• Title/Summary/Keyword: scanning electron microscope(SEM) image

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Photoluminescence Characteristics of $Y_3Al_5O_{12}$:$Tb^{3+}$ nano-Phosphors by various reagents (반응제에 따른 $Y_3Al_5O_{12}$ : $Tb^{3+}$ 나노형광체의 발광 특성)

  • Kwak, Hyun-Ho;Kim, Se-Jun;Cha, Jae-Hyeok;Choi, Hyun-Wook
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.440-441
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    • 2007
  • For this study, terbium-doped yttrium aluminum garnet (YAG:Tb) phosphor powders were prepared via the combustion process using the varous reagents. The characteristics of the synthesized nano powder were investigated by means of X-ray diffraction (XRD), Scanning Electron Microscope(SEM), and photoluminescence (PL). Single-phase cubic YAG:Tb crystalline powder was obtained at $1000^{\circ}C$ by directly crystallizing it from amorphous materials, as determined by XRD techniques. The SEM image showed that the resulting YAG:Tb powders had uniform sizes and good homogeneity. The photoluminescence spectra of the YAG:Tb nanoparticles were investigated to determinethe energy level of electron transition related to luminescence processes. There were three peaks in the excited spectrum, and the major one was a broad band of around 274 nm. Also, the YAG:Tb nanoparticles showed two emission peaks in the range of 450~500 nm and 525~560 nm, respectively, and had maximum intensity at 545 nm.

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Effect of Mg Additive in the Bi1.84Pb0.34Sr1.91Ca2.03Cu3.06O10+δ(110 K phase) Superconductors (Bi1.84Pb0.34Sr1.91Ca2.03Cu3.06O10+δ(110 K 상)산화물 고온초전도체에 Mg 첨가에 따른 영향)

  • 이민수
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.6
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    • pp.522-531
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    • 2003
  • Samples with the nominal composition, B $i_{1.84}$P $b_{0.34}$S $r_{1.91}$C $a_{2.03}$C $u_{3.06}$ $O_{10+{\delta}}$ high- $T_{c}$ superconductors containing MgO as an additive were fabricated by a solid-state reaction method. Samples with MgO of 5~30 wt% each were sintered at 820~86$0^{\circ}C$ for 24 hours. The structural characteristics, critical temperature, grain size and image of mapping with respect to MgO contents were analyzed by XRD(X-Ray Diffraction), SEM(Scanning Electron Microscope) and EDS(Energy dispersive X-ray spectrometer) respectively. As MgO contents increased, intensity of MgO Peaks and ratio of Bi-2212 phase in superconductors intensified and the proportion of the phase transition from Bi-2223 to Bi-2212 was increased.

Pseudo-strain hardening and mechanical properties of green cementitious composites containing polypropylene fibers

  • Karimpour, Hossein;Mazloom, Moosa
    • Structural Engineering and Mechanics
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    • v.81 no.5
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    • pp.575-589
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    • 2022
  • In order to enhance the greenness in the strain-hardening composites and to reduce the high cost of typical polyvinyl alcohol fiber reinforced engineered cementitious composite (PVA-ECC), an affordable strain-hardening composite with green binder content has been proposed. For optimizing the strain-hardening behavior of cementitious composites, this paper investigates the effects of polypropylene fibers on the first cracking strength, fracture properties, and micromechanical parameters of cementitious composites. For this purpose, digital image correlation (DIC) technique was utilized to monitor crack propagation. In addition, to have an in-depth understanding of fiber/matrix interaction, scanning electron microscope (SEM) analysis was used. To understand the effect of fibers on the strain hardening behavior of cementitious composites, ten mixes were designed with the variables of fiber length and volume. To investigate the micromechanical parameters from fracture tests on notched beam specimens, a novel technique has been suggested. In this regard, mechanical and fracture tests were carried out, and the results have been discussed utilizing both fracture and micromechanical concepts. This study shows that the fiber length and volume have optimal values; therefore, using fibers without considering the optimal values has negative effects on the strain-hardening behavior of cementitious composites.

Studies on the Secondary Battery Application of the Surface Fluorinated Microporous PE Separator Membranes (표면 불소화된 미세다공성 PE 격리막의 이차전지 적용을 위한 연구)

  • Byun, Hong-Sik;Kim, Dae-Hoon;Cho, Hyun-Il;Lee, Byung-Seong;Hong, Byung-Pyo;Lee, Sang-Yun;Nam, Sang-Yong;Seo, Myung-Su;Rhim, Ji-Won
    • Membrane Journal
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    • v.18 no.1
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    • pp.75-83
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    • 2008
  • In this research, the research for enhancing the stability at the mechanical strength and thermal stability and high power through the Direct Fluorination of the Polyethylene (PE, Asahi) for secondary battery was conducted. The surface of according to the fluorine gas exposure time and constructional change were observed through the scanning electron microscope image, and the contact angle. The mechanical property was confirmed through the tensile strength and surface hydrophilic property experiment. Charge and discharge experiment, the lifetime property, and the overcharge test were performed in order to confirm the electrochemical characteristic of produced and we confirmed at the high power that the stability about a temperature was improved.

Effects of oxide layer formed on TiN coated silicon wafer on the friction characteristics

  • Cho, C.W.;Lee, Y.Z.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.167-168
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    • 2002
  • In this study, the effects of oxide layer formed on the wear tracks of TiN coated silicon wafer on friction characteristics were investigated. Silicon wafer was used for the substrate of coated disk specimens, which were prepared by depositing TiN coating with $1\;{\mu}m$ in coating thickness. AISI 52100 steel balls were used for the counterpart. The tests were performed both in air for forming oxide layer on the wear track and in nitrogen to avoid oxidation. This paper reports characterization of the oxide layer effects on friction characteristics using X-ray diffraction (XRD). scanning electron microscopy (SEM) and friction force microscope (FFM).

