• Title/Summary/Keyword: rotary viscometer

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The Transesterification Prediction of Vegetable Oils Based on Viscosity Changes (점도변화에 의한 식물유의 전이 에스테르화 추산)

  • Hyun, Young-Jin;Kim, Hae-Sung
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.1
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    • pp.12-18
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    • 2006
  • The transesterification of vegetable oils into Biodiesel at $60^{\circ}C$ was performed on the rotary viscometer. The overall yield(%) of fatty acid methyl ester from canola oil at optimum conditions was 95%. The viscosities of fatty acid methyl esters were predicted by Orrick and Erbarr's model. The overall yield increased as the viscosities of fatty acid methyl esters decreased. The limiting molar ratio of methanol to oil appeared to be 1:5. The content of sodium hydroxide as the optimum catalyst appeared to be 0.5wt%.

Effects of Acetic Acid Concentration on Rheological Characteristics and Emulsion Stability of Mayonnaise (마요네즈의 유동 특성과 유화 안정성에 미치는 초산 농도의 영향)

  • 배효미;오명숙
    • Korean journal of food and cookery science
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    • v.5 no.1
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    • pp.9-13
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    • 1989
  • The effect of acetic acid concentration on the qualities of mayonnaise was studied. The rheological properties, emulsifying stability and color of the mayonnaise were determined by rotary viscometer, rotary shaker and centrifuge, and color and color difference meter, respectively. The rheological behavior of mayonnaise showed plastic behavior with yield stress and that of shear thinning. The yield stress and consistency index increased as the acetic acid concentration increased. The emulsion stability was lowest at 4% acetic acid concentration and highest at 1% acetic acid concentration. With the increase of the acetic acid concentration, lightness increased and yellowness decreased.

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Acoustic Viscosity Characteristics of Oils with High Molecular Weight VI Improver Additives (고분자량 점도지수향상제가 첨가된 오일의 음향점도 특성)

  • Kong, H.;Ossia, C.V.;Han, H.G.
    • Tribology and Lubricants
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    • v.25 no.4
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    • pp.236-242
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    • 2009
  • Oil viscosity is one of the important parameters for machinery condition monitoring. Basically, it is expressed as kinematic viscosity measured by capillary flow and dynamic or absolute viscosity measured by rotary shear viscometry. Recently, acoustic wave techniques appear in the market, measuring viscosity as the product of dynamic viscosity and density. For Newtonian fluids, knowledge of density allows conversion from one viscosity parameter to the other at a specific shear rate and temperature. In this work, oil samples with different chain lengths of viscosity index (VI) improvers and concentrations were examined by different viscometric techniques. Results showed that acoustic viscosity measurements give misleading results for oil samples with high molecular weight VI improvers and at low temperatures ${\leq}40^{\circ}C$.

Experimental study on types of polycarboxylate superplasticizers and their on the rheological properties of the cement paste (폴리카본산계 고성능 감수제의 종류와 시멘트 페이스트의 레올로지 특성에 미치는 영향에 관한 실험적 연구)

  • Ko, Hye-Bin;Kong, Tae-Woong;Cho, In-Sung;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.11a
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    • pp.81-82
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    • 2020
  • Cement paste is the basic material constituting concrete and the most basic data of workability. This study quantitatively evaluated the measured data using a ring flow and a rotary viscometer to estimate the flow of cement paste, and also evaluated the flow and rheology over time. For this, the current work has studied admixtures that affect the fluidity of cement paste. As a result of the experiment, since fluidity and plastic viscosity are inversely proportional to each other, more experimental studies are needed to obtain high fluidity and high viscosity at the same time.

