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Effects of Tempering Treatment on Microstructure and Mechanical Properties of Cu-Bearing High-Strength Steels (템퍼링에 따른 Cu 첨가 고강도강의 미세조직과 기계적 특성)

  • Lee, Sang-In;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.24 no.10
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    • pp.550-555
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    • 2014
  • The present study deals with the effects of tempering treatment on the microstructure and mechanical properties of Cu-bearing high-strength steels. Three kinds of steel specimens with different levels of Cu content were fabricated by controlled rolling and accelerated cooling, ; some of these steel specimen were tempered at temperatures ranging from $350^{\circ}C$ to $650^{\circ}C$ for 30 min. Hardness, tensile, and Charpy impact tests were conducted in order to investigate the relationship of microstructure and mechanical properties. The hardness of the Cu-added specimens is much higher than that of Cu-free specimen, presumably due to the enhanced solid solution hardening and precipitation hardening, result from the formation of very-fine Cu precipitates. Tensile test results indicated that the yield strength increased and then slightly decreased, while the tensile strength gradually decreased with increasing tempering temperature. On the other hand, the energy absorbed at room and lower temperatures remarkably increased after tempering at $350^{\circ}C$; and after this, the energy absorbed then did not change much. Suitable tempering treatment remarkably improved both the strength and the impact toughness. In the 1.5 Cu steel specimen tempered at $550^{\circ}C$, the yield strength reached 1.2 GPa and the absorbed energy at $-20^{\circ}C$ showed a level above 200 J, which was the best combination of high strength and good toughness.

An Experimental and Numerical Analysis on Performance Comparison of a Trigeneration Desiccant System and Conventional Air-conditioning System (Trigeneration 제습공조시스템과 일반공조시스템의 성능 비교 실험 및 수치해석)

  • Kim, Hyoung-Tae;Chae, Jungmin;Cho, Young-Ah;Park, So-jin;Song, Geun-Soo
    • Journal of the Korean Institute of Gas
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    • v.22 no.3
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    • pp.32-37
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    • 2018
  • Recently, the distributed power generation market using natural gas is expected to expand gradually according to the government's future energy conversion policy. Distributed power generation means small power generation source near the power demand site, which has the advantage of reducing the construction costs of the transmission and distribution infrastructure, operating cost and power loss. A typical example of distributed generation using natural gas is the trigeneration system. In this study, we conducted a basic study on the performance analysis of trigeneration desiccant system for dehumidifying / cooling / heating in the air conditioner room by using the cold and engine waste heat energy generated in the trigeneration system. It shows that the system efficiency increases and the energy consumption decreases as the temperature difference between the inlet and outlet of the trigeneration system increases compared with the general air conditioning system.

Fatty Acid Composition Analysis of Major Oil Crops by One-Step Extraction/Methylation Method (일단계 추출 및 메칠화법에 의한 유료작물의 지방산 분석)

  • 김진경;김남희;방진기;이병규;박충범;이봉호
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.45 no.3
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    • pp.211-215
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    • 2000
  • Lipid extraction preceding fatty acid methyl esters preparation for gas-liquid chromatography is time-consuming and cumbersome. We performed one-step extraction/methylation method with a mixture of methanol-heptane-benzene-DMP-H$_2$SO$_4$ without prior fat extraction. The simultaneous digestion and lipid transmethylation takes place at 8$0^{\circ}C$ in a single phase. After cooling till room temperature, two phases are formed. The upper one of the phases contains the fatty acid methyl esters ready for GLC. The fatty acid composition of major industrial crops obtained by the one step extraction/methylation method (method 1 and 2) was almost identical with the fatty acid composition of the pure fats extracted with hexane by the Soxtec instrument (method 3). Due to its simplicity, speed, and reduced organic solvent the one-step extraction/methylation method (method 1 and 2) should be useful to determine overall fatty acid composition, especially in situations where many samples have to be analyzed.

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Physicochemical Properties of Sugar-snap Cookies Prepared with Chrysanthemum indicum Linne Powder (감국 분말을 첨가한 슈거스냅 쿠키의 이화학적 품질 특성)

