• 제목/요약/키워드: second hardening

검색결과 77건 처리시간 0.02초

침장용 PLA 섬유에 대한 저온 경화유제에 관한 연구 (Study on Low Temperature Curing Emulsion of PLA Fiber for Bedding)

  • 안영무
    • 패션비즈니스
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    • 제16권1호
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    • pp.41-51
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    • 2012
  • Polyester is mainly used as a bedding filler material. PLA fiber as an eco-friendly material for substituting polyester has a low melting temperature and therefore a hardening process is impossible. This study is to develop the oil for feather touch that can treat at the melting temperature of PLA. The slippery and soft aminosilicone emulsion, and the bulky epoxysilicone emulsion were used. They had proper viscosity and particle size for flexibility and elasticity. When using methoxy aminosilane [$H_2NSi(OCH_3)_3$] as an aminosilane and [$Zn(OCOCH_3)_2$] as a catalyst, the hardening reaction was fast and effective. Feather touch process were treated by 2 steps. At first step, aminosilicone emulsion, epoxysilicone emulsion and methylaminosilane were mixed and homogenized, and at second step, 5% blened solution of the first step, Zn catalyst 1%, distilled water 94% were treated at PLA fiber. After treatment the static friction coefficient and dynamic friction coefficient were reduced to 23.5-60.8% and 30.0-61.3% respectively, and the laundry and sun light fastnesses have not shown any decrease.

Influence of Calcium on the Formation of Aluminosilicate Inorganic Polymer Binder

  • Ahn, Sangwook;Choi, Youngkue;Shin, Byeongkil;Lee, Jungwoo;Lee, Heesoo;Hui, Kwunnam
    • 대한금속재료학회지
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    • 제49권5호
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    • pp.362-366
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    • 2011
  • Aluminosilicate inorganic polymer binder has been studied as an alternative to ordinary Portland cement due to its higher physical properties, chemical resistance and thermal resistance. This study has been carried out in an attempt to understand the hardening characteristics of aluminosilicate binder by varying the content of calcium. Samples with four different ratios of Al, Si, and Ca were synthesized in this study with the Al:Si:Ca mol ratio being 1.00:1.85~1.98:0.29~2.12. Furthermore, an alkali silicate solution was prepared with the sodium hydroxide (NaOH) and sodium silicate (NaSi). The hardening characteristics of the specimens were analyzed using XRD, SEM, and TG/DTA. In addition, compressive strength and sintering time of specimens were measured as a function of calcium content. The results showed that the specimen containing 2.12 mol% calcium offered the highest compressive strength. However, the compressive strength of the specimen containing 0.26 mol% calcium was lower relative to the other specimens. The results displayed a distinct tendency that as more calcium was added to the inorganic polymer, setting time became shorter. When calcium was added to the inorganic polymer structure, a second phase was not formed, indicating that the addition of calcium does not affect the crystalline structure.

SiCp입자강화 Al 복합재료에 대한 합금원소의 영향과 시효특성에 관한 연구 (A Study on Ageing Characteristics and Alloy Elements of SiCp Reinforced Al Matrix Composites)

  • 김석원;이의종;우기도;김동건
    • 한국주조공학회지
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    • 제21권1호
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    • pp.7-14
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    • 2001
  • The research on new DRA(discontinuous reinforced alloy) and CRA(continous reinforced alloy) composites has been carried out to improve the properties of ceramic fiber and particle reinforced metal matrix composites(MMCs). Effects of alloying elements and aging conditions on the microstructures and aging behavior of Al-Si-Cu-Mg-(Ni)-SiCp composite have been examined. The specimens used in this study were manufactured by duplex process. The first squeeze casting is the process to make precomposite and the second squeeze casting is the process to make final composite. The hardening behavior was accelerated with decreasing the size of SiCp particle in the composites. It is considered that the dislocation density increased with increasing SiCp size, due to the different thermal deformation between Al matrix and SiCp during quenching after the solution treatment. Peak aging time to obtain the maximum hardness in 3 ${\mu}m$ SiCp reinforced Al composite was reduced than that in large size(5, 10 ${\mu}m$) of SiCp because of difference in dislocation density. Aging hardening responce(${\Delta}H$ = $H_{Max}.-H_{S.T}$) of composites was greater than that of unreinforced Al alloy because of higher density of second phases in matrix.