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Rheological behavior study of Marine Lubricating oil on the amount of MGO (Marine Gas Oil) dilution (해상용 경유의 희석량에 따른 선박용 윤활유의 유변학적 거동연구)

  • Song, In Chul;Lee, Young Ho;Yeo, Young Hwa;Ahn, Su Hyun;Kim, Dae il
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.22 no.2
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    • pp.240-245
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    • 2016
  • This paper describes the rheological behavior study such as viscosity and change of shear stress regarding marine lubricating oil according to the amount of Marine Gas Oil (MGO) dilution. The viscosity reduction due to fuel dilution is crucially important characteristic to decreasing engine durability because of the abrasion of piston ring or liner. The lubricating oil used in this paper was blended with magnetic stirrer diluted High Sulfur Diesel (HSD, 0.05 wt%) ratio of 3 %, 6 %, 10 %, 15 % and 20 %. The viscosity and shear stress of diluted lubricating oil were measured with the temperature range from $-10^{\circ}C$ to $80^{\circ}C$ using a rotary viscometer (Brookfield Viscometer). As the amount of MGO dilution increasing in lubricating oil, the viscosity and stress of those decreased, because the lubricating oil diluted MGO with low viscosity show the trends to decreased viscosity and shear stress. Especially, the viscosity and shear stress of lubricating oil radically decreased at low temperature ($0{\sim}-10^{\circ}C$) and doesn't effect in MGO dilution at over $40^{\circ}C$. As temperature risen, the reduction of the viscosity and shear stress in lubricating oil shows the Newtonian behavior. The lubricating oil was required to check up periodically to improve engine durability since the viscosity reduction by MGO dilution accelerating the engine abrasion.

Experimental Study on the Viscosity Characteristics of Diluted Engine Oils with Diesel Fuel (경유혼입 디젤엔진오일의 점도특성에 관한 실험적 연구)

  • Kim, Chung-Kyun;Kim, Han-Goo
    • Tribology and Lubricants
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    • v.24 no.1
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    • pp.1-6
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    • 2008
  • An experimental study was conducted to evaluate the viscosity characteristics of multi-grade engine oils in which contain diesel fuels. Unused engine oils of SAE 5W40, 10W40 and 15W40 were blended with a diesel fuel ratio of 5%, 10%, and 15%. The viscosity of a diluted engine oil was measured with temperature variation ranging from $-20^{\circ}C$ to $120^{\circ}C$ using a rotary viscometer. The diluted engine oil in which is blended to a diesel fuel plays an important role for decreasing an engine oil viscosity, which may decrease the oil film thickness and a load-carrying capacity. Test results show that the viscosity tends to fall for the increased temperature when engine oil is mixed with a diesel fuel. Especially, the viscosity at a low temperature zone is radically decreased compared with a high temperature zone. Based on the experimental results, the empirical equation that can predict the viscosity of diluted engine oil is expressed in the exponential function with the variation of the temperature and a fuel ratio of diluted engine oil. This equation may be possible to predict the limitation of the oil-fuel dilution rate at the concept design stage of the CDPF system, which doesn't affect the influence of the tribological components.

Fluid dynamical characteristics of microencapsulated phase change material slurries (미립잠열슬러리의 유체역학적 특성연구)

  • 이효진;이승우;이재구
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.11 no.4
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    • pp.549-559
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    • 1999
  • An experimental study was peformed to measure the viscosity of microencapsulated PCM slurries as the functions of its concentration and temperature, and also influence to its fluid dynamics. For the viscosity measurement, a rotary type viscometer, which was equipped with temperature control system, was adopted. The slurry was mixed with water and Sodium Lauryl Sulphate as a surfactant by which its suspended particles were dispersed well without the segregation of particles during the experiment. The viscosity was increased as the concentration of MicroPCM particle added. The surfactant increased 5% of the viscosity over the working fluid without particles. Experiments were proceeded by changing parameters such as PCM particles'concentration as well as the temperature of working fluid. As a result, a model to the functions of temperature for the working fluid and its particle concentration is proposed. The proposed model, for which its standard deviation shows 0.8068, is agreed well with the reference's data. The pressure drop was measured by U-tube manometer, and then the friction factor was obtained. It was noted that the pressure drop was not influenced by the state of PCM phase, that is solid or liquid in its core materials at their same concentration. On the other hand, it was described that the pressure drop of the slurry was much increased over the working fluid without particles. A friction factor was placed on a straight line in all working fluids of the laminar flow regardless of existing particles as we expected.

