• Title/Summary/Keyword: scratch test

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Effect of CrN barrier on fuel-clad chemical interaction

  • Kim, Dongkyu;Lee, Kangsoo;Yoon, Young Soo
    • Nuclear Engineering and Technology
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    • v.50 no.5
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    • pp.724-730
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    • 2018
  • Chromium and chromium nitride were selected as potential barriers to prevent fuel-clad chemical interaction (FCCI) between the cladding and the fuel material. In this study, ferritic/martensitic HT-9 steel and misch metal were used to simulate the reaction between the cladding and fuel fission product, respectively. Radio frequency magnetron sputtering was used to deposit Cr and CrN films onto the cladding, and the gas flow rates of argon and nitrogen were fixed at certain values for each sample to control the deposition rate and the crystal structure of the films. The samples were heated for 24 h at 933 K through the diffusion couple test, and considerable amount of interdiffusion (max. thickness: $550{\mu}m$) occurred at the interface between HT-9 and misch metal when the argon and nitrogen were used individually. The elemental contents of misch metal were detected at the HT-9 through energy dispersive X-ray spectroscopy due to the interdiffusion. However, the specimens that were sputtered by mixed gases (Ar and $N_2$) exhibited excellent resistance to FCCI. The thickness of these CrN films were only $4{\mu}m$, but these films effectively prevented the FCCI due to their high adhesion strength (frictional force ${\geq}1,200{\mu}m$) and dense columnar microstructures.

티타늄 임플란트와 수산화아파타이트 사이의 접착력 향상을 위한 Yttria-stabilized Zirconia Buffer Layer에 관한 연구

  • Park, Hyeong-Seok;Gang, Seong-Geun;Lee, Won-Jun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.386-386
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    • 2010
  • 최근 널리 보급되고 있는 치과용 임플란트는 티타늄(Ti) 또는 티타늄 합금(Ti-6Al-4V) 보철과 크라운을 연결하여 사용하고 있다. 티타늄은 생체 친화성이 우수하나, 생체 활성도가 없어 치유기간이 긴 단점이 있다. 이를 보완하기 위해 인체 경조직과 유사한 수산화아파타이트(hydroxyapatite, $Ca_{10}(PO_4)_6(OH)_2)$를 티타늄 임플란트 표면에 코팅하는 방법이 연구되고 있으나 수산화아파타이트 코팅은 티타늄과의 접착성이 나쁘기 때문에 시술 및 사용과정에서 코팅층이 임플란트로부터 박리되는 문제점이 있다. 본 연구에서는 티타늄과 수산화아파타이트 사이에서 접착력을 향상시키는 buffer layer로서 지르코니아(8YSZ, 8mol% Yttria-stabilized zirconia)를 연구하였다. 지르코니아는 고온에서 안정하며, 티타늄 합금과 수산화아파타이트 사이의 반응을 방지하며, 박막밀도와 기계적 강도가 좋은 생체세라믹스이다. 지르코니아 박막을 펄스 레이저 증착법을 이용하여 증착 온도 $600^{\circ}C$, 레이저 fluence $2\;J/cm^2$에서 산소($O_2$) 분압을 바꿔 가며 증착하였다. 그 위에 수산화아파타이트 박막을 역시 펄스 레이저 증착법으로 증착하였다. Scratch test와 Pull-off test를 통해 접착력을 평가한 결과 지르코니아 buffer layer 삽입에 의해 티타늄 합금과 수산화아파타이트 사이의 접착력이 향상되었음을 확인하였다. 또한 산소분압이 박막의 특성 및 접착력에 미치는 영향을 고찰하였다.