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The Preparation of Polyurethane Microcapsule and Its Breaking Behavior (폴리우레탄계 마이크로캡슐의 제조 및 그의 파괴 거동)

  • 박형인;김애경;이웅의;최창남
    • Textile Coloration and Finishing
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    • v.10 no.2
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    • pp.37-44
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    • 1998
  • In this study, the polyurethane microcapsules containing disperse dye were prepared by in-situ polymerization method using hexamethylene diisocyanate (HDI, aliphatic type) and m-xylene diisocyanate(XDI, aromatic type) with ethylene glycol (EG) And the size, shape, particle size distribution, and breaking behavior of microcapsules prepared were investigated. The size and shape of microcapsule were observed by scanning electron microscope (SEM) . The particle size distribution was analyzed by image analyzer. The breaking behavior of microcapsule was checked by measuring the optical density of solution that the disperse dye was dissolved after the microcapsule was broken by constant pressure. The particle size was inversely proportional to the stirring speed, and the size of microcapsule prepared from HDI and EG was smaller than that of microcapsule prepared from XDI and EG. Aliphatic type microcapsule was broken easily, compared with aromatic type one. It was considered due to the difference of reactivity between HDI and XDI. And the microcapsule prepared by stirring strongly was broken easily.

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Identification of Genus Triadinium for Plankton Monitoring Network (플랑크톤 모니터링 네트워크를 위한 Triadinium속의 동정)

  • Yeo, Hwan-Goo
    • Proceedings of the KAIS Fall Conference
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    • 2009.05a
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    • pp.842-844
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    • 2009
  • The major group which contains all the organisms that are commonly termed Dinoflagellates is called the division Pyrrophyta or Dinophyta in botanical systems and the order Dinoflagellida or Dinoflagellata in zoological systems. Most dinoflagellates are biflagellated solitary planktonic cells. A taxonomic survey of the dinoflagellate family, Triadiniaceae Dodge was conducted for plankton monitoring network in the coastal waters of Korea. Identification of species in water samples was usually done by using differential interference contrast (DIC), which revealed especially well lighted thecal structures. For the apparent three-dimensional image, scanning electron microscope (SEM) was used. Two species were identified and described, which were Triadinium orientale(Lindemann)Dodge and Triadinium sphaericum(Murray and Whitting)Dodge.

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Electrical Characteristics and Microstructure of Thin Films $BaTiO_3$ depending on The Sintering Temperature ($BaTiO_3$계 박막의 소결온도에 따른 미세구조와 전기적 특성)

  • Kim, D.K.;Jeon, J.B.;Park, C.B.;Song, M.J.;Kang, Y.C.;Park, H.A.;Soo, B.M.;Kim, T.W.;Kang, D.Y.
    • Proceedings of the KIEE Conference
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    • 1997.07d
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    • pp.1573-1576
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    • 1997
  • Thin films of $BaTiO_3$ system were prepared by radio frequency (rf)/dc magnetron sputtering method. We have investigated crystal structure, surface morphology and PTCR(positive-temperature coefficient of resistance) characteristics of the specimen depending on second heat - treatment temperatures. Scanning electron microscope(SEM) image of $BaTiO_3$ thin films shows that the specimen heat treated in between 900 and 1100[$^{\circ}C$] shows a grain growth. At 1100[$^{\circ}C$], the specimen stops grain-growing and becomes a crystal. A resistivity-temperature characteristics of the specimen depends on the doping concentrations of Mn.

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Study on the nonuniform modification of laser ablated HTS surface (레이저 융제된 HTS 표면의 불균일한 변조에 대한 연구)

  • Jeong, Young-Sik;Lee, Sang-Yeol
    • Proceedings of the KIEE Conference
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    • 1996.11a
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    • pp.251-253
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    • 1996
  • High temperature superconducting (HTS) target has been irradiated by excimer laser beam. The surface of HTS target has been changed and showed the formation of cones. The laser ablated HTS target surface has been systematically studied using a scanning electron microscope. A KrF excimer laser with a wavelength of 248 nm was used to ablate the HTS YBCO target. The size of laser beam focused on the target showed a rectangular shape of $9.7{\times}2\;mm^2$. The image of SEM shows the difference between the shapes of cones fanned at the boundary and at the center of the ablated area after 1,000 laser pulses.

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Detailed Morphology and Texture of Microlites in Obsidian observed through Electron Microscopy (전자현미경을 이용한 흑요석 내 미세결정의 형태와 조직 관찰)

  • Jwa, Yong-Joo;Hwang, Ga-hyun
    • Journal of the Korean earth science society
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    • v.39 no.6
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    • pp.568-574
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    • 2018
  • Microlite is crystallized under the supercooled condition of volcanic magma. This study reports the morphology and texture of microlites included in the obsidians from the Baekdusan (Mt. Baekdu), Kyushu (Japan), Hokkaido (Japan) and Lipari Island (Italy) by using a scanning electron microscope (SEM). Morphology and texture observed from the back scattered electron (BSE) image could give more detailed information on the microlite crystallization which cannot be acquired from the conventional optical microscope. Ten types of microlites are newly described according to the 14 morphological types of microlites by Clark (1961): Lath, Crenulite, Bacillite, Margarite, Belonites, Trichites, Arculites, Furculite, Scopulites, Scopulitic growth. Detailed description of the ten microlites can be used to interpret the crystallization and paragenetic relations of crystals during the cooling of acidic volcanic magma.