• Title/Summary/Keyword: secondary phase

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Microencapsulation of Caramel Flavor and Properties of Ready-to-drink Milk Beverages Supplemented with Coffee Containing These Microcapsules

  • Kim, Gur-Yoo;Lee, Jaehak;Lim, Seungtae;Kang, Hyojin;Ahn, Sung-Il;Jhoo, Jin-Woo;Ra, Chang-Six
    • Food Science of Animal Resources
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    • v.39 no.5
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    • pp.780-791
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    • 2019
  • This study aimed to extend the retention of flavor in coffee-containing milk beverage by microencapsulation. The core material was caramel flavor, and the primary and secondary coating materials were medium-chain triglyceride and maltodextrin, respectively. Polyglycerol polyricinoleate was used as the primary emulsifier, and the secondary emulsifier was polyoxyethylene sorbitan monolaurate. Response surface methodology was employed to determine optimum microencapsulation conditions, and headspace solid-phase microextraction was used to detect the caramel flavor during storage. The microencapsulation yield of the caramel flavor increased as the ratio of primary to secondary coating material increased. The optimum ratio of core to primary coating material for the water-in-oil (W/O) phase was 1:9, and that of the W/O phase to the secondary coating material was also 1:9. Microencapsulation yield was observed to be approximately 93.43%. In case of in vitro release behavior, the release rate of the capsules in the simulated gastric environment was feeble; however, the release rate in the simulated intestinal environment rapidly increased within 30 min, and nearly 70% of the core material was released within 120 min. The caramel flavor-supplemented beverage sample exhibited an exponential degradation in its flavor components. However, microcapsules containing flavor samples showed sustained flavor release compared to caramel flavor-filled samples under higher storage temperatures. In conclusion, the addition of coffee flavor microcapsules to coffee-containing milk beverages effectively extended the retention of the coffee flavor during the storage period.

Effect of Morphological Control of Secondary Phase using Yb2O3 and Ca-Al-Si-O-based Glass on Thermal and Mechanical Properties of AlN (CAS glass와 Yb2O3를 이용한 2차상의 형상 제어가 AlN 세라믹의 열전도도 및 기계적 특성에 미치는 영향)

  • Choi, Dong Kyu;Kim, Shi Yeon;Yeo, Dong Hun;Shin, Hyo Soon;Jeong, Dae Yong
    • Journal of Powder Materials
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    • v.27 no.6
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    • pp.498-502
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    • 2020
  • We investigate the effects of Yb2O3 and calcium aluminosilicate (CAS) glass as sintering additives on the sintering behavior of AlN. The AlN specimens are sintered at temperatures between 1700℃ and 1900℃ for 2 h in a nitrogen atmosphere. When the Yb2O3 content is low (within 3 wt.%), an isolated shape of secondary phase is observed at the AlN grain boundary. In contrast, when 3 wt.% Yb2O3 and 1 wt.% CAS glass are added, a continuous secondary phase is formed at the AlN grain boundary. The thermal conductivity decreases when the CAS glass is added, but the sintering density does not decrease. In particular, when 10 wt.% Yb2O3 and 1 wt.% CAS glass are added to AlN, the flexural strength is the highest, at 463 MPa. These results are considered to be influenced by changes in the microstructure of the secondary phase of AlN.

Enable Secondary User Spectrum Access in Cooperative Communication Scheme with Rayleigh Fading Channel (레일리 페이딩 채널에서 2차 사용자 스펙트럼 접근이 가능한 협력통신 기법)

  • Kim, Lyum;Kong, Hyung-Yun
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.10 no.5
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    • pp.113-119
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    • 2010
  • In this paper, the considered cognitive radio system has a pair of PT-PR and a pair of ST-SR. In first time slot(1 Phase), PT broadcast signal $x_p$ to PR, ST and SR. Then, each receivers(PR, ST, SR) decode received signal $x_p$. In second time slot(2 Phase), ST combine decoded signal ${x_p}^{\prime}$ and signal $x_s$, and it broadcast combined signal to PR and SR. PR and SR decode combined signal. At this time, PR can achieve diversity gain, due to using MRC, it combine 'received and decoded signal ${x_p}^{\prime}$ at 1 phase' and 'detected signal $x_p$ at 2 phase'. SR use linear combining technique and it can obtain $x_s$.