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SVM on Top of Deep Networks for Covid-19 Detection from Chest X-ray Images

  • Do, Thanh-Nghi;Le, Van-Thanh;Doan, Thi-Huong
    • Journal of information and communication convergence engineering
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    • v.20 no.3
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    • pp.219-225
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    • 2022
  • In this study, we propose training a support vector machine (SVM) model on top of deep networks for detecting Covid-19 from chest X-ray images. We started by gathering a real chest X-ray image dataset, including positive Covid-19, normal cases, and other lung diseases not caused by Covid-19. Instead of training deep networks from scratch, we fine-tuned recent pre-trained deep network models, such as DenseNet121, MobileNet v2, Inception v3, Xception, ResNet50, VGG16, and VGG19, to classify chest X-ray images into one of three classes (Covid-19, normal, and other lung). We propose training an SVM model on top of deep networks to perform a nonlinear combination of deep network outputs, improving classification over any single deep network. The empirical test results on the real chest X-ray image dataset show that deep network models, with an exception of ResNet50 with 82.44%, provide an accuracy of at least 92% on the test set. The proposed SVM on top of the deep network achieved the highest accuracy of 96.16%.

The Effect of Combined Exercise on Body Composition, Functional Fitness and Muscle Protein Synthesis Related Hormone in Sarcopenic Obesity Elderly Women (복합운동이 근감소증을 동반한 비만 여성고령자의 신체조성과 기능적 체력 및 근단백질합성 관련 호르몬에 미치는 영향)

  • So, Yong-Seok
    • Journal of the Korea Convergence Society
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    • v.7 no.3
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    • pp.185-193
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    • 2016
  • The purpose of this study was to analyze the effects of combined exercise on body composition, funtional fitness and muscle protein synthesis related hormone in sarcopenic obesity elderly women. The subjects for the study were 20 obesity elderly women over 65 years old. They were divided into two groups, the sarcopenic obesity group(n=10) and non-sarcopenic obesity group(n=10). The variables of body composition and cardiovascular fitness were measured in all the subjects before and after 12-week combined exercise. The findings of this study were as follows; In the sarcopenic obesity elderly women (SG), % body fat significantly decreased in the SG group, FFM and ASM significantly increased. In the chair stand test and arm curl test, SG group significantly increased. SG group significantly changed in chair sit-and-reach test, back scratch test, 2-minute step test. In the muscle protein synthesis related hormone(growth hormone and IGF-1), SG group significantly increased.

Correlations among Respiratory Function, UPDRS and Senior Fitness in Parkinson's Disease Patients (파킨슨병환자의 호흡기능, UPDRS 및 Senior Fitness의 관련성)

  • Kang, Dong-Yeon;Cheon, Sang-Myung;Cheon, Sang-Myung;Lee, Kyung-Soon;Kim, Kyoung
    • The Journal of Korean Physical Therapy
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    • v.26 no.2
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    • pp.48-55
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    • 2014
  • Purpose: The purpose of this study was to examine correlations among UPDRS, respiratory function, and senior fitness and to investigate the effects of restrictive respiratory function on these factors in Parkinson's disease patients. Methods: Subjects (n=25, Hoehn & Yahr (H&Y) stage: 2-3, $69.3{\pm}5.9$ yrs) from D Hospital Parkinson's Disease Center at Busan metropolitan area in the Republic of Korea volunteered for this study. They performed the pulmonary function test, UPDRS, and the senior fitness test. SPSS 18.0 was used for analysis of data, and the collected data were analyzed using Pearson's correlation coefficient (n=25). In addition, Independent t-test was used for determination of differences between two groups (between the normal pulmonary function group (n=10) and the restrictive pulmonary function group (n=10)). Results: Forced vital capacity (FVC (L)) showed significant negative correlation (r=-0.44, p<0.05) with H&Y stage in Parkinson's disease patients, and chair stand showed significant negative correlations (r=0.41, 0.43, 0.42, p<0.05) with FVC (L), FVC (%), and FEV1 (L). FVC (%) showed significant positive correlations (r=0.44, r=0.44, p<0.05) with right and left back scratch. In addition, the restrictive respiratory function group showed significantly lower FVC (%) (p<0.01) and was significantly slower (p<0.05) in the 8-foot up-and-go test than the normal respiratory function group. Conclusion: In conclusion, these results suggest that restrictive respiratory function in PD was related to H&Y stage. In addition, agility of PD patients was lower in the restrictive respiratory function group than in the normal function group.

