• Title/Summary/Keyword: scanning electronic microscope (SEM)

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Dispersibility, Electrical Property of Nano-Composite by Solution Mixing Method (용액혼합법에 따른 나노복합재료 분산성 및 전기적 특성)

  • Yang, Hoon;Park, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.04c
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    • pp.73-74
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    • 2008
  • In this paper, we have investigated dispersibility, volume resistivity of nano-composite by solution mixing method. Dispersibility measured by FE-SEM(Field Emission Scanning Electron Microscope. And volume resistivity measured by ASTM D991. To expect interaction used dual filler system. But, dual filler system had influence on polymer complex. So, polymer chain mobility doesn't resist.

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Synthesis of Alinite Cement Using Combustion Ash of Solid Wastes (고형 폐기물 소각재를 이용한 alinite 시멘트의 합성)

  • 강현주;홍성수;임계규;오희갑;김정석;민경소
    • Journal of the Korean Ceramic Society
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    • v.37 no.8
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    • pp.768-773
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    • 2000
  • Alnite clinker, which is based on CaO-SiO2-CaCl2 system, was synthesized by recycling Cl-containing waste, and its hydraulic properties were onvestigated. Alinite coinkers with two different chemical compositions were burned for 10∼30 minutes in the range of temperature, 1350∼1450$^{\circ}C$. The microstructures of those clinkers were characterized by powder X-ray diiffracuion analysis, optical microscope, and scanning electronic microscope and heat of hydration of alinite cements which was measured in order to investigate hydraulic properties. X-ray analysis shwoed that f-CaO in both clinkers with different compositions significantly was decreased with transforming C2S(belite) to C3S(alite). From the results of microscopy and scanning electron microscopy(SEM), crystal of synthesized alite(C3S) was larger and better crystallinity than that of ordinary portland cement.

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Characterization Method for Testing Circuit Patterns on MCM/PCB Modules with Electron Beams of a Scanning Electron Microscope (MCM/PCB 회로패턴 검사에서 SEM의 전자빔을 이용한 측정방법)

  • Kim, Joon-Il;Shin, Joon-Kyun;Jee, Yong
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.35D no.9
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    • pp.26-34
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    • 1998
  • This paper presents a characterization method for faults of circuit patterns on MCM(Multichip Module) or PCB(Printed Circuit Board) substrates with electron beams of a SEM(Scanning Electron Microscope) by inducing voltage contrast on the signal line. The experimentation employes dual potential electron beams for the fault characterization of circuit patterns with a commercial SEM without modifying its structure. The testing procedure utilizes only one electron gun for the generation of dual potential electron beams by two different accelerating voltages, one for charging electron beam which introduces the yield of secondary electron $\delta$ < 1 and the other for reading beam which introduces $\delta$ > 1. Reading beam can read open's/short's of a specific net among many test nets, simultaneously discharging during the reading process for the next step, by removing its voltage contrast. The experimental results of testing the copper signal lines on glass-epoxy substrates showed that the state of open's/short's had generated the brightness contrast due to the voltage contrast on the surface of copper conductor line, when the net had charged with charging electron beams of 7KV accelerating voltages and then read with scanning reading electron beams of 2KV accelerating voltages in 10 seconds. The experimental results with Au pads of a IC die and Au plated Cu pads of BGA substrates provided the simple test method of circuit lines with 7KV charging electron beam and 2KV reading beam. Thus the characterization method showed that we can test open and short circuits of the net nondestructively by using dual potential electron beams with one SEM gun.

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Dispersion Property of CNT/CB Composite influenced EEA (EEA에 미치는 CNT/CB Composite 분산 특성)

  • Yang, Hoon;Park, Dae-Hee
    • Proceedings of the KIEE Conference
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    • 2008.05a
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    • pp.185-186
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    • 2008
  • Use of the carbon nanotube is superior to general powder state materials of dispersion property. Because its ratio of diameter and length(aspect ratio) is very large, it has been known as a type of ideal nano-reinforcement composite. It used solution mixing method for specimen fabrication. To research dispersion property, we used FE-SEM(Field Emission Scanning Electron Microscope) and AFM(Atomic Force Microscope). As a result, this tendency confirms new conductivity network in which the carbon nanotube between carbon black constitute molecules shows a bond by similar constructive property.

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Electrical and optical characteristics of ITO films with different composition (ITO의 조성에 따른 전기적, 광학적 특성)

  • Lee, Seo-Hee;Jang, Gun-Eik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.216-216
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    • 2010
  • ITO는 n- type 반도체 재료로 Sn의 첨가로 인한 매우 낮은 전기저항과 안정성때문에 널리 사용되고 있는 재료이며 비교적 높은 band gap(3.55Ev)를 가짐으로 인하여 가시광선 영역에서 높은 투과도를 가지는 특징이 있다. 단점으로는 박막 제조 시에 증착시간의 증가함에 따라 음이온 충격 및 온도 상공으로 인한 막의 표면손상이 발생하게 되고 이것은 전기저항이 증가하는 요인으로 작용하는 문제점이 있다. 본 연구에서는 3가지 조성의 ITO박막을 스퍼터 장치를 이용하여 증착하고 그에 따른 전기적, 구조적, 광학적 특성을 분석 하였다. 증착된 ITO성막의 표면분석을 위해 AFM (Atomic Force Microscope)으로 표면 거칠기값 분석, XRD (X-ray diffraction)을 이용 결정성장분석, SEM (Scanning Electron Microscope)으로 표면의 미세구조관찰, 4Point pobe로 면 저항분석, spectrophotometer로 박막의 투과율과 흡수율을 분석하였다. 조성변화와 공정변수에 따른 전기적, 구조적, 광학적 특성변화의 원인분석으로 고효율의 ITO 박막성장 가능성을 조사하였다.