Sintering and Microwave Dielectric Properties Of Ba2Ti9O20 Ceramics Prepared by Precursor Method

  • Sung, Je-Hong;Lee, Joon-Hyung;Kim, Jeong-Joo;Lee, Hee-Young;Cho, Sang-Hee
    • Journal of the Korean Ceramic Society
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    • v.40 no.4
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    • pp.365-370
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    • 2003
  • The phase development process of $Ba_2$ $Ti_{9}$ $O_{20}$ ceramics is not clearly known and frequently accompanies second phases which deteriorate dielectric properties. In synthesizing $Ba_2$ $Ti_{9}$ $O_{20}$ ceramics, in order to trace the reaction sequence during conventional solid-state reaction in BaO-Ti $O_2$ system, different barium sources of BaC0$_3$ and BaTi0$_3$ precursor were used as starting materials. From the analysis of XRD patterns, different secondary phases could be identified depending on the barium source used, which might mean that the equilibrium phases in BaO-Ti $O_2$ system are very difficult to be synthesized. Because the BaTi0$_3$ precursor provides short diffusion paths of ions, the system revealed less secondary phases during solid state reaction. In synthesizing BaO-xSm$_2$0$_3$-4.5Ti0$_2$ system using different barium sources, different secondary phases were developed also. Microstructure and dielectric properties were examined and discussed in terms of secondary phase development.

Analysis of Wall-Thinning Effects Caused by Power Uprates in the Secondary System of a Nuclear Power Plant (원전 2차계통의 출력증강 운전에 따른 배관감육 영향 분석)

  • Yun, Hun;Hwang, Kyeongmo;Lee, Hyoseoung;Moon, Seung-Jae
    • Corrosion Science and Technology
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    • v.15 no.3
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    • pp.135-140
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    • 2016
  • Piping and equipment are degraded by flow-accelerated corrosion (FAC) in nuclear power plants. FAC causes numerous problems and nuclear utilities maintain programs to control FAC. The key parameters influencing FAC are hydrodynamic conditions, water chemistry, and effect of materials. Recently, a nuclear utility has planned slight power uprates in Korea. Operating conditions need to be changed in the secondary system according to power uprates. This study analyzed the effect of wall-thinning caused by power uprates. The change of operation data in the secondary cycle is reviewed, and wall-thinning rates are analyzed in the main lines. As a result, two phase (mixture of water and steam) lines have a greater impact than a water line under power uprate conditions. Also, the quality of steam is the most important factor for FAC in two phase lines.

MOVPE of ZnSe with DIPSe and DMZn

  • Soo, Huh-Jeung;Ok, Lim-Jeong
    • Journal of Korean Vacuum Science & Technology
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    • v.2 no.2
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    • pp.118-121
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    • 1998
  • Diisopropylselenide (DIPSe) is employed for the metalorganic vapor phase epitaxy (MOVPE) of ZnSe in order to eliminate premature gas phase reaction while maintaining negligible carbon incorporation and preserving relatively low growth temperature. In combination with dimethylzinc, single crystalline ZnSe layers were grown on GaAs at temperature around 450$^{\circ}C$. Secondary ion mass spectrometry showed a negligible carbon incorporation in ZnSe films grown from DIPSe even at high [Ⅵ]/[II] ratios, in contrast of a carbon concentration of 1021 cm-3 in ZnSe films grown from diallyselenide (DASe). Crystalline and interface quality are demonstrated by secondary electron microscopy, secondary ion mass spectroscopy and double crystal X-ray diffraction.

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Technique development of Bi-2212/2223 superconductor thick film manufacturing by plasma spraying and heat treatment (플라즈마 용사 및 열처리 공정을 통한 Bi-2212/2223 초전도체 thick film 제조의 기술 개발)

  • Lee, Seon-Hong;Cho, Sang-Hum;Ko, Young-Bong;Park, Kyeung-Chae
    • Proceedings of the KWS Conference
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    • 2005.11a
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    • pp.262-264
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    • 2005
  • $Bi_{2}Sr_{2}CaCu_{2}O_{x}$(Bi-2212) and $Bi_{2}Sr_{2}Ca_{2}Cu_{3}O_{y}$(Bi-2223) high-$T_{c}$ superconductor(HTS) coating have been prepared by plasma spraying and heaat treatment. The Bi-2212 HTS coating later is synthesized through the peritectic reaction between Sr-Ca-Cu oxide coating layer and Bi-Cu oxide coating later, and $Bi_{2}Sr_{2}CaCu_{2}O_{y}$(Bi-2212) superconducting phase grow by partial melting process. The superconducting characteristic depends strongly on the conditions of the partial melting process. the Bi-2212 HTS layer consists of the whiskers grown in the diffusion direction. Above the 2212 layer, Bi-2223 phase and secondary phase was observed. The secondary phase is distributed uniformly over the whole surface. This is caused to the microcrack on the coatings surface. Despite everything, the film shows superconducting with an onset $T_{c}$ of about 115K. There are two changes steps. One changes (1step) at 115K is due to the diamagnetism of the Bi-2223 phase and the other changes (2step) at 78K is due to the diamagnetism of the Bi-2212 phase.