The Effect of Hyaluronic Acid on the Invasiveness of Malignant Glioma Cells : Comparison of Invasion Potential at Hyaluronic Acid Hydrogel and Matrigel

  • Jin, Shu-Guang;Jeong, Young-Il;Jung, Shin;Ryu, Hyang-Hwa;Jin, Yong-Hao;Kim, In-Young
    • Journal of Korean Neurosurgical Society
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    • v.46 no.5
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    • pp.472-478
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    • 2009
  • Objective : Hyaluronidase (HAse), a degrading enzyme of hyaluronic acid (HA), is highly expressed in patients with malignant glioma. The purpose of this study was to verify whether HAse is related to the invasion of glioma cells. We also investigated if glioma cells with higher mobility in 2-dimensioal (2-D) method have also higher mobility at 3-dimensional (3-D) environment. Methods : Malignant glioma cell lines (U87MG, U251MG, U343MG-A, and U373MG) were used, and their HAse expressions were evaluated by HA zymography. The migration ability was evaluated by simple scratch technique. The invasiveness of each cell lines was evaluated by Matrigel invasion assay and HA hydrogel invasion assay. In HA hydrogel invasion assay, colonies larger than $150\;{\mu}m$ were regarded as positive ones and counted. Statistical analysis of migration ability and invasion properties of each cell lines was performed using t-test. Results : In scratch test to examine migration ability of each cell lines, U87MG cells were most motile than others, and U343MG-A least motile. The HAse was expressed in U251MG and U343MG-A cell lines. However, U87MG and U373MG cell lines did not express HAse activity. In Matrigel invasion assay, the cell lines expressing HAse (U251MG and U343MG-A) were more invasive in the presence of HA than HAse deficient cell lines (U87MG and U373MG). In HA hydrogel invasion assay, the HAse-expressing cell lines formed colonies more invasively than HAse-deficient ones. Conclusion : Malignant Glioma cells expressing HAse were more invasive than HAse-deficient ones in 3-dimensional environment. Therefore, it might be suggested that invasion of malignant gliomas is suppressed by inhibition of HAse expression or HA secretion. Additionally, the ability of 2-D migration and 3-D invasion might not be always coincident to each other in malignant glioma cells.

Mechanical Properties of Ta/TaN Multilayer (Ta/TaN 복합 다층 피막의 기계적 특성)

  • Gang, Yeong-Gwon;Lee, Jong-Mu;Choe, Sang-Uk
    • Korean Journal of Materials Research
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    • v.9 no.8
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    • pp.837-842
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    • 1999
  • The Ta/TaN multilayer structure with repeating layers of a poly-crystalline Ta layer of high ductility and a TaN layer of high hardness is expected to exhibit toughness. This paper reports the results on the hardness and the adhesion strength of Ta/TaN multilayers and compositional gradient Ta/TaN layers deposited on the high speed steel substrate by reactive sputtering as a function of annealing temperature. The TaN film deposited with the $N_2$/Ar ratio of 0.4 in the reactive sputtering process exhibits the highest crystallinity, and the highest hardness and the results of scratch test of the Ta/TaN multilayers. The hardness and adhesion strength of the Ta/TaN multilayers becomes deteriorated with increasing the annealing temperature in the heat treatment right after depositing the layers. Therefore, post-annealing treatments are not desirable in the case of the Ta/TaN multilayers from the standpoint of mechanical properties. Also the hardness of Ta/TaN multilayers increases with decreasing the compositional modulation wavelength, but the adhesion property of the layers is nearly independent of the wavelength. On the other hand, the compositional gradient Ta/TaN film exhibits the highest hardness and the value of scratch test for the post-annealing temperatures of 20$0^{\circ}C$ and 40$0^{\circ}C$, respectively. This tendency of the compositional gradient Ta/TaN films differs from that of the Ta/TaN multilayers.

