• Title/Summary/Keyword: salt analysis

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Investigation on Dissolution and Removal of Adhered LiCl-KCl-UCl3 Salt From Electrodeposited Uranium Dendrites using Deionized Water, Methanol, and Ethanol

  • Killinger, Dimitris Payton;Phongikaroon, Supathorn
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.18 no.4
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    • pp.549-562
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    • 2020
  • Deionized water, methanol, and ethanol were investigated for their effectiveness at dissolving LiCl-KCl-UCl3 at 25, 35, and 50℃ using inductively coupled plasma mass spectrometry (ICP-MS) to study the concentration evolution of uranium and mass ratio evolutions of lithium and potassium in these solvents. A visualization experiment of the dissolution of the ternary salt in solvents was performed at 25℃ for 2 min to gain further understanding of the reactions. Aforementioned solvents were evaluated for their performance on removing the adhered ternary salt from uranium dendrites that were electrochemically separated in a molten LiCl-KCl-UCl3 electrolyte (500℃) using scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS). Findings indicate that deionized water is best suited for dissolving the ternary salt and removing adhered salt from electrodeposits. The maximum uranium concentrations detected in deionized water, methanol, and ethanol for the different temperature conditions were 8.33, 5.67, 2.79 μg·L-1 for 25℃, 10.62, 5.73, 2.50 μg·L-1 for 35℃, and 11.55, 6.75, and 4.73 μg·L-1 for 50℃. ICP-MS analysis indicates that ethanol did not take up any KCl during dissolutions investigated. SEM-EDS analysis of ethanol washed uranium dendrites confirmed that KCl was still adhered to the surface. Saturation criteria is also proposed and utilized to approximate the state of saturation of the solvents used in the dissolution trials.

Thermal dehydration tests of FLiNaK salt for thermal-hydraulic experiments

  • Shuai Che;Sheng Zhang;Adam Burak;Xiaodong Sun
    • Nuclear Engineering and Technology
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    • v.56 no.3
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    • pp.1091-1099
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    • 2024
  • Fluoride-salt-cooled High-temperature Reactor (FHR) is a promising nuclear reactor technology. Among many challenges presented by the molten fluoride salts is the corrosion of salt-facing structural components. Higher moisture contents, in the FLiNaK (LiF-NaF-KF, 46.5-11.5-42 mol%) salt, aggravate intergranular corrosion and pitting for the given alloys. Therefore, several thermal dehydration tests of FLiNaK salt were performed with a batch size suitable for thermal-hydraulic experiments. Thermogravimetric Analysis (TGA) was performed for the three constituent fluoride salts individually. Preliminary thermal dehydration plans were then proposed for NaF and KF salts based on the TGA curves. However, the dehydration process may not be required for LiF since its low mass loss (<1.3 wt%). To evaluate the performance of these thermal dehydration plans, a batch-scale salt dehydration test facility was designed and constructed. The preliminary thermal dehydration plans were tested by varying the heating rates, target temperature, and holding time. The sample mass loss data showed that the high temperatures (>500 ℃) were necessary to remove a significant amount of moisture (>1 wt%) from NaF salt, while relatively low temperatures (around 300 ℃) with a long holding time (>10 h) were sufficient to remove most of the moisture from KF salt.

An Effective Defensive Response in Thai Aromatic Rice Varieties(Oryza sativa L. spp. indica) to Salinity

  • Cha-um, Suriyan;Vejchasarn, Phanchita;Kirdmanee, Chalermpol
    • Journal of Crop Science and Biotechnology
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    • v.10 no.4
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    • pp.257-264
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    • 2007
  • Rice is one of the world's staple crops and is a major source of carbohydrate. Rice is exported from several countries, providing a major source of income. There are many documents reporting that rice is a salt-sensitive crop in its developmental stages. The objective of this investigation is to evaluate the effective salt-tolerance defense mechanisms in aromatic rice varieties. Pathumthani 1(PT1), Jasmine(KDML105), and Homjan(HJ) aromatic rice varieties were chosen as plant materials. Rice seedlings photoautotrophically grown in-vitro were treated with 0, 85, 171, 256, 342, and 427 mM NaCl in the media. Data, including sodium ion$(Na^+)$ and potassium ion$(K^+)$ accumulation, osmolarity, chlorophyll pigment concentration, and the fresh and dry weights of seedlings were collected after salt-treatment for 5 days. $Na^+$ in salt-stressed seedlings gradually accumulated, while $K^+$ decreased, especially in the 342-427 mM NaCl salt treatments. The $Na^+$ accumulation in both salt-stressed root and leaf tissues was positively related to osmolarity, leading to chlorophyll degradation. In the case of the different rice varieties, the results showed that the HJ variety was identified as being salt-tolerant, maintaining root and shoot osmolarities as well as pigment stabilization when exposed to salt stress or $Na^+$ enrichment in the cells. On the other hand, PT1 and KDML105 varieties were classified as salt-sensitive, determined by chlorophyll degradation using Hierarchical cluster analysis. In conclusion, the HJ-salt tolerant variety should be further utilized as a parental line or genetic resource in breeding programs because of the osmoregulation defensive response to salt-stress.