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Evaluation of Microwave Dielectric Properties of MgO-TiO2 System by Dielectric Mixing Rules

  • Kim, Eung-Soo;Seo, Seock-No
    • Journal of the Korean Ceramic Society
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    • v.47 no.2
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    • pp.163-168
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    • 2010
  • Effects of compositions on the microwave dielectric properties of the MgO-$TiO_2$ system were investigated as a function of the molar ratio of MgO to $TiO_2$ ($0.9{\leq}MgO/TiO_2\;(x){\leq}1.2$). With the compositional changes, secondary phases of $MgTi_2O_5$ and $Mg_2TiO_4$ were also detected along with $MgTiO_3$. Microwave dielectric properties of the specimens were dependent on the types of phases developed in the sintered specimens. A single phase of $MgTiO_3$ showed a dielectric constant (K) of 18.2, a quality factor (Qf) of 198,000 GHz, and a temperature coefficient of resonant frequency (TCF) of $-51\;ppm/^{\circ}C$. However, the dielectric properties of the specimens with a secondary phase of $MgTi_2O_5$ (K=19.9, Qf=48,000 GHz) and/or $Mg_2TiO_4$ (K=15.6, Qf=56,000 GHz) were worsened. Dependence of the microwave dielectric properties on the secondary phase of the MgO-$TiO_2$ system was also discussed in terms of dielectric mixing rules.

Test Results of a Three Phase 10㎸A HTS Transformer With Double Pan Cake Coils (3상 10kVA 더블 팬케익 코일형 고온초전도 변압기 특성시험 결과)

  • 이승욱;이희준;차귀수;이지광;최경달;류경우;한송엽
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.52 no.3
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    • pp.101-106
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    • 2003
  • The high temperature superconductor transformers gain interests from the industries. This paper described construction and test results of 10㎸A HTS transformer Three phase transformer with double pancake windings were constructed. To reduce the leakage magnetic field, secondary coil were placed between the two primary coils. BSCCO-2223 wire. silicon sheet steel core and FRP cryostats were used to construct the transformer. Three coils were stacked in one cryostat. Two double pancake coils were connected in series for the primary coil and one double pancake coil was used for the secondary coil. Total number of turns of the primary winding and the secondary winding were 112turns and 98urns, respectively, The rated voltages of each winding were 440/220V. The rated currents of each winding were 13.1/26.2A. After the tests of basic properties of the three phase HTS transformer using no-load test, short-circuit test and full-load test, continuous operation of 100 hours with pure resistive load has been carried out. Test results proved over-load capability and reliability of the HTS transformer.

Effects of Ca, Si on the Microstructure and Aging Characteristic of AZ91 Alloy (AZ91합금의 조직(組織)과 시효특성(時效特性)에 미치는 Ca 및 Si의 영향(影響))

  • Jhee, T.G.;Kim, Y.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.15 no.6
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    • pp.260-268
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    • 2002
  • The effects of calcium and silicon on microstructure and aging characteristics of AZ91 magnesium alloy during T5 treatment was investigated. The addition of 0.88% calcium or 0.25% silicon to AZ91 alloy made dendrite cell smaller. Especially, silicon is more effectively acted as refinement of the dendrite cell than calcium. It is due to that $Mg_2Si$ precipitated at the dendrite cell boundary or in the matrix during T5 treatment of Si added AZ91 alloy retarded the growth of the secondary phase. In the mean while, without inducing the precipitates containing calcium, calcium was segregated mainly around secondary phase such as $Mg_{17}Al_{12}$ and partially dissolved in ternary eutectic (Mg-Al-Ca) structure. In the AZ91 alloy containing both silicon and calcium, more finely distributed $Mg_2Si$ in matrix homogeneously and much finer microstructure were obtained than those containing silicon or calcium. Hence, An AZ91 containing both silicon and calcium was more effective to retarding the growth of the secondary phase than the other AZ91 alloy such as AZ91 alloy containing silicon or AZ91 alloy containing calcium.