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A Study on the standardize the characteristic evaluation of DC magnetron sputtered silver coatings for engineering purposes (D.C. magnetron sputter를 이용한 Ag layer 건식 도금층의 특성 평가 국제 표준화에 대한 연구)

  • Gyawali, Gobinda;Choi, Jinhyuk;Lim, Tae Kwan;Jung, Myoung Joon;Lee, Soo Wohn
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.11a
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    • pp.249-249
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    • 2015
  • Silver films have been of considerable interest for years due to their better performance relative to other metal films for engineering applications. A series of multi-layer silver coatings with different thickness (i.e. 0.3 um to 1.5 um) were prepared on Aluminium substrate containing copper undercoat by direct current (DC) magnetron sputtering method. For the comparative purpose, similar thickness silver coatings were prepared by electrolytic deposition method. Microstructural, morphological, and mechanical characteristics of the silver coatings were evaluated by means of scanning electron microscope (SEM), X-ray diffraction (XRD), Surface roughness test, microhardness test and nano-scratch test. From the results, it has been elucidated that the silver films prepared by DC magnetron sputtering method has superior properties in comparison to the wet coating method. On the other hand, DC magnetron sputtering method is relatively easier, faster, eco-friendly and more productive than the electrolytic deposition method that uses several kinds of hazardous chemicals for bath formulation. Therefore, a New Work Item Proposal (NWIP) for the test methods standardization of DC magnetron sputtered silver coatings has recently been proposed via KATS, Korea and a NP ballot is being progressed within a technical committee "ISO/TC107-metallic and other inorganic coating".

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Evaluation of Adhesive Properties in Polymeric Thin Film by Ultrasonic Atomic Force Microscopy (UAFM을 이용한 폴리머 박막의 접합 특성 평가)

  • Kwak, Dong-Ryul;Park, Tae-Sung;Park, Ik-Keun;Miyasaka, Chiaki
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.2
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    • pp.142-148
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    • 2012
  • This study presents the assessment results of adhesive properties on the interface between a silicon wafer and nano-scale polymer thin film pattern through UAFM images by using the contact resonance frequency of the cantilever. For the experiment, we varied surface treatment processes for the silicon wafer and fabricated a 300nm polymer thin film pattern through lithography. Images from the optical microscope were used to compare the produced test specimens for adhesive condition and the critical load value from the nano scratch test was used to verify the adhesive condition of the nano pattern. Each test specimen resulted in a $1{\mu}m{\times}1{\mu}m$ surface image and subsurface adhesive image. Adhesive condition was evaluated by image contrast differences on the interface according to the changing amplitudes and phases of contact resonance frequency.

Evaluation of Age-Hardening Characteristics of Squeeze-Cast A356 Alloy by Using Micro/Nano Indenter with AFM (나노/마이크로 인덴터와 AFM을 이용한 스퀴즈 캐스트 A356 합금의 시효경화특성 평가)

  • Youn S.W.;Kim K.D.;Kang C.G.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.1398-1401
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    • 2005
  • The nano/microstructure, the aging response (in T5 heat treatment), and the mechanical/tribological properties of the eutectic regions in squeeze-cast A356 alloy were investigated using nano/micro-indentation and mechanical scratching, combined wit optical microscopy and atomic force microscope(AFM). Most eutectic Si crystals in the A356 alloy showed a modified morphology as fine-fibers. The loading curve for the eutectic region was more irregular than that of the primary Al region due to the presence of various particles of varying strength. In addition, the eutectic region showed lower pile-up and higher elastic recovery than the primary Al region. The aging responses of the eutectic regions in the squeeze-cast A356 alloys aged at $150^{\circ}C$ for different times(0, 2, 4, 8, 10, 16, 24, 36 and 72 h) were investigated. As the aging time increased, acicular Si particles in the eutectic regions gradually came to a fine structure. Both Vickers hardness ($H_V$) and indentation ($H_{IT}$) test results showed almost the same trend of aging curves, and the peak was obtained at the same aging time of 10 h. A remarkable size-dependence of the tests was found. The friction coefficient for the eutectic region was lower than that for the primary Al region.

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