pp.12-20
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    • 2009
  • 연구목적: 임플란트가 식립되어질 때 매식체는 조직액과 접촉하게 된다. 임플란트의 조직액 흡착은 표면처리에 따라 다양하게 나타난다. 이 때 임플란트 시편의 표면 거칠기와 젖음성과의 상관관계를 분석하고자 하였다. 연구재료 및 방법: 표면 거칠기와 젖음성의 상관관계를 측정하기 위해 네 종류의 임플란트 시편을 각각 5종류 만들었다. 각각의 그룹은 그룹 A: Machined Surface, 그룹 B: Anodized surface, 그룹 C: RBM (HA blasting) surface, 그룹 D: CMP (calcium methaphosphate) coating surface이다. 연구결과: 1. 표면의 거칠기는 RBM, CMP, Anodized, Machined 그룹 순서로 거칠었다. RBM과 CMP는 통계적으로 유의차가 없었다 (P<.05). 2. 젖음성은 Anodized, RBM, CMP, Machined 그룹 순서로 높았다. CMP와 Machined는 통계적으로 유의차가 없었다 (P<.05). 3. 표면 거칠기와 젖음성과의 상관관계는 없었다.

SiO$_2$-CaO-Al$_2$O$_3$계 유리 솔더에 의한 알루미나의 접합 현상에 관한 연구 (A Study for Joining of Alumina Soldered by SiO$_2$-CaO-A1$_2$O$_3$ Glasses)

  • 안병국
    • Journal of Welding and Joining
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    • 제21권2호
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    • pp.35-41
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    • 2003
  • Sintered alumina ceramics were joined by 2 kinds of SiO$_2$-CaO-A1$_2$O$_3$ glass solders having a similar expansivity as alumina. Wetting of glass/alumina was examined by sessile drop method. The observation of interface and bending strength related to alumina/glass/alumina systems were investigated by means of SEM/EDX and 4-point bending test. the result are summarized as follow: (1) Wetting of glass solders on alumina was good at temperatures higher than 145$0^{\circ}C$. (2) When the joining temperature wan high, diffusion and/or reactions between solder md alumina took place at the interface. These diffusions and reactions occurring at the interface greatly affected the bending strength of joining body. (3) Highest strength corresponding to 80% that of alumina was obtained by the solder of 35SiO$_2$-35CaO-30A1$_2$O$_3$(wt%) glass.

세라믹 기판에 대한 저온 용융프릿트의 침윤 거동 (Wetting Behavior of Low Temperature Molten Frits on Various Ceramic Substrates)

  • 노태준;오근호;이종근;김대웅
    • 한국세라믹학회지
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    • 제20권3호
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    • pp.199-204
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    • 1983
  • An attempt was made to study wetting behavior of various low temperature molten frist on ceramic substrates including high alumina silicon carbide and porous fired clay plates by Sessile-drop method. The cosine values of contact angles between substrates and molten frist were linear as a function of temperature unless chemical reactions between substrate and molten frit occured. Addition of BaO to frit composition indicated that cosine of values of contact angles were gradually increased with increasing temperature but in the frist contained $Li_2O$ consine values were abruptly increased with increasing temperature after reached a certain temperature. The contact angle increased with increasing roughness of the substrate surface in case of alumina substrate plate.

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텅스텐판상에서 구리액상의 습윤거동에 미치는 온도 및 니켈 첨가의 효과 (The Effcts of Temperature and Ni Addition on the Wetting Behaviour of Cu on W)

  • 이재성
    • 한국표면공학회지
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    • 제16권2호
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    • pp.41-47
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    • 1983
  • An investigation has been performed on the effects of temperature and Ni addition on the wetting behaviour of Cu on W substrate in hydrogen atmosphere. An sessile drop method was used to measure a wetting angle. The concentration profiles of W, Cu and Ni elements in W/Cu - 5 Ni specimen were made by EPMA. With increasing temperature, the wetting angle of Cu droplet on W plate decreases and the time to reach an equilibrium wetting angle is shortened in hydrogen atmosphere. The addition of Ni improves appreciably the wettability of Cu on W. With increasing Ni content in Cu liquid droplet(0, 1, 3, 5%), the wetting angle is decreased from 21$^{\circ}$to 0$^{\circ}$.

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Evaluation of Dynamic Wettability of Liquid Zn with Steel Sheets Containing Si and Mn

  • Tanaka, Toshihiro
    • Corrosion Science and Technology
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    • 제9권2호
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    • pp.87-91
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    • 2010
  • It is pointed out that non-wetting behavior of liquid Zn alloy occurs on high-tensile strength steels, which usually contain Si and Mn. There have been a lot of investigations to improve the above wettability of liquid Zn alloy with steels containing Si and Mn. Although those studies evaluated the wettability qualitatively by observation of the surface of steels galvanized by Zn or exfoliation test of Zn with substrate steels and so on, it is required to evaluate the wettability of liquid Zn with steels by measuring contact angle, work of adhesion, spreading velocity etc. which are usually used to assessment of general wetting behavior. In the present work, we evaluated the wettability of liquid Zn with steels containing Si and Mn by applying a sessile drop method to measure the change in contact angle and diameter of liquid Zn droplet wetted on steels.

캐니 에지 검출 알고리즘을 이용한 접촉각 측정 기법 (A Contact Angle Measurement Method using Canny Edge Detect Algorithm)

  • 윤여빈;송재오;전진환;이상문
    • 한국컴퓨터정보학회:학술대회논문집
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    • 한국컴퓨터정보학회 2016년도 제53차 동계학술대회논문집 24권1호
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    • pp.251-252
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    • 2016
  • 접촉각을 이용한 표면에너지 측정방법은 부품소재분야를 비롯한 폴리머 화학제품 등에서 널리 사용되고 있다. 그중 측정할 대상의 고체 표면에 액체 방울을 떨어뜨리고 측면 접점 방향에 대한 영상을 촬영하여 고체 표면과 액체 방울이 이루고 있는 각도를 측정하는 방식을 가장 많이 사용하고 있다. 본 논문에서는 기존 접촉각 측정기의 배경과 액체 방울 사이의 명암 차를 이용하여 경계선을 찾는 Sessile-drop 영상처리 기법을 보완 및 개선하기 위하여 캐니 에지 검출 알고리즘을 적용하였다.

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