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Friction Assessment of Canola Oil on Contact Bearing Materials

  • Okechukwu, Nicholas Nnaemeka;Byun, JaeYoung;Kim, JongSoon;Park, JongMin;Kwon, SoonGoo;Chung, SungWon;Kwon, SoonHong;Choi, WonSik
    • Tribology and Lubricants
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    • v.36 no.1
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    • pp.11-17
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    • 2020
  • In manufacturing operations, oil plays a crucial role in reducing friction and wear among interacting surfaces at varying velocities, loads, and temperature. Hydrocarbon oil is considered the origin of lubrication oils. However, this base oil has been limited in its use as it is a principal cause of pollution. This research focuses on identifying a biodegradable base oil lubricant that possesses a stable coefficient of friction and viscosity with temperature. Friction analysis is conducted by employing a pin on a disk tribotester with a fixed load of 10 N at varying sliding speeds ranging from 0.06 m/s to 0.34 m/s. Oil viscosity analysis is perfomed at room temperature by using a rotary viscometer. Tests are performed using canola oil and paraffin oil as lubricants. The results indicate that the viscosity of canola oil is more efficient than paraffin oil. The non-dimensional characteristic number according to the Stribeck curve reveals an elastohydrodynamic lubrication regime with canola oil lubrication. A comparison of both lubricants reveals that, the friction efficiency of canola oil and paraffin oil does not differ considerably. However, the friction in canola oil is observed to decrease more than that in paraffin oil at an elevated sliding speed. The tests confirm that canola oil is potent in minimizing the friction coefficient of SCM440 bodies interacting with one another as well as acted upon by load.

A Fluidity Experiment of Pre-Mix Cement for Dispersibility Improvement of Mineral Admixture (광물질 혼화재의 분산성 향상을 위한 프리믹스 시멘트의 유동성 실험)

  • Han, Cheon-Goo;Lee, Hai-Ill;Noh, Sang-Kyun;Kim, Ki-Hoon
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.2
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    • pp.90-96
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    • 2009
  • The high rising building construction makes increasing the requirement of high strength concrete. Especially, the workability analysis is related with dispersion of admixture such as SF for improving strength and FA, BS for reducing construction cost and improving durability of Ultra High Strength Concrete which has over 100 MPa of compressive strength is very important. Precisely, decreases dispersion because of lumping situation of each admixture and it causes the workability of admixture is decreased. Therefore, the workability of cement paste is tested for analyze effects of pre-mixed cement for solving those problems with it to this research. The summary of the results are like below. First of all, OBS is increasing workability more than OFS. This result causes that the glassy surface of BS in the OBS is increasing workability and the absorption of admixture of FA in the OFS is decreasing workability. In the case of mixing methods, pre-mixing method is increasing workability more than normal one. This result shows that the normal mixing method is bad dispersion of binders. The other side, the pre-mixing method is good. Furthermore, depending on the mixing time, according to the increasing mixing time such as 30, 60, and 120 seconds, the dispersion of binders and workability turns better.

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The Rheology of Cement Paste Using Polycarboxylate-Based Superplasticizer for Normal Strength-High Fluidity Concrete (보통강도 고유동 콘크리트용 PC계 고성능 감수제를 사용한 시멘트 페이스트의 레올로지 특성 평가)

  • Kong, Tae-Woong;Lee, Han-Seung
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.9 no.3
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    • pp.276-286
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    • 2021
  • General high fluidity concrete is the area of high strength concrete with a high amount of cement to secure the required fluidity and workability. Since most of the concrete structures currently used have normal strength, there is a limit to the practical expansion and practicality of use. Thus it is necessary to develop normal strength-high fluidity concrete with low binders that can be used not only in general buildings but also in special buildings, and can greatly reduce construction time and save labor costs. This requires to develop and apply the polycarboxylate-based superplasticizer. In this study, PCE was prepared for each combination of starting materials(WR, HB, RT) and the rheological properties of cement paste were analyzed using ringflow cone and a rotary viscometer. As a result, when PCE with a combination of WR 80%, HB 6.5%, and RT 13.5% was applied, the yield stress can be minimized while securing the plastic viscosity at level of the normal strength. In addition, high fluidity due to the high dispersion effect was confirmed.