  • Bae, Hyun-Joo;Lee, Hye-Yeon;Paik, Jae-Eun
    • The Korean Journal of Food And Nutrition
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    • v.22 no.4
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    • pp.570-576
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    • 2009
  • This study investigated the physicochemical characteristics of sugar-snap cookies made with various levels(0, 1.5, 3, 4.5, and 6% w/w) of Chrysanthemum indicum Linne powder. Dough pieces were baked for 11 min at $180^{\circ}C$ in an electrically heated rotary oven. All items were measured after cooling for 1 hour at room temperature. The results were as follows. Dough pH was significantly decreased in the 3%, 4.5% and 6% samples in contrast to the control sample(p<0.001). Furthermore, lightness (L*-value) and spread factor decreased significantly according to increasing Chrysanthemum indicum Linne powder concentration(p<0.001). However, dough density was significantly increased in the 3%, 4.5%, and 6% samples in contrast to the control sample(p<0.001). Likewise, the hardness and redness(a*-value) of the cookies increased significantly with increasing Chrysanthemum indicum Linne powder concentration(p<0.001). However, the moisture content of the dough was not significantly affected by the Chrysanthemum indicum Linne powder concentration. Finally, the powder concentration had positive correlations with dough density(p<0.01) and hardness(p<0.01). However, it had negative correlations with dough pH(p<0.01), lightness(L*-value)(p<0.05), and spread factor(p<0.01). Overall, the results showed that there were significant correlations between Chrysanthemum indicum Linne powder concentration and the physicochemical characteristics of the cookies.

Preparation of PVDF Hollow Fiber Membrane via TIPS (Thermally Induced Phase Separation) and Stretching (열유도 상분리와 연신공정을 이용한 PVDF 중공사막의 제조)

  • Park, Minsoo;Kim, Jinho;Jang, Moonseog;Kim, Sung Soo
    • Membrane Journal
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    • v.24 no.2
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    • pp.158-166
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    • 2014
  • In this research, microporous and bicontinuous poly vinylidene fluoride(PVDF) hollow fiber membranes were prepared via hybrid process of the thermally induced phase separation (TIPS) and stretching method. The mechanism of the membrane preparation is based on liquid-liquid phase separation. The final membranes have characteristic structures which have both bicontinuous and fibrillar morphology by applying the stretching method. They showed quite different structure when compared with the spherulitic or nodular structure from S/L TIPS and bicontinuous structure from L/L TIPS. At first, PVDF hollow fiber precursors were prepared via TIPS method using various kind of diluent mixtures. We used gamma-butyrolacton, dimethyl phthalate (DMP), diethyl phthalate (DEP), dibutyl phthalate (DBP) as diluents. We could make hollow fiber membranes which had porous outer surface or dense outer surface by controling the parameters such as cooling conditions, PVDF concentration and the ratio of diluent mixtures. Finally, these hollow fiber were stretched at room temperature and diluents were extracted by ethanol. Effects of the stretching ratio on the membrane morphology were investigated using scanning electron microscope (SEM), and its effects on water flux, porosity, pore size, roughness and tensile strength were examined.

PTCR Characteristics of Multifunctional Polymeric Nano Composites (PTCR 나노 복합기능 소재의 전류 차단 특성 연구)

  • 김재철;박기헌;서수정;이영관;이성재
    • Polymer(Korea)
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    • v.26 no.3
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    • pp.367-374
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    • 2002
  • Electrical characteristics of crystalline polymer composites filled with nano-sized carbon black particle were studied. The developed composite system exhibited a typical positive temperature coefficient resistance (PTCR) characteristic, where the electrical resistance sharply increased at a specific temperature. The PTCR effect was sometimes followed by a negative temperature coefficient resistance (NTCR) feature with temperature, which seemingly caused by the coagulation of nano-sized carbon black particles in the excessive quantity. The PTCR temperature was controlled by the carbon black content and the external voltage. The change of electric conductivity was shown as a function of carbon black content, and the resistance was constant when the carbon black content was over 20 wt%. The room-temperature resistance was maintained by a repeated heating and cooling. The excellent PTCR characteristic was demonstrated by the low resistance in the initial stage and the instantaneous heating capability.

An Experimental Study on Annulus Muffler of Automobile (자동차용 환상형 소음기에 관한 실험적 연구)

  • Kim, Byoung-Sam;Song, Kyu-Keun;Sim, Sang-Cherl;Cheong, Byeong-Kuk
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2006.11a
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    • pp.217-222
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    • 2006
  • Internal combustion engine is the main source of environmental pollutants and therefore advanced technology is required to reduce harmful elements from the exhaust gases all over the world. Especially, when the exhaust gas is released front the automotive muffler, exhaust noise has many bad influence on the surrounding environment. In order to reduce the exhaust noise, it is necessary that automotive muffler must be designed for best exhaust efficiency. The sound insulation room was installed for the analysis of an acoustics characteristics of the noise from automotive muffler, in this study. Exhaust gas noise, noise distribution characteristics, pressure and temperature of exhaust gas were investigated with the change of annulus temperature of air cooled annulus automotive muffler and cooled annulus automotive muffler. The following results were obtained with this study. From the frequency analysis of automotive muffler, high noise distribution was observed in the range $100{\sim}2000Hz$. It means that the noise in this range has an dominate influence for the overall noise. Noise reduction of automotive muffler was affected by the temperature of annulus. It is caused the result that the high temperature and pressure of exhaust gas are changed lower by the drop of annulus temperature. The tendencies of noise, the temperature and pressure of exhaust gas are similar to the performance curve of engine. Exhaust gas pressure is determined by the r.p.m. of engine and affected by the cooling performance of automotive muffler.

