• Title/Summary/Keyword: salt bath

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Effect of Fluoride Conversion Coating on the Corrosion Resistance and Adhesion of E-painted AZ31 Magnesium Alloy

  • Fazal, Basit Raza;Moon, Sungmo
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.124.2-124.2
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    • 2016
  • Corrosion resistance and adhesion of electro-paint (E-paint) with fluoride conversion coating (FCC) on AZ31 Mg alloy were studied. Corrosion resistance and adhesion were studied as a function of FCC-treatment time and concentration of FCC-bath. Aqueous hydrogen fluoride (HF) solutions, with concentrations ranging from 0.5 M to 5 M, were used to form FCC on chemically polished AZ31 Mg alloy samples for six different times; 10, 30, 60, 90, 120, and 180s. The results from salt spray test (SST) showed that corrosion resistance of E-paint appeared to decrease with increasing FCC treatment times in low concentration FCC baths. The number of blisters formed on the FCC-treated samples increased with increasing FCC treatment time of more than 1 min in low concentration (0.5 M to 1 M) solutions. On the other hand, samples treated in the 5 M HF solution for 120s showed no delamination or blistering even after 1200h of SST.

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Effects of Alloying Elements and Pro-eutectoid Ferrite on Mechanicl Properties in Medium Carbon Steels (중탄소강에서 합금원소 및 초석 페라이트가 기계적성질에 미치는 영향)

  • 심혜정;송형락;남원종
    • Transactions of Materials Processing
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    • v.13 no.4
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    • pp.350-358
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    • 2004
  • The effects of alloying elements on microstructural features and mechanical properties in 0.55%C medium carbon steels were investigated. The samples were austenitized at 105$0^{\circ}C$ for 30min. followed by quenching in a salt bath in the temperature range of 500 ~ $620^{\circ}C$. The addition of Cr resulted in the decrease of the volume fraction of pro-eutectoid ferrite and interlamellar spacing in pearlite and the increase of strength. However, the addition of B caused the increase of the volume fraction of pro-eutectoid ferrite. Reduction of area and Charpy impact values were influenced by the combined effect of microstructural features, such as the volume fraction of pro-eutectoid ferrite, interlamellar spacing and the thickness of lamellar cementite in pearlite.

The Formation Rate and Activation Energy of Diffusion Layer and Compound Layer in Ion-Nitriding (이온질화 에 있어 확산층 및 합성층 의 생성속도 및 질소 의 활성화에너지)

  • 성환태;유봉환;조규식
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.8 no.5
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    • pp.476-480
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    • 1984
  • This paper deals with nitrogen diffusion velocity and activation energy in diffusion layer and compound layer in ion-nitriding, and presents observations on the effect of deformation according to nitriding methods. During the experiment the activation energy and diffusion velocity of nitrogen have been examined in S45C steel samples. It is found that the results of an investigation correspond with the theoretical data and the ion-nitriding method offers less deformation than conventional salt-bath method of nitriding.

The Sliding Wear Characteristics of Ion-Nitrided Steel (이온질화 처리강 의 미끄름 마멸 특성)

  • 유봉환;성환태;조규식
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.8 no.3
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    • pp.217-223
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    • 1984
  • An attempt is made to predict the wear behavior of ion-nitrided metal, when wear arises from asperity interactions. The analysis demonstrates that wear mechanisms are not inconsistent with observed behavior, indicates and approaches to a better appreciation of the effects of such factors as nitrided layer formation and surface topographical features. It was found on ion-nitriding that penetration rate and case development are faster and wear properties of the final product are more improved than conventional gas and salt-bath methods of nitriding.

A Research for Facilities of HAN ZEONG MAG and Actual Condition of It's Use (한증막(汗蒸幕)의 시설 및 이용 실태 조사)

  • Lee, Kyung-Hee;Park, Hung-Ki
    • Journal of Korean Physical Therapy Science
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    • v.1 no.1
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    • pp.187-194
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    • 1994
  • The Han Zeong Mag was the typical hydro-therapy of Korea. It looks like hot air bath of western physical therapy. It developed out of the CHO-SEON, King SE JONG(1422). It is warmed fire of pine wood in the room. At first, it runs a temperature about a few hundred and drop to $80^{\circ}C$ through 12 hours then the room air is exceeding dry. After 12h. reheated in the room. Women makes use of that place with bare body. Because for use salt rub of skin. They have low back pain, pain of muscle, muscle spasm, swelling of arthritis, stiffness of joint and it takes effect on the cosmetic of skin. The treatment effect was excellent to pain(28%), next arthritis(25%). But they have not order for treatment of a doctor. It's dangers of heat stroke and heart disease. Imtortant, must educated method of it's use and danger when it's bad use.