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면진원전의 층응답스펙트럼 해석 (Floor Response Spectrum Analysis of a Base-isolated Nuclear Power Plant)

  • 정재욱;이상민;홍정욱
    • 한국전산구조공학회논문집
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    • 제29권4호
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    • pp.355-362
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    • 2016
  • 대규모 지진에 대한 원전의 안전성을 확보하는 방안으로 기존 원전 구조물에 면진장치를 설치하는 방안이 도입되고 있다. 면진장치를 설치함으로써 상부구조와 지반의 거동을 격리시킬 수 있고, 구조물 자체의 고유주기가 길어지게 되는데, 이를 통해 지진하중에 대한 구조물의 응답을 감소시킬 수 있게 된다. 특히 원전구조물 설계 시 원전구조물 자체뿐만 아니라 원전 내부 기기에 대한 안전성 확보가 필수적이다. 이를 위해 특정 층에 위치한 기기의 설계를 위해 각 층의 최대 요구 응답을 나타내는 층응답스펙트럼이 일반적으로 사용된다. 본 논문에서는 원전 구조물의 지진해석을 통해 특정 층의 층응답스펙트럼을 평가하고, 면진 장치의 거동 특성중 하나인 2차 경화에 대한 영향 또한 평가하였다.

Wave propagation of FG polymer composite nanoplates reinforced with GNPs

  • She, Gui-Lin
    • Steel and Composite Structures
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    • 제37권1호
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    • pp.27-35
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    • 2020
  • This study examines the wave propagation of the functionally graded polymer composite (FG-PC) nanoplates reinforced with graphene nanoplatelets (GNPs) resting on elastic foundations in the framework of the nonlocal strain gradient theory incorporating both stiffness hardening and softening mechanisms of nanostructures. To this end, the material properties are based on the Halpin-Tsai model, and the expressions for the classical and higher-order stresses and strains are consistently derived employing the second-order shear deformation theory. The equations of motion are then consistently derived using Hamilton's principle of variation. These governing equations are solved with the help of Trial function method. Extensive numerical discussions are conducted for wave propagation of the nanoplates and the influences of different parameters, such as the nonlocal parameter, strain gradient parameter, weight fraction of GNPs, uniform and non-uniform distributions of GNPs, elastic foundation parameters as well as wave number.

2D continuum viscodamage-embedded discontinuity model with second order mid-point scheme

  • Do, Xuan Nam;Ibrahimbegovic, Adnan
    • Coupled systems mechanics
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    • 제7권6호
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    • pp.669-690
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    • 2018
  • This paper deals with numerical modeling of dynamic failure phenomena in rate-sensitive brittle and/or ductile materials. To this end, a two-dimensional continuum viscodamage-embedded discontinuity model, which is based on our previous work (see Do et al. 2017), is developed. More specifically, the pre-peak nonlinear and rate-sensitive hardening response of the material behavior, representing the fracture-process zone creation, is described by a rate-dependent continuum damage model. Meanwhile, an embedded displacement discontinuity model is used to formulate the post-peak response, involving the macro-crack creation accompanied by exponential softening. The numerical implementation in the context of the finite element method exploiting the second-order mid-point scheme is discussed in detail. In order to show the performance of the model several numerical examples are included.

Plasticity-damage model parameters identification for structural connections

  • Imamovic, Ismar;Ibrahimbegovic, Adnan;Knopf-Lenoir, Catherine;Mesic, Esad
    • Coupled systems mechanics
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    • 제4권4호
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    • pp.337-364
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    • 2015
  • In this paper we present methodology for parameters identification of constitutive model which is able to present behavior of a connection between two members in a structure. Such a constitutive model for frame connections can be cast in the most general form of the Timoshenko beam, which can present three failure modes. The first failure mode pertains to the bending in connection, which is defined as coupled plasticity-damage model with nonlinear softening. The second failure mode is seeking to capture the shearing of connection, which is defined as plasticity with linear hardening and nonlinear softening. The third failure mode pertains to the diffuse failure in the members; excluding it leads to linear elastic constitutive law. Theoretical formulation of this Timoshenko beam model and its finite element implementation are presented in the second section. The parameter identification procedure that will allow us to define eighteen unknown parameters is given in Section 3. The proposed methodology splits identification in three phases, with all details presented in Section 4 through three different examples. We also present the real experimental results. The conclusions are stated in the last section of the paper.