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Operating Criteria of Core Exit Temperature in Nuclear Power Plant with using Channel Statistical Allowance (총채널 불확실도를 적용한 원전 노심출구온도의 운전가능 판정기준)

  • Sung, Je Joong;Joo, Yoon Duk;Ha, Sang Jun
    • Journal of the Korean Society of Safety
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    • v.29 no.6
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    • pp.166-171
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    • 2014
  • Nuclear power plants are equipped with the reactor trip system (RTS) and the engineered safety features actuation system (ESFAS) to improve safety on the normal operation. In the event of the design basis accident (DBA), a various of post accident monitor(PAM)systems support to provide important details (e.g. Containment pressure, temperature and pressure of reactor cooling system and core exit temperature) to determine action of main control room (MCR). Operator should be immediately activated for the accident mitigation with the information. Especially, core exit temperature is a critical parameter because the operating mode converts from normal mode to emergency mode when the temperature of core exit reaches $649^{\circ}C$. In this study, uncertainty which was caused by exterior environment, characteristic of thermocouple/connector and accuracy of calibrator/indicator was evaluated in accordance with ANSI-ISA 67.04. The square root of the sum of square (SRSS) methodology for combining uncertainty terms that are random and independent was used in the synthesis. Every uncertainty that may exist in the hardware which is used to measure the core exit temperature was conservatively applied and the associative relation between the elements of uncertainty was considered simultaneously. As a result of uncertainty evaluation, the channel statistical allowance (CSA) of single channel of core exit temperature was +1.042%Span. The range of uncertainty, -0.35%Span ($-4.05^{\circ}C$) ~ +2.08%Span($24.25^{\circ}C$), was obtained as the operating criteria of core exit temperature.

Optical Preperties of HgS and HgS : Co Crystals and Films (HgS 및 HgS : Co 결정과 박막의 광학적 특성)

  • 박복남;방태환;김종룡;장우선;최성휴
    • Journal of the Korean Vacuum Society
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    • v.5 no.3
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    • pp.213-217
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    • 1996
  • HgS and HgS: Co crystals and films grown by the slow cooling and the chemical bath deposition method were used to measure their crystal structure and their optical absorption spectra. HgS and HgS: Co crystals are hexagonal structure with the lattice constant $a_0=4.155{\AA}$, $c_0=9.505{\AA}$ for HgS and $a_0=4.148{\AA}$, $c_0=9.462{\AA}$ for HgS and $a_0=4.135{\AA}$, $c_0=9.442{\AA}$ for HgS: Co, respectively. The optical energy gap of these crystals are given as 2.040 eV for HgS and 1.900 eV for HgS: Co, and the optical energy gap of these films were 2.440 eV for HgS and 1.940 eV for HgS: Co at room temperature, respectively.

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Formation of Retainted Austenite and Mechanical Properties of 4~8%Mn Hot Rolled TRIP Steels (4~8%Mn 열연 TRIP강의 잔류오스테나이트 생성과 기계적 성질)

  • Kim D. E.;Park Y. K.;Lee O. Y.;Jin K. G.;Kim S. J.
    • Korean Journal of Materials Research
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    • v.15 no.2
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    • pp.115-120
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    • 2005
  • The aim of this research is to develop the TRIP aided high strength low carbon steels using reverse transformation process. The $4\~8\%$ Mn steel sheets were reversely transformed by slow heating to intercritical temperature region and furnace cooling to room temperature. The stability of retained austenite depends on the enrichment of carbon and manganese by diffusion during the reverse transformation. The amount of retained austenite formed after reversely transformed at $625^{\circ}C$ for 6 hrs was about $50\;vol.\%$ in the $8\%Mn$ steel. The change in volume fraction of retained austenite with a holding temperature was consistent with the changes in elongation and the strength-ductility combination. The maximum strength-ductility combination of 40,000 $MPa{\cdot}\%$ was obtained when the $8\%Mn$ steel reversely transformed at $625^{\circ}C$ for 12 hrs. However, it's property was significantly decreased at higher holding temperature of $675^{\circ}C$ resulting from the decrease of ductility.