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A Study on Surface Case Hardening of Blend Heat Treated Mild Steel (복합열처리(複合熱處理)한 연강(軟鋼)의 표면경화(表面硬化)에 관한 연구)

  • Chung, In-Sang;Chon, Hae-Dong;Sin, Soug-Mok
    • Journal of the Korean Society for Heat Treatment
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    • v.5 no.1
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    • pp.23-31
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    • 1992
  • It is investigated that Fe-C-N compound layer, defusion layer, and induction hardened layer produced by nitrocarburizing blend heat treatment in austenitic temperature with high frequency induction heating of mild steel specimen sprayed sursulf salt-bath. As the temperature of blend-heat treatment got increased, the thickness and hardness of compound layer and diffusion layer were increased. Compound layer(max. $35{\mu}m$), diffusion layer (max. 2.5mm) and induction hardened layer were gained in the shortest time 10 sec and in the case of $1000^{\circ}C$ total hardness depth of those was about 3.5mm. When the blend-heat treated specimen was reheated, maximum hardness of compound layer was dropped more than that of the reheated compound layer after sursulf treated, whereas hardness of diffusion layer was increased.

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Refining of Manganese from Anode Slime of Electrolytic Zinc and Waste Dry Cell (전해아연의 Anode Slime과 건전지의 폐기물로부터 금속망간의 회수)

  • Yoon, Byoung-Ha;Kim, Dai-Ryong
    • Journal of the Korean institute of surface engineering
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    • v.19 no.1
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    • pp.13-19
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    • 1986
  • Manganese in the Anode slime and the paste-positive material of waste-dry cell was recovered by leaching with the hydrochloric acid solution. The impurities (Zn, Fe, Pb), co-leached with manganese were removed from the leached solution prior to electrolysis by hydrometallurgical techniques such as the neutralization with ammonium hydroxide and cementation on manganese powder. The electrodeposition of manganese from the purified chloride solution with sodium selenate was performed. Cathode current efficiency was found to be affected significantly by the concentration of sodium selenate and ammonium chloride salt, bath temperate, current density and PH. The current efficiency of about 88.7% was obtained by electrolysis manganese chloride solution with sodium selenate (0.1/g) at 10$^{\circ}C$.

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Effect of Cold Reduction Ratio on Spheroidization Rate of High Carbon Steel Sheet (고탄소강 열연판재의 냉간압하율에 따른 구상화 속도)

  • Lee, K.D.;Ha, T.K.;Jeong, H.T.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.543-546
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    • 2008
  • In the present study, the effect of cold reduction ratio on the spherodization rate of SK85 high carbon steel sheet was investigated. High carbon steel sheet fabricated by POSCO was soaked at $800^{\circ}C$ for 2 hr in a box furnace and then treated at $570^{\circ}C$ for 5 min in a salt bath furnace followed by water quenching to obtain a fine pearlite structure. Cold rolling was conducted on the sheets of fine pearlite by reduction ratios of 20, 30, and 40 % and heat treatment for spheroidization was carried out at $720^{\circ}C$ for the various time intervals from 0.1 to 32 hrs. Area fraction of spheroidized cementite was measured with an image analyzer as a function of cold reduction ratios and duration times.

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Microstructural Factors on Ductility in Steels containing Pearlite (펄라이트 함유강에서 연성에 영향을 미치는 미세조직 인자)

  • 심혜정;송형락;남원종
    • Transactions of Materials Processing
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    • v.13 no.5
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    • pp.415-421
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    • 2004
  • The effect of transformation temperature on microstructural features and their effects on ductility in 0.55%C steels were investigated, compared with in 0.82%C eutectoid steel. The samples were austenitized at 100$0^{\circ}C$ for 30min. followed by quenching in a salt bath in the temperature range of 500 ~ $620^{\circ}C$. It was found that reduction of area(RA) increased with increasing transformation temperature and then, decreased after reaching its maximum value in steels containing pro-eutectoid ferrite less than 6%. The thickness of lamellar cementite was found to be the main factor controlling RA. Additionally, the presence of cementite thickness for the maximum ductility in all the tested steels was observed as about 0.015${\mu}{\textrm}{m}$ for tested steels.

BORIDING OF STEEL WITH PECVD METHOD

  • Lee, M.J.;Lee, K.Y.;Lee, J.H.;Kim, Y.H.
    • Journal of the Korean institute of surface engineering
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    • v.32 no.3
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    • pp.249-252
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    • 1999
  • Boriding is one of the chemical method to increase surface hardness as well as carburizing, and nitriding. Gas boriding and boron paste boriding methods were investigated to replace salt bath boriding. Boron paste boriding method is selected due to safety, small waste and low cost. And then boriding is also carried out micro-pulsed PECVD in order to increase efficiency of boriding. Mechanical properties, microstructure, surface concentration, and depth profile of borided layer is investigated by micro-vickers hardness tester, SEM, XRD, and AES.

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