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A study of the formation of the liner $\lambda$-DNA bridge using the electrostatic interactions on the gold nanoelectrodes (금 나노 전극위에 정전기적 상호작용을 이용한 선형 $\lambda$-DNA 브리지 형성에 관한 연구)

  • Kim, Hyung-Jin;Yi, In-Sun;Roh, Yong-Han;Hong, Byung-You
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.04b
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    • pp.64-67
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    • 2004
  • 본 논문에서는 DNA를 이용한 나노 소자에 응용하기 위하여, photo-lithograpy를 사용하여 나노크기(<100)의 간격을 갖는 금 전극을 제작하였다. 그리고 제작되어진 되어진 나노 전극위에 2-Amino ethanthiol(AET)를 코팅하여 AET와 $\lambda$-DNA 사이의 정전기적 상호 작용을 이용, 금 나노전극 사이에 간단하고 고착율을 높이는 실험을 하였다. SEM(Scanning Electron Microscope) 분석을 통해 나노 크기의 전극 간격을 확인하였고, 두 전극사이에 연결되어진 $\lambda$-DNA는 AFM(Atomic force microscope)을 확인하였다.

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Preparation of High-Temperature catalytic Support from Gibbsite II. Properties of Amophous Alumina as Precursor of Catalyst Support (깁사이트를 원료로 한 고온촉매용 담체의 제조 II, 비정질 알루미나의 담체 전구체로서의 특성)

  • 김성연;김연식
    • Journal of the Korean Ceramic Society
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    • v.33 no.1
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    • pp.92-100
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    • 1996
  • Amorphous alumina(AA) the precursor of ${\gamma}$-alumina for catalyst support was made in the newly designed ball filled heating column. Some properties of AA as precursor were investigated. In observation of microstruc-ture and pore structure of AA and its derivatives scanning electronic microscope(SEM) and transmission electronic microscope(TEM) were used. It was found that the width of one particle in AA was 45~60$\AA$ and the average distance among the particles ranged 9~12 $\AA$ which suggested a micropore structure. When AA was reacted with water the shape of the surface was found to be altered and acicular bioehmite was formed inside AA which contributed inproved formability. Pore distribution was evaluated for the three samples of AA ground and granulated lump and La2O3 coated alumina. Acid sites were quantitatively determined by ammonia TPD method and the effect of impurity of Na on acid sites was discussed. Water adsorption capacity was evaluated in terms of a desiccant.

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Scanning Electronic Microscopy Examination for the Egg of Skin Parasite, Entobdella hippoglossi on the Commercially Important Culture Fish, the Atlantic Halibut, Hippoglossus hippoglossi

  • Yoon Gil Ha
    • Fisheries and Aquatic Sciences
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    • v.1 no.1
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    • pp.68-71
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    • 1998
  • The egg structure and shape of the skin parasite, Entobdella hippoglossi from the Atlantic halibut, Hippoglossus hippoglossus was examined using scanning electronic microscope. The newly produced eggs of E. hippoglossi were yellowish in color and tetrahedral in shape. The eggs were entwined together in a complicated chain-like fashion by a long filament. The appendage showed the presence of buoy-like structures. The buoy-like structures on the appendage of the eggs of E. hippoglossi in the present study were totally different from other sticky droplets. It is suggested that these structures are not sticky droplets but buoys for floating eggs which have entwined together on the bottom of the sea. It seems that these buoy-like structures may be needed for preventing the eggs from being covered by mud or particles and thus maintaining the eggs in an oxygenated environment.

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The Analysis of Oxidization Characteristics according to the shapes of RCD contacts (RCD 접점형태에 따른 산화특성 분석)

  • Kim, Dong-Woo;Kim, Hyang-Kon;Gil, Hyoung-Jun;Han, Woon-Kim;Choi, Chung-Seog
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.576-577
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    • 2005
  • In this paper, the oxidization characteristics were analyzed according to the shapes of Residual Current Protective Device(RCD) contacts. RCD is an electrical safety device specially designed to immediately switch the electricity off when electric leakage is detected at a level harmful to a person using electrical equipment. The shapes of RCD contacts are a little bit different according to the models. When RCD is turned on, stationary and moving contact do not fit together. So, it can cause the increase of contact resistance. To discover the deterioration characteristics of RCD contacts by switching repetition, the contacts were analyzed by stereo microscope, Scanning Electron Microscope(SEM) and Energy Dispersive X-ray Spectrometer(EDS).

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극저온 볼 밀링을 통한 Ibuprofen 분말의 나노화

  • 조현갑;이경엽;박훈재;이상목
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.05a
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    • pp.158-158
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    • 2004
  • 본 연구에서는 이부프로펜(Ibuprofen)분말을 마이크론(Micron) 크기의 입자로 만들기 위하여 극저온 볼 밀링 공정(Cryogenic Ball Milling Process)을 사용하였다. 극저온 볼 밀링 공정은 약 -18$0^{\circ}C$의 질소 분위기에서 6시간 동안 실행되어 졌다 이부프로펜 분말 형상의 변화는 SEM(Scanning Electronic Microscope)촬영을 통하여 관찰하였으며, 분말의 입자 크기와 분포는 입도 분석기(Particle Size Analysis)를 사용하여 극저온 볼 밀링 공정 전ㆍ후의 변화를 관찰하였다(중략)

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