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Soil Factors Affecting the Plant Communities of Wetland on Southwestern coast of Korea (한국 서남해안 습지의 식물 군집에 미치는 토양요인)

  • 임병선;이점숙
    • The Korean Journal of Ecology
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    • v.21 no.4
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    • pp.321-328
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    • 1998
  • To describe the major environmental factors operating in coastal wetland and to characterize the distribution of the plant species over the wetland in relation to the major environmental gradients, 12 soil physical and chemical properties were determined. The gradient of water and osmotic potential of soil, electrical conductivity, sodium and chloride content and soil texture alsong the three habitat types of salt marshes, salt swamp and sand dune were occurred. The 24 coastal plant communities from principal component analysis (PCA) on the 12 variables were at designated as a gradient for soil texture and water potential related with salinity by Axis I and as a gradient for soil moisture and total nitrogen gradient by Axis II On Axis I were divided into 3 groups (1) 9 salt marsh communities including Salicornia herbacea communities (2) 5 salt swamp communities including Scirpus fluviatilis communities and (3) 10 sand dune communities including Jmperata cylindrica communities on Axis II were divided into 2 groups (1) salt marsh and sand dune communities, and (2) 3 salt swamp communities. The results could account for the zonation of plant communities on coastal wetland observed alsong envionmental gradients.

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Evaluation of Physico-chemical and Textural Properties, and Sensory Evaluation of No-fat Sausages Manufactured with Various Salt Levels

  • Lee, Hong-C.;Chin, Koo-B.
    • Proceedings of the Korean Society for Food Science of Animal Resources Conference
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    • 2004.05a
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    • pp.239-241
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    • 2004
  • pH, proximate analysis and functional properties were not significantly affected by reduced salt levels in NFS which contained 75${\sim}$76% moisture, 14${\sim}$15% protein < 0.5% fat in the final products. However, NFSs had differences in color and EM (%) values as compared to RFS, The results of textural test showed that they were not different with reduced salt levels (0.75${\sim}$1.5%) among the RFS and no-fat treatments (P>0.05). NFS containing 1.0% salt had similar sensory color, flavor and saltiness values to those RFS. These results indicated that NFSs was successfully manufactured with 1.0% salt level and these may contribute to the 'healthier meat products' for consumers due to no-fat and low-salt meat products.

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The Distribution Characteristics of Salt Contaminants in West Coast Region with the Distance from Sea (해안도달 거리에 따른 서해안 지역 염해 오손물의 분포특성)

  • Choi, Nam-Ho;Han, Sang-Ok
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.50 no.6
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    • pp.276-280
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    • 2001
  • This paper presents the result of a study on the distribution characteristics of salt contaminants in the west coast region, from Inchon to Yearsoo, of South Korea. To evaluate the distribution characteristics of salt contaminants, we had measured the equivalent salt deposit density(ESDD) with brush wiping method for thirteen month(from May 1999 to June 2000). Under the consideration on the measuring interval and method, normalization method was applied for the ESDD data. Besides the measurement, the chemical analysis (chromatography) was carried to investigate the relationship, between the electrical property and the amount of specific ingredient, such as sodium, magnesium and chloride. From the result, we could get the representative value of contamination for each site and distribution characteristics of salt contaminants with the distance from sea in the west coast.

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Analysis of Salt Contamination on the Location and the Distance from the coastline (지역 및 해안거리에 따른 염분오손 분석에 관한 연구)

  • Kim, Chan-Young;Kim, Dong-Myung;Kwon, Tae-Ho;Chun, Sung-Nam;Ko, Dong-Hyeon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.511-512
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    • 2006
  • The salt contamination on the distribution facilities is one of the major concern areas because more than 90% of salt contaminated failure occurs in distribution facilities. The periodic measurement of the Equivalent Salt Deposit Density(ESDD) is essential to manage and operate the power line. The ESDD has taken from the 112 position which is located on the coastline of the Korean Peninsula. The ESDD will be presented with the location and the distance from the coastline.