Nb 첨가 Zr 합금의 미세조직과 Creep 특성에 미치는 마지막 열처리 온도의 영향 (Effect of Final Annealing Temperature on Microstructure and Creep Characteristics of Nb-containing Zirconium Alloys)

  • 박용권;윤영권;위명용;김택수;정용환
    • 한국재료학회지
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    • 제11권10호
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    • pp.879-888
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    • 2001
  • The effects of final annealing temperature on the microstructure and creep characteristics were investigated for the Zr-lNb-0.2X (X=0, Mo, Cu) and Zr-lNb- 1Sn-0.3Fe-0.1X (X=0, Mo, Cu) alloys. The microstructures were observed by using TEM/EDS, and grain size and distributions of precipitates were analyzed using a image analyzer. The creep test was performed at $400^{\circ}C$ under applied stress of 150 MPa for 10 days. The $\beta$-Zr was observed at annealing temperature above $600^{\circ}C$. In the temperature above$ 600^{\circ}C$, the grain sizes of both alloy systems appeared to be increased with increasing the final annealing temperature. The creep strengths of Zr-1Nb-1Sn-0.3Fe-0.1X alloys were higher than those of Zr-1Nb-0.2X ones due to the effect of solid solution hardening by Sn in Zr-lNb-lSn-0.3Fe-0.1X alloy system. Also, Mo addition showed the strong effect of precipitate hardening in both alloy systems. The creep strength rapidly decreased with increasing the annealing temperature up to $600^{\circ}C$. However, a superior creep resistance was obtained in the sample that annealed to have a second phase of $\beta$-Zr. It was considered that the appearance of $\beta$-Zr would play an important role in the strengthening mechanism of creep deformation.

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낙엽송 마루판재의 표면강화 처리기술 개발(II) (Development of Surface Improvement Technique of Japanese Larch Flooring Board(II))

  • 박상범
    • Journal of the Korean Wood Science and Technology
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    • 제28권1호
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    • pp.28-35
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    • 2000
  • 본 연구는 재면이 약한 낙엽송재의 재질개량의 일환으로 경도와 내마모성 등 표면성능의 개선을 도모하기 위한 표면 강화처리기술을 개발하기 위하여 수행되었다. 본 연구에서는 2가지의 도장법을 적용하였다. 첫째, UV경화형 에폭시아크릴에트수지도료에 관능성 모노머와 내마모제를 첨가하였으며, 둘째, 불포화폴리에스테르수지도료를 밑칠용으로 그리고 내마모제가 첨가된 아크릴수지도료를 마감칠로 사용하였다. 제 1도장법에 의해 표면경도가 2H에서 3H로 개선되었으며, 제 2도장법에 의해 4H로 크게 개선되었으며 내마모성도 향상되었다. 이들 처리에 의해 충격에 의한 도막의 갈라짐은 거의 발생하지 않았다. 제 2도장법에 의한 표면강화처리 마루판은 케루잉재의 대체재로서 중보행용의 실내 마루판으로 이용 가능한 것으로 시사된다.

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연고제(軟膏劑)의 경도(硬度)에 관(關)한 연구(硏究) ( II ) -약전수재연고제(藥典收載軟膏劑)의 외견상(外見上)의 대수경도(對數硬度)- (The Study Concerned with the Hardness of Ointment ( II ) -The Apparent Logarithmic Hardness of Ointment Registered on the Pharmacopea of Korea-)

  • 김종갑;이숙향
    • Journal of Pharmaceutical Investigation
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    • 제4권1_2호
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    • pp.39-45
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    • 1974
  • According to previous paper, the hardness of semi-solid as ointments and suppositories causes the tough or skin, the pain and connected with absorption, the state of spread or the efficiency of drug. When the hardening agent or the softening agent is added to ointment whid, is registered on the pharmacopeia of the republic of Korea, the experimertal data by apparent logarithmic hardness are shown is Table 1. The results are as the folloring. 1) In case of the softening agent which is added to ointment base, each has shown two different equation with differnented slope as $K_1$ and $K_2$ value determined (Fig. 1,2). 2) When the hardening agent is added to same ointment base, these studies indicated that there is a direct correlation between $K_1$ and $K_2$. However, in case of softening agent $K_1$ and $K_1$ are not correlated as indicated in Fig. $3{\sim}8$. 3) On condition of same ointment base, the critical poit is proportional to $K_1$ 4) The second effect is at least $3{\sim}17$ times more. sensitive than the first effect or in average 8.3 times more sensitive, Therefore, the results presented in this paper. Suggest that, when the drug is added to a certain ointment base, it should be added within this first effect before the critical point is reached.

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