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Comparison of endotracheal intubation speed and ease by using the supraglottic airway laryngopharyngeal tube: A manikin study (성문위기도기 인후두튜브(SALT)를 이용한 기관내삽관 신속성과 용이성 비교: 마네킨을 이용한 연구)

  • Yun, Seong-Woo
    • The Korean Journal of Emergency Medical Services
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    • v.19 no.2
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    • pp.29-38
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    • 2015
  • Purpose: The purpose of this study was to improve airway management ability by comparing the speed, angle of the neck, and confidence and ease of supraglottic airway laryngopharyngeal tube (SALT) and endotracheal intubation via direct laryngoscopy. Methods: The subjects of this experimental research study with a randomized crossover design were 44 emergency medicine technician - paramedics working in the fire department of 'J' - do. SPSS version 19.0 was used in the statistical analysis. Results: Speed and angle of the neck (p<.001), as well as confidence and ease (p<.001), showed significant differences between endotracheal intubation with a SALT and endotracheal intubation via direct laryngoscopy. Conclusion: If endotracheal intubation via direct laryngoscopy is difficult to use or in trauma patients, using a SALT is safe and enables fast intubation. Moreover, in order to improve the efficiency of advanced airway management, the application of SALT should be introduced in the domestic scene.

Selection and Genetic Relationship of Salt Tolerant Rice Mutants by in vitro Mutagenesis

  • Song, Jae Young;Kim, Dong Sub;Lee, Myung-Chul;Lee, Kyung Jun;Kim, Jin-Baek;Kim, Sang Hoon;Yun, Song Joong;Kang, Si-Yong
    • Journal of Radiation Industry
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    • v.4 no.4
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    • pp.307-312
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    • 2010
  • Plants have evolved physiological, biochemical and metabolic mechanisms to increase their survival under the adverse conditions. This present study has been performed to select salt-tolerant rice mutant lines through in vivo and in vitro mutagenesis with gamma-rays. For the selection of the salt-tolerant rice mutants, we conducted three times of selection procedure using 1,500 gamma ray mutant lines resulted from an embryo culture of the original rice cv. Dongan (wild-type, WT): first, selection in the a nutrient solution with 171 mM NaCl; second, selection under in vitro condition with 171 mM NaCl; and third, selection in a reclaimed saline land. Based on a growth comparison of the entries, out of the mutant lines, two putative 2 salt tolerant (ST) rice mutant lines, ST-87 and ST-301, were finally selected. The survival rate of the WT, ST-87 and ST-301 were 36.6%, 60% and 66.3% after 7 days in 171 mM NaCl treatment, respectively. The WT and two salt tolerant mutant lines were used to analyze their genetic variations. A total of 21 EcoRI and Msel primer combinations were used to analyze the genetic relationship of among the two salt-tolerant lines and the WT using the ABI3130 capillary electrophoresis system. In the AFLP analysis, a total of 1469 bands were produced by the 21 primer combinations, and 700 (47.6%) of them were identified as having polymorphism. The genetic similarity coefficients were ranged from 0.52 between the ST-87 and WT to 0.24 between the ST-301 and the WT. These rice mutant lines will be used as a control plot for physiological analysis and genetic research on salt tolerance.

Reuse of Sodium Sulfate Recovered from Farm Drainage Salt as Dyeing Builder of Levelling Dyes - Analysis of Color Difference -

  • Jung, Jiyoon
    • The International Journal of Costume Culture
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    • v.6 no.1
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    • pp.11-18
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    • 2003
  • Agricultural drainage salt generated during irrigation of crops in San Joaquin Valley, California, exceeds 600,000 tons annually and cumulates in the field in a rapid rate. As a result, the waste is taking out more farmlands for salt storage and disposal, imposing serious concerns to environment and local agricultural industry. In searching for a potential solution to reduce or eliminate the waste, this research explored feasibility of producing a value-added product, sodium sulfate, from the waste and utilizing the product in textile dyeing. The results indicated that sodium sulfate could be produced from the salt and could be purified by a recrystallization method in a temperature range within the highest and lowest daily temperatures in summer in the valley. The recovered sodium sulfate samples, with purities ranging from 67% to 99.91, were compared with commercially available sodium sulfate in the dyeing of levelling dyes. In nylon fabrics, the salt samples had little color difference in the dyeing with C.I. Acid Yellow 23 and C.I. Acid Blue 158. All salt samples' gray scale was 5 grade. In wool fabrics, the salt samples had little color difference in dyeing with C.I. Acid Yellow 23 and C.I. Arid Blue 158. All salt samples' gray scale was 5 grade. Generally, the dyeing of levelling dyes using recovered salts from farm drainage had little color difference than the dyeing of levelling dyes using commercial sodium sulfate.

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